• Title/Summary/Keyword: Sampling Tube

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Effect of Relative Humidity on the Breakthrough of Charcoal Tubes during Mixed Organic Vapor Sampling (혼합 유기용제 포집시 습도가 활성탄관의 파과에 미치는 영향)

  • Yang, Hyeok Syng;Kim, Hyunwook
    • Journal of Korean Society of Occupational and Environmental Hygiene
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    • v.6 no.1
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    • pp.125-137
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    • 1996
  • This study was designed to investigate effects of relative humidity on the breakthrough of charcoal tubes at a fixed vapor concentration and sampling time during mixed organic vapor sampling. A vapor generator was used to generate three different concentrations of mixed organic vapor and a stainless steel chamber was fabricated and utilized to maintain three different percentages of relative humidity while maintaining a constant temperature. The results were as follows; 1. At high relative humidity, breakthrough of mixed organic vapor occurred quickly at low vapor concentration than at high vapor concentration because of the reduced adsorption volume of charcoal tube due to humidity. 2. Breakthrough by competitive adsorption of vapors onto charcoal tube was observed at first from n-hexane having the lowest boiling point and highest vapor pressure among the three organic vapors investigated, followed by TCE. No breakthrough was observed from toluene under all experimental conditions. 3. For n-hexane, breakthrough was observed after 2 hours of sampling and breakthrough rates were increased as relative humidity increased. For TCE, breakthrough was found after 3 hours of sampling and breakthrough rates by sampling time were increased as vapor concentration increased. 4. The adsorbed amount of mixed organic vapor at breakthrough was shown to have statistically significant correlations with sampling time, relative humidity, and vapor concentration in descending order of correlation. Relative humidity and sampling time for n-hexane and sampling time and concentration for TCE were both statistically significantly correlated. 5. Relative humidity was found to affect the amount of breakthrough of mixed organic vapor and n-hexane. Among three percentages of relative humidity investigated, the amount of breakthrough at 85 % relative humidity was significantly larger than those of at lower percentages of relative humidity. No statistically significant difference was found between 25 % and 55 % relative humidity. 6. The results of multiple regression analysis between breakthrough and relative humidity, vapor concentrations showed that the coefficient of determination of mixed organic vapor was 0.263 and those of n-hexane and TCE were 0.275 and 0.189, respectively. 7. Flow rates of sampling pumps used were found to be affected by relative humidity present. At 25 %, 55 %, and 85 % relative humidity, the relative errors of sampling pump were 1.4 %, 13.4 %, and 18.6 %, respectively. In conclusion, the results of this study showed that high relative humidity could reduce the adsorption volume of charcoal tubes and subsequently increase breakthrough rates. Therefore, to prevent breakthrough when sampling mixed organic vapors, it is suggested that either sampling volume be reduced on the flow rate be lowered so as to minimize breakthrough of the most volatile organic vapor in the mixture. In addition, since the flow rates of a sampling pump can be adversely affected by high relative humidity, it is recommended to use a constant flow mode pump when sampling in the highly humid environment.

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On the Sampling and Transport of Radioactive Aerosols from Waste Thermal Process

  • Yang, Hee-Chul;Kim, Joon-Hyung;Yong Kang
    • Nuclear Engineering and Technology
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    • v.29 no.4
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    • pp.269-279
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    • 1997
  • The errors associated with incorrect sampling and transport of radioactive aerosol from radwaste thermal process off-gas are analyzed and the conditions of representative sampling and correct transport of radioactive aerosol for off-gas system evaluation are discussed. An estimation method of sampling errors for individual radionuclides is proposed and applied to simulated vitrification melter aerosols. Prediction methods for particle deposition in sample transport tube under laminar as well as turbulent flow conditions are also described by example calculations with simulated incinerator off-gas From the results of example calculations and plots, instrumental and operational conditions of radioactive aerosol sampling system with minimized errors and correction methods for nonideal sampling and transport are recommended.

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A study on the cross-section profile of the seal ring in the stern tube sealing system (선미관 밀봉 장치 시일링의 단면 형상에 관한 연구)

  • 남정길
    • Journal of the Korean Society of Fisheries and Ocean Technology
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    • v.35 no.1
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    • pp.50-53
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    • 1999
  • In this paper, the mechanical movement of lip seal-ring which plays the most important function in stern-tube sealing system and the possibility of leakage caused by pressure fluctuation are studied by theory and experiment. By the finite element method for axial symmetry object which receives the torsional bending load, the displacement and stress analysis of the seal-rings are executed for products of several representative manufacturers of seal-rings, and also the possibility of crack occurance are checked by theoretical analysis. A sample seal-ring id designed and manufactured using the program of displacement and stress analysis developed in this study and made an experimental apparatus to test the sampling seal-ring. The sampling seal-ring functioned excellently, but it had its durability and this problem may be solved by using the Viton instead of NBR.

