• 제목/요약/키워드: DC sputtering

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Fabrication and Characterization of Ni-Cr Alloy Thin Films for Application to Precision Thin Film Resistors

  • Lee, Boong-Joo;Shin, Paik-Kyun
    • Journal of Electrical Engineering and Technology
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    • 제2권4호
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    • pp.525-531
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    • 2007
  • Ni(75 wt.%)-Cr(20 wt.%)-Al(3 wt.%)-Mn(4 wt.%)-Si(1 wt.%) alloy thin films were prepared using the DC magnetron sputtering process by varying the sputtering conditions such as power, pressure, substrate temperature, and post-deposition annealing temperature in order to fabricate a precision thin film resistor. For all the thin film resistors, sheet resistance, temperature coefficient of resistance (TCR), and crystallinity were analyzed and the effects of sputtering conditions on their properties were also investigated. The oxygen content and TCR of Ni-Cr-Al-Mn-Si resistors were decreased by increasing the sputtering pressure. Their sheet resistance, TCR, and crystallinity were enhanced by elevating the substrate temperature. In addition, the annealing of the resistor thin films in air at a temperature higher than $300^{\circ}C$ lead to a remarkable rise in their sheet resistance and TCR. This may be attributed to the improved formation of NiO layer on the surface of the resistor thin film at an elevated temperature.

고주파 마그네트론 스퍼터장치로 증착한 Ti 박막의 특성에 관한 연구 (A Study on the Characteristics of Ti Films Deposited by a DC Magnetron Sputtering Assisted with RF Voltage)

  • 배창환;이주희;한창석
    • 열처리공학회지
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    • 제22권3호
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    • pp.143-148
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    • 2009
  • We have fabricated Ti metal films on Cu wire substrates by using a RF magnetron sputtering method at different RF powers (0, 30 and 60 W) in a high vacuum, and we have investigated the thin film characteristics and resistivity. The ion bombardment effect is increased by the method to superimpose RF power to DC power applied to two poles of the base; thus, the thin film is deposited at sputtering gas pressures below 1 Pa. Moreover, the thin film formation of the multilayer structure becomes possible by gradually injecting the RF power, and the thin film quality is improved.

직류 마그네트론 스퍼터링 공정 중 타겟 오염에 따른 박막 및 계면 형성 특성 (Interlayer Formation During the Reactive DC Magnetron Sputtering Process)

  • 이진영;허민;이재옥;강우석
    • 반도체디스플레이기술학회지
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    • 제18권1호
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    • pp.1-4
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    • 2019
  • Reactive sputtering is widely used because of its high deposition rate and high step coverage. The deposition layer is often affected by target poisoning because the target conditions are changed, as well, by reactive gases during the initial stage of sputtering process. The reactive gas affects the deposition rate and process stability (target poisoning), and it also leads unintended oxide interlayer formation. Although the target poisoning mechanism has been well known, little attention has been paid on understanding the interlayer formation during the reactive sputtering. In this research, we studied the interlayer formation during the reactive sputtering. A DC magnetron sputtering process is carried out to deposit an aluminum oxide film on a silicon wafer. From the real-time process monitoring and material analysis, the target poisoning phenomena changes the reactive gas balance at the initial stage, and affects the interlayer formation during the reactive sputtering process.

반응성 DC 마그네트론 스퍼터링 법으로 증착한 ITO 박막의 전기적 특성 평가 (Electrical properties of ITO thin film deposited by Reactive DC magnetron sputtering)

