• Title/Summary/Keyword: Injection buffer

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Analysis of Water-soluble Vitamins in Pharmaceutical Products by Capillary Electrophoresis (모세관 전기영동법을 이용한 제제중의 수용성 비타민 분석)

  • Lee, Jong-Jin;Moon, Dong-Cheul;Lee, Kong-Joo
    • YAKHAK HOEJI
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    • v.38 no.1
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    • pp.38-45
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    • 1994
  • An analytical method using capillary electrophoresis (CE) was developed for quantitation of water soluble vitamin contents in various vitamin products. The method includes the optimization of separation of 11 water soluble vitamins changing the micellar concentration and pH of running buffer, applied voltage and sample preparation. Best resolution was obtained with 25 mM phosphate buffer (pH=8.0) containing 50 mM sodium dodecyl sulphate (SDS) as micellar phase. At optimum condition, water soluble vitamins were determined in orange juice and vitamin products such as vitamin C pulvis, vitamin injection, coated multivitamin tablet. The quantitative analysis of water soluble vitamins with CE was suitable for quality control of pharmaceutical products with sound reproducibility.

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Study of Plasma Process Induced Damages on Metal Oxides as Buffer Layer for Inverted Top Emission Organic Light Emitting Diodes

  • Kim, Joo-Hyung;Lee, You-Jong;Jang, Jin-Nyoung;Song, Byoung-Chul;Hong, Mun-Pyo
    • 한국정보디스플레이학회:학술대회논문집
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    • 2008.10a
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    • pp.543-544
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    • 2008
  • In the fabrication of inverted top emission organic light emitting diodes (ITOLEDs), the organic layers are damaged by high-energy plasma sputtering process for transparent top anode. In this study, the plasma process induced damages on metal oxide hole injection layers (HILs) including $WO_3$, $MoO_3$, and $V_2O_5$ as buffer layer are examined. With the result of IV characteristic of hole-only devices, we propose that $MoO_3$ and $V_2O_5$ are stable materials against plasma sputtering process.

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INVESTIGATIONS OF CONDUCTION MECHANISM OF ORGANIC MOLECULES USED AS BUFFER HOLE INJECTING LAYER IN OLEDS

  • Shekar, B. Chandar;Rhee, Shi-Woo
    • 한국정보디스플레이학회:학술대회논문집
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    • 2003.07a
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    • pp.966-969
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    • 2003
  • Thin film capacitors with Al-Polymer-Al sandwich structure were fabricated. The bottom and top aluminium (Al) electrodes were deposited by vacuum evaporation and copper phthalocyanine (CuPc), polyaniline-emeraldine base (Pani-EB) and cobalt phthalocyanine/polyaniline - emeraldine base (CoPc /Pani-EB) blend films (which can be used as buffer hole injection layer in OLEDs) were deposited by spin coating technique. X-ray diffractograms indicated amorphous nature of the polymer films whose thicknesses were measured by capacitance and Rutherford Backscattering Spectrometry (RBS) methods. AC conduction studies revealed that the conduction mechanism responsible in these films is variable range hopping of polarons. From D.C conduction studies, it is observed that, the nature of conduction is ohmic in the lower fields and at higher fields the dominating D.C conduction is of Poole-Frenkel type.

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Voltage-Current-luminance Characteristics of Organic : Light-Emitting Diodes depending on Hole-Injection Buffer Layer (유기 발광 소자에서 정공 주입 버퍼층에 의한 전압-전류-휘도 특성)

  • Jeong Joon;Kim Tag-Yong;Ko Keel-Young;Lee Deok-Jin;Hong Jin-Woong
    • 한국컴퓨터산업교육학회:학술대회논문집
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    • 2003.11a
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    • pp.49-54
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    • 2003
  • In this work, we have seen the effect of hole-transporting layer in organic light-emitting diodes using N,N'-biphenyl-N,N'-bis-(3-methylphenyl)-[1,1'-biphenyl]-4,4'-diamine(TPD) and N,N'-biphenyl-N,N'-bis-(1-naphenyl)-[1,1'-biphenyl]-4,4'-diamine(NPB). NPB is regarded as a better hole trans porting material than TPD, since it has a higher glass transition temperature$(T_g)$. And current -voltage, luminance-voltage and external quantum efficiency of device were measured with the thickness variation of buffer layer using copper phathalocyanine(CuPc) and polytetrafluoroethylene (PTFE) at room temperature. We have obtained an improvement of External quantum efficiency when the CuPc 30[nm] and PTFE 1.0[nm] is used.