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Dilution methods for combustion aerosol measurement from stationary emission sources: A review (고정 오염원의 연소과정에서 발생하는 먼지를 측정하기 위한 희석방법 연구동향)

  • Woo, Chang Gyu;Kim, Hak-Joon;Kim, Yong-Jin;Han, Bangwoo;Kang, Su Ji;Chun, Sung-Nam
    • Particle and aerosol research
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    • v.13 no.4
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    • pp.165-172
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    • 2017
  • For precise particle measurements in combustion environments, various dilution sampling methods were compared. Dilution equipments using dilution tunnels and hot/cold dilution with porous tube dilutors were most frequently used so far. The combination of porous tube dilutor and ejector diluter has relatively small footprint, and it results in lower particle losses compared to other methods. To determine the portion of condensable particulate matter, proper temperature control and flow control is required.

A Low-Cost Open-Source Air Sampler for the Sorbent Tube Sampling for TD-GC/MS Analysis

  • Jang, Hwa-yong;Oh, Han Bin
    • Mass Spectrometry Letters
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    • v.11 no.4
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    • pp.95-102
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    • 2020
  • In this study, we provide full descriptions of how to make a low-cost and completely open-source laboratory-made air sampler that will be used for sample adsorption for thermal desorption-gas chromatography mass spectrometry (TD-GC/MS) analysis. It is well known that harmful gases cause bad effects on human bodies, so it is necessary to identify the types and amounts of gases in industrial sites. One of the most commonly used methods for gas sampling is to utilize a sorbent tube using an air sampler. Commercially available air samplers are expensive, typically priced between $1,000 and $2,000, and their design often cannot be modified to fit the experiment. To address these shortcomings, we have developed a do-it-yourself (DIY) air sampler that is not only cheap enough, but also completely open-source. Furthermore, the performance of the fabricated air sampler was validated in conjunction with TD-GC/MS for the analysis of volatile compounds.

Advancement of Sequential Particle Monitoring System (측정점 교환방식 미세입자 모니터링 시스템 고도화)

  • An, Sung Jun
    • Journal of the Semiconductor & Display Technology
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    • v.21 no.1
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    • pp.17-21
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    • 2022
  • In the case of the manufacturing industry that produces high-tech components such as semiconductors and large flat panel displays, the manufacturing space is made into a cleanroom to increase product yield and reliability, and various environmental factors have been managed to maintain the environment. Among them, airborne particle is a representative management item enough to be the standard for actual cleanroom grade, and a sequential particle monitoring system is usually used as one parts of the FMS (Fab or Facility monitoring system). However, this method has a problem in that the measurement efficiency decreases as the length of the sampling tube increases. In this study, in order to solve this problem, a multiple regression model was created. This model can correct the measurement error due to the decrease in efficiency by sampling tube length.

Integrity Assessment of Sharp Flaw in CANDU Pressure Tube Using Probabilistic Fracture Mechanics (확률론적 파괴역학을 도입한 CANDU 압력관의 예리한 결함에 대한 건전성평가)

  • Lee, Jun-Seong;Gwak, Sang-Rok;Kim, Yeong-Jin;Park, Yun-Won
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.26 no.4
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    • pp.653-659
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    • 2002
  • This paper describes a probabilistic fracture mechanics(PFM) analysis based on Monte Carlo(MC) simulation. In the analysis of CANDU pressure tube, the depth and aspect ratio of an initial semi-elliptical surface crack, a fracture toughness value and delayed hydride cracking(DHC) velocity are assumed to be probabilistic variables. As an example, some failure probabilities of piping and CANDU pressure tube are calculated using MC method with the stratified sampling MC technique, taking analysis conditions of normal operations. In the stratified MC simulation, a sampling space of probabilistic variables is divided into a number of small cells. For the verification of analysis results, a comparison study of the PFM analysis using other commercial code is carried out and a good agreement was observed between those results.

