• 제목/요약/키워드: niobium

검색결과 193건 처리시간 0.023초

분말고속도공구강의 마찰마모특성에 미치는 Nb의 영향 (The Effect of Niobium on Wear and Friction Characteristics of High Speed Steel by Powder Metallurgy)

  • 이한영;백금주;김용진;배종수;홍성현
    • 한국윤활학회:학술대회논문집
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    • 한국윤활학회 1999년도 제29회 춘계학술대회
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    • pp.14-19
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    • 1999
  • In order to evaluate the effect of Nb on wear properties of high speed steel by powder metallurgy(PM-HSS), niobium-alloyed PM-HSS have been prepared by adding 0%, 1%, 3% and 5%Nb to PM-HSS of 6%W-5%Mo-4%Cr-5%V-5%Co presented in the previous paper. Sliding wear test have been conducted in various sliding speed conditions under the constant pressure using a pin-on-disc type machine. The results of this study shows that the wear resistance of PM-HSS has been increased by the addition of Nb in the range of experimental sliding speed. However, the amount of Nb shows to be unimportant parameter for the improvement of the wear resistance. It may be due to the thermal stability of carbide and high temperature properties of matrix by adding Nb comparing to the case of no addition.

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Investigation of Nb-Zr-O Thin Film using Sol-gel Coating

  • Kim, Joonam;Haga, Ken-ichi;Tokumitsu, Eisuke
    • JSTS:Journal of Semiconductor Technology and Science
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    • 제17권2호
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    • pp.245-251
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    • 2017
  • Niobium doped zirconium oxide (Nb-Zr-O:NZO) thin films were fabricated on Si substrates by a sol-gel technique with an annealing temperatures of $500{\sim}1000^{\circ}C$ in air ($N_2:O_2=3:1$) for 20 minutes. It was found that the NZO film is based on tetragonal $ZrO_2$ polycrystalline structure with the Nb 5+ ion state and there is almost no diffusion of Nb or Zr to Si substrate. The relative dielectric constant for the NZO film with the Nb composition of 30 mol% and annealed at $800^{\circ}C$ was around 40. The root mean roughness was 1.02 nm. In addition, the leakage current of NZO films was as low as $10^{-6}A/cm^2$ at 4.4 V.

Niobium과 Cobalt를 첨가한 Multiferroic BiFeO3 박막의 유전 특성 및 자성 특성 (Dielectric and Magnetic Properties of Niobium and Cobalt Co-substituted Multiferroic BiFeO3 Thin Films)

  • 전윤기;홍성현
    • 한국세라믹학회지
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    • 제45권9호
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    • pp.556-560
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    • 2008
  • The effects of Nb and Co ion substitution on the dielectric and magnetic properties of the multiferroic $BiFeO_3$ thin films have been investigated. Heteroepitaxial $BiFeO_3$ thin films were deposited by Pulsed Laser Deposition method. Nb substitution decreased the leakage current by 6 orders of magnitude and Co substituted $BiFeO_3$ thin films showed an enhanced magnetization, 2 times larger than that of un-substituted $BiFeO_3$. Through the co-substitution of Co and Nb, $BiFeO_3$ thin films with a low leakage current and an enhanced magnetization could be obtained.

솔-젤법에 의한 $Pb(Sc_{1/2}Nb_{1/2})O_3$ 분말의 제조 (Preparation of $Pb(Sc_{1/2}Nb_{1/2})O_3$ Powders by the molten salt synthesis method)

  • 박경봉;김태희
    • 한국결정성장학회지
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    • 제7권4호
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    • pp.555-559
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    • 1997
  • lead acetate, scandium acetate, niobium isopropoxide를 전구체로 사용한 솔-젤법으로 $Pb(Sc_{1/2}Nb_{1/2})O_3$ 분말을 제조하였다. 젤 분말에 대한 결정화 거동과 상변화가 연구되었다. 솔-젤법을 이용하여 $700^{\circ}C$에서 1시간 동안 열처리를 행하여 97 % 이상의 매우 순수한 $Pb(Sc_{1/2}Nb_{1/2})O_3$ 상을 얻을 수 있었으며 0.2 $\mu \textrm{m}$ 이하의 평균 입자 크기를 가진 매우 미세한 분말의 제조가 가능하다.

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Mo, Nb첨가가 TiAl합금의 산화에 미치는 영향 (Effect of Mo and Nb on High Temperature Oxidation of TiAl Alloys)

  • 김재운;이동복
    • 한국재료학회지
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    • 제14권9호
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    • pp.614-618
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    • 2004
  • Alloys of $Ti46\%Al-2\%Mo-2\%Nb$ were oxidized between 800 and $1000^{\circ}C$ in air, and their oxidation characteristics were studied. The alloys displayed good oxidation resistance due mainly to the beneficial effects of Mo and Nb. The oxide scales formed consisted primarily of an outer $TiO_2$ layer, an intermediate $Al_{2}O_3-rich$ layer, and an inner mixed layer of ($TiO_{2}+Al_{2}O_3$). Molybdenum and niobium dissolved in the scale effectively improved oxidation resistance. They were mainly distributed in the inner mixed layer of ($TiO_{2}+Al_{2}O_3$).