  • 김민제;강세원;송풍근
    • 한국표면공학회:학술대회논문집
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    • 한국표면공학회 2014년도 추계학술대회 논문집
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    • pp.235-236
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    • 2014
  • 인듐 주석 산화물 박막을 In/Sn (2, 5 wt.%) 합금 타겟을 사용하여 DC 마그네트론 반응성 스퍼터링법을 이용하여 증착하였다. 기판온도는 상온에서 증착하였으며, 증착 중 DC 파워는 70W부터 120W 까지 10W 단위로 증가시켜 증착하였다. 증착 된 박막을 대기중에서 후 열처리를 각 6, 12 시간 진행하여 전기적 특성을 평가하였으며 평가 장비는 Hall-effect measurements system을 사용하였다. ITO (Indium Tin Oxide) 박막의 비저항은 합금의 Sn 조성별로 다르게 나타났다. Sn 5wt.% 타겟을 이용한 경우에는 DC 파워 90W를 기준으로 더 낮은 파워에서는 열처리에 따라 비저항이 증가하였고, 더 높은 파워에서는 열처리를 한 경우 비저항이 더 낮게 나타났다. 이러한 결과가 나온 이유는, DC 파워가 높은 경우 스퍼터링 공정 중 발생하는 고 에너지 입자 충돌에 의해 산소가 re-sputtering되어 산소가 부족한 박막이 형성되기 때문인 것으로 판단된다. Sn 2 wt.% 타겟의 경우에는 큰 차이를 나타내지 않았으며, 이러한 원인은 Sn 함량이 적기 때문에 산소 공급으로 인해 결정성이 향상되더라도 활성화 Sn의 양이 적기 때문에 나타나는 현상으로 판단된다.

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DC magnetron sputtering 방법으로 형성한 Indium-Tin-Oxide(ITO) 박막의 특성 연구 (A Study on the Properties of Indium-Tin-Oxide(ITO) Films Deposited by DC magnetron sputtering method)

  • 안명환
    • 한국정보통신학회논문지
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    • 제10권3호
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    • pp.473-478
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    • 2006
  • DC 마그네트론 스퍼터링 방법으로 ITO 박막을 형성하였다. 박막 형성 시 스퍼터 전압을 변화시켜 음이온에 의한 손상을 최소화하였으며, 또한 기판온도와 산소유입량을 변화시켜 비저항 $1.6\times10^{-4}{\Omega}cm$, 광투과도 90% 이상의 값을 갖는 양질의 박막을 형성 할 수 있었다. 박막 형성 시 $O_2$ 가스의 유량이 4sccm 이상으로 산소공급이 과다할 경우는 ITO 박막의 비저항이 증가하고, 광 투과도가 포화됨을 알 수 있었다.

반응성 RF 마그네트론 스퍼터링에 의한 TiNx 상온 성막에 있어서 기판 상의 펄스상 직류 바이어스 인가 효과 (Pulsed DC Bias Effects on Substrate in TiNx Thin Film Deposition by Reactive RF Magnetron Sputtering at Room Temperature)

  • 김세기
    • 한국표면공학회지
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    • 제52권6호
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    • pp.342-349
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    • 2019
  • Titanium nitride(TiN) thin films have been deposited on PEN(Polyethylene naphthalate) substrate by reactive RF(13.56 MHz) magnetron sputtering in a 25% N2/Ar mixed gas atmosphere. The pulsed DC bias voltage of -50V on substrates was applied with a frequency of 350 kHz, and duty ratio of 40%(1.1 ㎲). The effects of pulsed DC substrate bias voltage on the crystallinity, color, electrical properties of TiNx films have been investigated using XRD, SEM, XPS and measurement of the electrical properties such as electrical conductivity, carrier concentration, mobility. The deposition rates of TiNx films was decreased with application of the pulsed DC substrate bias voltage. The TiNx films deposited without and with pulsed bias of -50V to substrate exhibits gray and gold colors, respectively. XPS depth profiling revealed that the introduction of the substrate bias voltage resulted in decreasing oxygen concentration in TiNx films, and increasing the electrical conductivities, carrier concentration, and mobility to about 10 times, 5 times, and 2 times degree, respectively.