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Development of the Discrimination Methods for Geographical Origin of Bracken(Pteridium aquilinum) by Capillary Electrophoresis (Capillary electrophoresis를 이용한 한국산 및 중국산 고사리의 원산지 판별방법 개발)

  • Kim, Eun Young;Kim, Jung Hyun;Chung, Kyung Sook;Rhyu, Mee Ra
    • Analytical Science and Technology
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    • v.17 no.2
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    • pp.192-197
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    • 2004
  • The discrimination of bracken (Korean vs. Chinese) has been attempted using capillary electrophoresis (CE). Bracken (Pteridium aquilinum) was extracted with 30% methanol and separated on a uncoated fused-silica ($50{\mu}m{\times}27cm$) capillary. Conditions for optimal analysis include: temperature, $40^{\circ}C$; voltage, 8 kV; and pressure injection time, 5 sec. The optimal separation buffer was 0.3 M borate buffer (pH 8.5) containing 40 mM CHAPS with 30% ethylene glycol. Under the optimal conditions established for CE, the ratio of specific peak area (peak PA-1) to other peak area (peak PA-2) was effective in discrimination of Korean and Chinese bracken. The mean accuracy for discrimination of Korean and Chinese brackens were 80% and 86%, respectively.

Transient Analysis of PT-IGBT with Different Temperature (PT-IGBT의 온도에 따른 과도특성해석)

  • 이호길;류세환;이용국;안형근;한득영
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2000.07a
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    • pp.25-28
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    • 2000
  • In this study, Transient Characteristics of the Punch-Through Insulated Gate Bipolar Transistor (PT-IGBT) has been studied. On the contraty to Non-Punch Through Insulated Gate Bipolar Transistor(NPT-IGBT), PT-IGBT has buffer layer It has a simple drive circuit controlled by the gate voltage of the MOSFET and the low on-state resistance of the bipolar junction transistor. In this paper, the transient characteristics with temperature of the PT-IGBT has been analyzed analytically. PT-IGBT is made to reduce switching power loss. Excess Minority carrier distribution inactive base region and base charge, the rate of voltage with time is expressed analytically to include buffer layer.

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Determination of Pd(II) and Pt(II) Metal Cyano Complexes Using Capillary Electrophoresis

  • Lee, Hue-Jin;Lee, Sang-Ho;Chung, Koo-Soon;Lee, Kwang-Woo
    • Bulletin of the Korean Chemical Society
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    • v.15 no.11
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    • pp.945-949
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    • 1994
  • Mixtures of cyano complexes of palladium(II) and platinum(II) were separated by capillary electrophoresis using a fused silica capillary as a separation column and 30 mM phosphate buffer (pH 7) containing 15 wt. % acetonitrile as a running buffer. By virtue of the high ionic mobilities of the negatively charged cyano complexes of Pd(II) and Pt(II), they were separated using a cathodic injection and anodic detection scheme. The metal complexes eluted through the capillary were detected by direct UV absorption at 214 nm. A linear relationship between peak area and concentration was obtained for both ions and the detection limit was lower than $10^{-14}$ mole. The proposed method was applied to real sample, e.g., anode slime obtained from an electrolytic copper refinary, as a method for the simultaneous determination of palladium and platinum.

Analytical Delay-Time Modeling of BICMOS Buffere (BICMOS 버퍼의 해석적 지연시간 모델링)

  • 이희덕;조인성;한철희
    • Journal of the Korean Institute of Telematics and Electronics B
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    • v.30B no.1
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    • pp.38-44
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    • 1993
  • A model for BICMOS buffer switching operation is presented, including the influence of bipolar base transit time and collector-base capacitances. A closed-form solution for the propagation delay-time is obtained assuming low level injection and channel velocity limitation. For the high level injection case, the delay-times are numerically obtained using effective current gain. These results are compared with those by HSPICE simulation, which shows good agreement. It is noted that the collector-base capacitance strongly affects the delay-time. The effects of voltage scaling are also investigated, which shows the model can be applied for the reduced supply voltages.

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A Parallel Coupled QVCO and Differential Injection-Locked Frequency Divider in 0.13 μm CMOS

  • Park, Bong-Hyuk;Lee, Kwang-Chun
    • Journal of electromagnetic engineering and science
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    • v.10 no.1
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    • pp.35-38
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    • 2010
  • A fully integrated parallel-coupled 6-GHz quadrature voltage-controlled oscillator (QVCO) has been designed. The symmetrical parallel-coupled quadrature VCO is implemented using 0.13-${\mu}m$ CMOS process. The measured phase noise is -101.05 dBc/Hz at an offset frequency of 1 MHz. The tuning range of 710 MHz is achieved with a control voltage ranging from 0.3 to 1.4 V. The average output phase error is about $1.26^{\circ}$ including cables and connectors. The QVCO dissipates 10 mA including buffer from the 1.5 V supply voltage. The output characteristic of the differential injection-locked frequency divider (DILFD), which has similar topology to the QVCO, is presented.

Implementation of the COHO Unit for Phase-locking of Radar (레이다 위상동기를 위한 COHO Unit의 구현)

  • Cho, Tae-Bok;Shin, Hye-Jin;Lee, Taek-Kyung
    • Journal of Advanced Navigation Technology
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    • v.3 no.1
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    • pp.1-12
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    • 1999
  • For the phase measurement of radar signal in the coherent-on-receiver system, the COHO(Coherent Oscillator) generates the signal which locks to the phase of the transmit pulse. In this paper, COHO unit is developed to generate 60 MHz phase-locked signal. ILO(Injection Locking Oscilator) locks to the sample of the transmit pulse. Gate circuit, ILO, buffer amplifier, and pulse generator are designed and implemented.

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