열기계적 처리한 Ti-45.4%Al-4.8%Nb 합금의 고온산화 (High Temperature Oxidation of Thermomechanically Treated Ti-45.4%Al-4.8%Nb Alloys)

  • 김재운;이동복
    • 한국재료학회지
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    • 제14권7호
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    • pp.457-461
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    • 2004
  • The thermomechanically treated $Ti-45.4\%Al-4.8\%Nb(at\%)$ alloy was oxidized between 800 and $1000^{\circ}C$ in air, and the oxidation characteristics were studied. The dissolution of Nb in the oxide scale was observed from the TEM study. The Pt marker test revealed that the oxidation process was controlled by the outward diffusion of Ti ions and the inward diffusion of oxygen ions. During oxidation, the evaporation of Nb-oxides was found to occur to a small amount. Niobium tended to pile-up at the lower part of the oxide scale, which consisted primarily of an outer $TiO_2$ layer, and an intermediate $Al_{2}O_{3}-rich$ layer, and an inner mixed layer of ($TiO_{2}+Al_{2}O_{3}$).

Ti과 Nb에 의한 HSS 작업롤재의 미세조직 제어 (Microstructural Control of High Speed Steel Roll Material with Titanium and Niobium)

  • 김진수;김동규;최진원;이희춘
    • 한국소성가공학회:학술대회논문집
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    • 한국소성가공학회 1999년도 제3회 압연심포지엄 논문집 압연기술의 미래개척 (Exploitation of Future Rolling Technologies)
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    • pp.262-271
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    • 1999
  • This work was intended to modify the solidification structure of high speed steel roll material for hot strip mill, by the introduction of alloying elements designed to form primary carbide dispersions via melt treatment procedure. Solidification structure was modified by the melt treatment with titanium and distribution. This modifying effect could be attributed to the fact that the nuclie formed at high temperature upon inoculation induce the formation of fine equiaxed grain and primary carbide during solification, which is also likely to be responsible for the fact that TiC acts as effective nuclie for primary VC solidification.

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NaF 전해질 양극산화에 의한 마이크로콘 구조 니오븀 산화물 제조 (Formation of Nb2O5 Microcone Structure in NaF Electrolyte by Anodization)

  • 정봉용;정은혜
    • 한국세라믹학회지
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    • 제48권6호
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    • pp.625-629
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    • 2011
  • In this study, we show that by anodization of Nb in NaF electrolytes microcone niobium oxide layers can be formed under a range of experimental conditions. It is found that a single NaF electrolyte leads to the formation of microcones. At 1 M NaF, 40 V, 1 h, well-ordered microcones were generated on Nb discs. XRD results show that the initially formed anodic oxide is amorphous, but an amorphous to crystalline transition occurs during anodization. For the formation of favorable microcones, it is considered that proper parameters such as electrolyte concentration, voltage, anodizing time are necessary according to the kind of electrolytes.

Effects of Niobium Microalloying on Microstructure and Properties of Hot-Dip Galvanized Sheet

  • Mohrbacher, Hardy
    • Corrosion Science and Technology
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    • 제9권2호
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    • pp.67-73
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    • 2010
  • Niobium microalloying is effective in hot-rolled and cold-rolled steels by providing a fine-grained microstructure resulting in increased strength. To optimize the strengthening effect, alloy design and hot-rolling conditions have to be adapted. As a key issue the dissolution and precipitation characteristics of Nb are discussed in particular with regard to the run-out table conditions. It is then considered how the hot-rolled microstructure and the solute state of Nb interact with the hot-dip galvanizing cycle. The adjusted conditions allow controlling the morphology and distribution of phases in the cold-rolled annealed material. Additional precipitation hardening can be achieved as well. The derived options can be readily applied to produce conventional HSLA and IF high strength steels as well as to modern multiphase steels. It will be explained how important application properties such as strength, elongation, bendability, weldability and delayed cracking resistance can be influenced in a controlled and favorable way. Examples of practical relevance and experience are given.

Line-shaped superconducting NbN thin film on a silicon oxide substrate

  • Kim, Jeong-Gyun;Suh, Dongseok;Kang, Haeyong
    • 한국초전도ㆍ저온공학회논문지
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    • 제20권4호
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    • pp.20-25
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    • 2018
  • Niobium nitride (NbN) superconducting thin films with the thickness of 100 and 400 nm have been deposited on the surfaces of silicon oxide/silicon substrates using a sputtering method. Their superconducting properties have been evaluated in terms of the transition temperature, critical magnetic field, and critical current density. In addition, the NbN films were patterned in a line with a width of $10{\mu}m$ by a reactive ion etching (RIE) process for their characterization. This study proves the applicability of the standard complementary metal-oxide-semiconductor (CMOS) process in the fabrication of superconducting thin films without considerable degradation of superconducting properties.