DC, RF 마그네트론 코스퍼터링법으로 증착한 ZTO/GZO 투명전도성막의 열처리 조건이 박막의 물성에 미치는 영향 (Effect of Annealing on the Electrical Property and Water Permeability of ZTO/GZO Double-layered TCO Films Deposited by DC, RF Magnetron Co-sputtering)

  • 오성훈;강세원;이건환;정우석;송풍근
    • 한국표면공학회지
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    • 제45권3호
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    • pp.117-122
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    • 2012
  • ZTO/GZO double layered films were prepared on unheated non-alkali glass substrates. ZTO films were deposited by RF/DC hybrid magnetron co-sputtering using ZnO (RF) target and $SnO_2$ (DC) targets, and then GZO films were deposited by DC magnetron sputtering using an GZO ($Ga_2O_3$:5.57 wt%) target. These films were post-annealed at temperature of 200, $300^{\circ}C$ in air and vacuum ambient for 30 min. In the case of post-annealing in air, ZTO/GZO double layer showed relatively low resistivity change, compared to GZO single layer. Furthermore, ZTO/GZO double layer revealed low WVTR, compared to GZO single layer. Therefore, it can be confirmed that ZTO film doing a role with barrier for water or oxygen diffusion.

DC 마그네트론 스퍼터링 방법에 의해 증착된 Mo 박막의 특성 (Characteristics of Mo Thin Films Deposited by DC Magnetron Sputtering)

  • 공선미;소우빈;김은호;정지원
    • Korean Chemical Engineering Research
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    • 제49권2호
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    • pp.195-199
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    • 2011
  • DC 마그네트론 스퍼터링 방법을 이용하여 soda lime glass 위에 Mo 박막을 증착하였다. DC power와 증착 압력을 변화시키면서 상온에서 Mo 박막을 증착하였고 증착된 박막의 전기적 성질 및 구조적 성질을 조사하였다. DC power가 증가할수록 박막의 증착속도는 증가되었고 전기 저항도는 감소하였으며 박막의 결정성이 향상되는 것을 관찰할 수 있었다. 증착 압력이 감소할수록 박막의 증착속도와 전기 저항도가 감소하였으며 가늘고 긴 모양의 결정입자가 조밀하게 박막을 형성하였다. 압력이 증가함에 따라서 결정입자는 원형으로 변형되었으며 박막의 표면에 공극의 생성이 증가하였다. Mo 박막의 전기 저항도는 Mo 원자에 결합된 산소의 양이 많아질수록 증가하게 되고, 박막의 결정성이 높아지면 산소의 결합도가 감소하여 낮은 저항도를 갖게 되는 것을 확인하였다.

비대칭 마그네트론 스퍼터링법으로 성장된 a-C:H의 물리적 특성 (Characteristics of Hydrogenated Amorphous Carbon (a-C:H) Thin Films Grown by Close Field UnBalanced Magnetron Sputtering Method)

  • 박용섭;홍병유
    • 한국전기전자재료학회논문지
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    • 제17권3호
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    • pp.278-282
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    • 2004
  • The Hydrogenated amorphous carbon(a-C:H) thin films are deposited on silicon with a close field unbalanced magnetron(CFUBM) sputtering systems. The experimental data are obtained on the depositon rate and physical properties of a-C:H films using DC bias voltage and Ar/C$_2$H$_2$ pressure. The depostion rate and the surface roughness decrease with DC bias voltage, but the hardness of the thin films increases with DC bias voltage. And the position of G-peak moves to lower wavenumber indicating an increase in diamond-like carbon characteristics with the lower Ar/C$_2$H$_2$ pressure.

DC Magnetron Sputtering에 의해 증착된 알루미늄 박막의 특성 (The Characteristics of Aluminum Thin Films using DC Magnetron Sputtering)

  • 표재확;연충규;황기웅
    • 대한전기학회:학술대회논문집
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    • 대한전기학회 1993년도 정기총회 및 추계학술대회 논문집 학회본부
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    • pp.258-260
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    • 1993
  • Aluminum thin films were deposited on glass substrate using DC Magnetron Sputtering. Deposition rate, specular reflectance, and resistivity were investigated as a function of the input power, pressure, substrate temperature, and deposition time. Reflectance was reduced with increasing power, also with prolonging deposition time. Topography of the surface, which influences the properties such as electromigration, was observed from scanning electron microscope (SEM) and there was a close relation between the topography and measured reflectance.

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