• 한국소음진동공학회:학술대회논문집
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• 한국소음진동공학회 2005년도 추계학술대회논문집
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• pp.930-935
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• 2005

In order to synthesis of the materials and modulus for floor impact sound reduction, we investigated effect on dynamic elastic modulus of floor impact sound reduction materials and module made by inorganic porous materials, EVA chips and so on. We find correlation property between dynamic elastic modulus and light-weight impact noise. And we measured the dynamic elastic modulus of materials and module for floor impact sound reduction. And we predicted reduction efficiency on floor Impact Noise of those. The dynamic elastic modulus is reduced by increase of filler contents and filler species. When the materials for floor impact sound reduction is consisted of l5wt% EVA Chip and l5wt% inorganic porous materials, its dynamic elastic material is the lowest. And when the module is consisted of PE (upper side), PS embossing board(lower side) and the materials for floor impact sound reduction(middle), its dynamic elastic material is the lowest.

• 한국재료학회지
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• 제27권8호
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• pp.438-444
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• 2017

In this work, the effects of hydrogen reduction on the microstructure and thermoelectric properties of $(GeTe)_{0.85}(AgSbTe_2)_{0.15}$ (TAGS-85) were studied by a combination of gas atomization and spark plasma sintering. The crystal structure and microstructure of TAGS-85 were characterized by X-ray diffraction(XRD) and scanning electron microscopy (SEM). The oxygen content of both powders and bulk samples were found to decrease with increasing reduction temperature. The grain size gradually increased with increasing reduction temperature due to adhesion of fine grains in a temperature range of 350 to $450^{\circ}C$. The electrical resistivity was found to increase with reduction temperature due to a decrease in carrier concentration. The Seebeck coefficient decreased with increasing reduction temperature and was in good agreement with the carrier concentration and carrier mobility. The maximum power factor, $3.3{\times}10^{-3}W/mK^2$, was measured for the non-reduction bulk TAGS-85 at $450^{\circ}C$.

• 한국분말재료학회지
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• 제31권2호
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• pp.163-168
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• 2024

As the demand for lithium-ion batteries for electric vehicles is increasing, it is important to recover valuable metals from waste lithium-ion batteries. In this study, the effects of gas flow rate and hydrogen partial pressure on hydrogen reduction of NCM-based lithium-ion battery cathode materials were investigated. As the gas flow rate and hydrogen partial pressure increased, the weight loss rate increased significantly from the beginning of the reaction due to the reduction of NiO and CoO by hydrogen. At 700 ℃ and hydrogen partial pressure above 0.5 atm, Ni and Li₂O were produced by hydrogen reduction. From the reduction product and Li recovery rate, the hydrogen reduction of NCM-based cathode materials was significantly affected by hydrogen partial pressure. The Li compounds recovered from the solution after water leaching of the reduction products were LiOH, LiOH·H₂O, and Li₂CO₃, with about 0.02 wt% Al as an impurity.

• 한국소음진동공학회:학술대회논문집
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• 한국소음진동공학회 2007년도 추계학술대회논문집
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• pp.1145-1148
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• 2007

Resilient materials are generally used for the floating floors to reduce the floor impact sound. Dynamic stiffness of resilient material, which has the most to do with the floor impact sound reduction. The resilient materials available in Korea include EPS (Styrofoam), recycled urethane types, EVA (Ethylene Vinylacetate) foam rubber, foam PE (Polyethylene), glass fiber & rock wool, recycled tire, foam polypropylene, compressed polyester, and other synthetic materials. In this study, we tested floor impact sound reduction characteristic to a lot of kinds of resilient material. The result of test showed that the amount of the heavy-weight impact sound reduction appeared by being influenced from this dynamic stiffness of resilient material. The dynamic stiffness looked like between other resilient materials, a similar to the amount of the heavy-weight impact sound reduction was shown.

• 한국자동차공학회논문집
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• 제10권5호
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• pp.138-146
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• 2002

The new type of vibration reduction material far an automotive interior, which is spray-type liquid material, is developed in this study The new material has better damping property and lower mass density than other damping materials, for example asphalt sheet. It can be sprayed by an automatic robot, so it is expected to improve productivity and cut down manpower. And it solves a poor adhesion problem and makes an automotive to be lightweight by optimizing spray process. So, It is a next generation automotive vibration reduction material. In this paper, the chemical process for making the new damping materials is described. And then, the damping properties of the vibration reduction materials are analyzed by modal testing of damping treatment specimens. The new vibration reduction materials have good damping properties than asphalt sheet in the experimental results.