Influence of Sampling and Preparation Method on Stress-Strain Behavior of Weathered Granite Soils (채취방법과 성형방법이 화강 풍화토의 응력-변형률 거동에 미치는 영향)

  • Cho, Wan-Jei
    • Journal of the Korean Society of Safety
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    • v.25 no.2
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    • pp.55-64
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    • 2010
  • Since various weathered soils are encountered in many domestic construction sites, it is necessary to estimate characteristics of natural weathered soils. However, the remolded sample of weathered soils are commonly used to estimate their characteristics because it is very difficult to sample weathered soils in undisturbed states. However, it is well known that the behavior of remolded sample is different from that of the undisturbed sample particularly in the dynamic response, because the particle structure of undisturbed sample maintains its original structure from the mother rock. Thus, to evaluate the influence of sampling method and preparation method on stress-strain behavior, the resonant column tests were performed on the block, tube samples, remolded samples with static compression and remolded samples with tamping of the weathered granite soils. The shear modulus of the remolded sample with tamping is larger than the other samples presumably due to the high tamping pressure enough to induce particle breakage. The tube samples show larger damping ratios than other samples. Furthermore, one-dimensional ground response analysis was performed to compare the results qualitatively.

A Study on Polynuclear Aromatic Hydrocarbons Emitted by Coking Time and Sampling Method in a Coke Oven Plant (코크스제조공정에서 탄화시간과 시료채취방법에 따른 다핵방향족탄화수소 발생에 관한 연구)

  • Yun, Chung Sik;Paik, Nam Won
    • Journal of Korean Society of Occupational and Environmental Hygiene
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    • v.3 no.1
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    • pp.37-53
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    • 1993
  • The polynuclear hydrocarbons (PAHs) emitted from coke oven standpipe were sampled using three sampling systems, including glass fiber filter+silver membrane filter, glass fiber filter+silver membrane filter+XAD-2 adsorbent tube, PTFE membrane filter+XAD-2 adsorbent tube, extracted by methylene chloride and analysed by gas chromathography using flame ionization detector. The results of this study were as follows. 1. Because the amounts of coke oven emissions(COE) were large, the analyses of PAHs were simple and possible without evaporation and concentration. Although the generation of COE was high during early stage of coking, the airborne concentration of PAHs was low and increased during late coking. 2. The contents of PAHs in COE were 1.35-2.81%. 3. The index components of PAHs were fluoranthene and pyrene. Their correlation coefficient to total PAHs were 0.96, 0.95, respectively. 4. The particulate PAHs were sampled by filter and gaseous PAHs by adsorbent tube. The collection efficiency of glass fiber filter+silver membrane filter was 20% of total amount sampled by filters+adsorbent and PTFE membrane filter 50%. Adsorbent tube must be attached to the filter to collect light and small PAH components. 5. The generation of acenaphthene and indeno (1,2,3-cd) pyrene were low and concentrations of fluorene and anthracene were $20-40ug/m^3$ throughout coking time. Other PAH eoncentrations were sometimes high. The generation of PAHs was low at 4-6 hours of coking time. The gaseous PAHs were generated earlier than particulate PAHs.

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Factors Affecting Hemolysis in Blood Sampling and Repeated Sampling in the Emergency Department (응급실에서의 채혈로 인한 용혈 및 재채혈 관련요인)

  • Cho, Myung Sook;Hwang, Moon Sook
    • Journal of Korean Clinical Nursing Research
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    • v.17 no.3
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    • pp.399-410
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    • 2011
  • Purpose: This study was conducted to investigate the incidence of blood hemolysis and repeated blood sampling and to identify factors contributing to hemolysis and repeated blood sampling in the emergency department. Methods: A cross-sectional descriptive design was used. Participants were the patients who came to emergency department and are required a blood sampling for electrolyte level. All blood samples were collected by emergency department nurses and determined for hemolysis by experienced laboratory technologists. Data were analyzed using $x^2$-test, Fisher's exact test, Mann-Whitney u test and Binary Logistic Regression to determine significant differences. Results: A total of 402 valid samples were collected. Of these, 30 blood samples (7.5%) were found to be hemolyzed and 9 (2.2%) to be recollected. Statistically significant factors affecting on hemolysis and repeated blood sampling included the time of bloods sampling (night), the time of tourniquet application, and too-fast blood draw into the test tube. Conclusion: We recommend that nurses who take the blood sampling to consider the findings of the study and take the related factors into account as they set up the standardized care protocol in order for nursing quality improvement.