• 한국분말재료학회지
• /
• 제10권1호
• /
• pp.34-39
• /
• 2003

Porous TiNi bodies were produced by Self-propagating High-temperature Synthesis (SHS) method from a powder mixture of Ti and Ni. Porosity, pore size and structure, mechanical property, and transformation temperature of TiNi product were investigated. The average porosity and pore size of produced porous TiNi body are 63% and $216\mutextrm{m}$, respectively. XRD analysis showed that the major phase of produced TiNi body is B2 phase. Its average fracture strength and elastic modulus measured under dry condition were $22\pm2$ MPa and $0.18\pm0.01$GPa, respectively. It could be strained up to 7.3 %. The transformation temperatures determined by DSC showed the $M_s$ temperature of $67^{\circ}C$ and $A_f$ temperature of $99^{\circ}C$.

• 동력기계공학회지
• /
• 제5권4호
• /
• pp.24-30
• /
• 2001

The substructure synthesis method(SSM) is developed for overcoming disadvantages of the Finite Element Method(FEM). The concept of the SSM is as follows. After dividing a whole structure into several substructures, every substructures are analyzed by the FEM or experiment. The whole structure is analyzed by using connecting condition and the results of substructures. The concept of the transfer stiffness coefficient method(TSCM) is based on the transfer of the nodal stiffness coefficients which are related to force vectors and displacement vectors at each node of analytical mode1. The superiority of the TSCM to the FEM in the computation accuracy, cost and convenience was confirmed by the numerical computation results. In this paper, the author suggests an efficient vibration analysis method of structures by using the TSCM and the SSM. The trust and the validity of the present method is demonstrated through the numerical results for computation models.

• Biomolecules & Therapeutics
• /
• 제16권1호
• /
• pp.28-33
• /
• 2008

Atorvastatin calcium salt (1) was obtained through the preparation of lactone compound (8) from 2-((4R,6R)-6-(2-(2-(4-fluorophenyl)-5-isopropyl-3-phenyl-4-(phenylcarbamoyl)-1H-pyrrol-1-yl)-ethyl)-2-phenyl-1,3,2-dioxaborinan-4-yl)acetic acid tert-butyl ester (9) by hydrolysis in basic condition. Efficient hydrolysis of boronate compound 9 aimed at the viable synthesis for commercial production and purification of Atorvastatin calcium is reported. Detail studies of evaluation procedure are also reported.

• 한국소음진동공학회:학술대회논문집
• /
• 한국소음진동공학회 2006년도 춘계학술대회논문집
• /
• pp.1366-1371
• /
• 2006

A structural coupling method is developed for the dynamic analysis of a nonlinear structure with concentrated nonlinear hinge joints or sliding lines. Component mode synthesis method is extended to couple substructures and the nonlinear models. In order to verify the improved coupling method, a numerical plate model consisting of two substructures and torsional springs, is synthesized by using the proposed method and its model parameters are compared with analysis data. Then the coupling method is applied to a three-substructure-model with the nonlinearity of sliding lines between the substructures. The coupled structural model is verified from its dynamic analysis. The analysis results show that the improved coupling method is adequate for the structural nonlinear analyses with the nonlinear hinge and sliding mode condition.

• 한국정밀공학회지
• /
• 제15권3호
• /
• pp.88-98
• /
• 1998

In many automatization applications, a rigid body is required to go forward and backward repeatedly through a set of given position/orientations precisely while a crank is rotated. Such a motion can be generated by 6 bar mechanism adding a dyad to a 4 bar mechanism. If this is the case for 3 position synthesis of the 4 bar mechanism, the feasible solution area for designing the 4 bar mechanism will be limited over the general solution area. This paper proposes a procedure to synthesize 4 bar mechanism to be used to generate the required motion. It is found that the only input crank of the 4 bar mechanism should be limited to satisfy the condition. And the feasible design area for the circle point/ center point of the input crank is identified so that design of the undesired mechanism could be avoided. The method is tested and the results are shown.

• 한국분말재료학회지
• /
• 제6권1호
• /
• pp.75-80
• /
• 1999

The formation of $n-TiO_2$ powder by oxidation of Ti-ethoxied vapor in a flat flame burner reactor maintained under 20 torr has been studied. The produced powder were characterized in terms of crystal structure, chemical composition by XRD and TEM. The results showed that the powder consisted of loose agglomerated anatase and rutile particles and their size were about 10 nm and 20 nm, respectively. In the course of synthesis, changes of the flame color were happened to each condition during heating up the bubbler. The flame color transition phenomena reveled that a critical precursor delivery rate was needed for the powder formation (obtainable powder yield). The critical precursor delivery rate was estimated by a simple function of the bubbler temperature and the carrier gas flow rate. The critical precursor delivery rate was reviewed as an important variable of the nanopowder synthesis.

• International Journal of Control, Automation, and Systems
• /
• 제6권2호
• /
• pp.171-179
• /
• 2008

This paper addresses the synthesis of an iterative learning controller for a class of linear systems with norm-bounded parameter uncertainties. We take into account an iterative learning algorithm with current cycle feedback in order to achieve both robust convergence and robust stability. The synthesis problem of the developed iterative learning control (ILC) system is reformulated as the ${\gamma}$-suboptimal $H_{\infty}$ control problem via the linear fractional transformation (LFT). A sufficient convergence condition of the ILC system is presented in terms of linear matrix inequalities (LMIs). Furthermore, the ILC system with fast convergence rate is constructed using a convex optimization technique with LMI constraints. The simulation results demonstrate the effectiveness of the proposed method.

• 한국농촌건축학회논문집
• /
• 제8권2호
• /
• pp.62-71
• /
• 2006

This study on the rational planning of water supply and sewage system for rural village development projects. Present, when establishment and standard about maintenance of water supply and sewage system were not presented in rural village synthesis development projects, it is real condition that service industry is depending on presenting simple plan in basis planning phase and business enforcement step. This study wishes to present basic data so that can be planned more rationally and enforce and contribute in rural village synthesis development projects water supply and sewage system that is enforced as part of rural village synthesis development projects.

• Bulletin of the Korean Chemical Society
• /
• 제34권2호
• /
• pp.394-398
• /
• 2013

An efficient process for the synthesis of N-azaaryl anilines via Smiles rearrangement as a tool. A variety of N-azaaryl anilines were generated by the reaction of substituted phenols, substituted anilines, aminopyridines and chloroacetyl chloride or pyridols, under base condition in good to excellent yields.

• 제어로봇시스템학회:학술대회논문집
• /
• 제어로봇시스템학회 1993년도 한국자동제어학술회의논문집(국제학술편); Seoul National University, Seoul; 20-22 Oct. 1993
• /
• pp.138-143
• /
• 1993

A well-defined relative degree, which is one of the basic assumptions in adaptive control or nonlinear synthesis problems, is addressed. It is shown that this is essentially a necessary condition for asymptotic tracking in discrete-time nonlinear systems. To show this, tracking problems are defined, and a local linear input-output behavior of a discrete-time system is introduced in relation to a well-defined relative degree. It is then shown that if a plant is invertible and accessible from the origin and a compensator solves the local asymptotic tracking problem, then the plant necessarily has a well-defined relative degree at the origin.