• 한국분말재료학회지
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• 제13권3호
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• pp.205-210
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• 2006

The effect of Cu content on hydrogen reduction behavior of ball-milled $WO_3$-CuO nanocomposite powders was investigated. Hydrogen reduction behavior and reduction percent(${\alpha}$) of nanopowders were characterized by thermogravimetry (TG) and hygrometry measurements. Activation energy for hydrogen reduction of $WO_3$ nanopowders with different Cu content was calculated at each heating rate and reduction percent(${\alpha}$). The activation energy for reduction of $WO_3$ obtained in this study existed in the ranging from 129 to 139 kJ/mol, which was in accordance with the activation energy for $WO_3$ powder reduction of conventional micron-sized.

• 한국분말재료학회지
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• 제26권5호
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• pp.410-414
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• 2019

The hydrogen reduction behavior of the $CuO-SCo_3O_4$ powder mixture for the synthesis of the homogeneous Cu-15at%Co composite powder has been investigated. The composite powder is prepared by ball milling the oxide powders, followed by a hydrogen reduction process. The reduction behavior of the ball-milled powder mixture is analyzed by X-ray diffraction (XRD) and temperature-programmed reduction at different heating rates in an Ar-10%H2 atmosphere. The scanning electron microscopy and XRD results reveal that the hydrogen-reduced powder mixture is composed of fine agglomerates of nanosized Cu and Co particles. The hydrogen reduction kinetics is studied by determining the degree of peak shift as a function of the heating rate. The activation energies for the reduction of the oxide powders estimated from the slopes of the Kissinger plots are 58.1 kJ/mol and 65.8 kJ/mol, depending on the reduction reaction: CuO to Cu and $SCo_3O_4$ to Co, respectively. The measured temperature and activation energy for the reduction of $SCo_3O_4$ are explained on the basis of the effect of pre-reduced Cu particles.

• 열처리공학회지
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• 제18권4호
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• pp.242-246
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• 2005

Silver nanoparticles were synthesized by liquid phase reduction method from aqueous silver nitrate solution and borohybride as a reduction agent. The morphology, particle size and shape were influenced by the reaction conditions such as the concentration of $AgNO_3$, a reduction agent and addition of surfactant. The particle size decreased with decreasing the concentration of silver nitrate and using a borohydride. The obtained Ag particles showed the spherical shape with the range of 10-20 nm.

• 대한조선학회논문집
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• 제44권5호
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• pp.488-495
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• 2007

In this paper, SBN (Structure-Borne Noise) reduction of resiliently mounted machinery and effect of the foundation impedance on mount performance is studied. SBN reduction through the mount is analyzed by using two theoretical models; mass-spring model and wave model, in which longitudinal wave propagation is included. It is found that floor impedance greatly affects SBN reduction through lower mount, while it is almost negligible to SBN reduction through upper mount. Comparisons between measurement and predictions shows that the mass-spring model is valid only in low frequency range below few hundred Hz, while for high frequency ranges longitudinal wave propagation in the mount must be considered.

• 대한금속재료학회지
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• 제49권1호
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• pp.52-57
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• 2011

Nickel ferrite ($NiFe_2O_4$) powder was prepared through the ceramic route by calcination of a stoichiometric mixture of nickel oxide (NiO) and iron oxide ($Fe_2O_3$). The pressed pellets of $NiFe_2O_4$ were isothermally reduced in pure hydrogen at 800, 900, 1000 and $1100^{\circ}C$. Based on thermogravimetric analysis, the reduction behavior and the kinetic reaction mechanisms of the synthesized ferrite were studied. The initial ferrite powder and various reduction products were characterized by XRD, SEM, reflected light microscope and VSM to reveal the effect of hydrogen reduction on the composition, microstructure, magnetic properties and reaction kinetics of the produced Fe-Ni alloy. Complete reduction of the $NiFe_2O_4$ was achieved with synthesis of homogeneous nanocrystalline Fe-Ni alloys. Arrhenius equation with the approved mathematical formulations for a gas-solid reaction was applied for calculating the activation energy ($E_a$) values and detecting the controlling reaction mechanism.