• Title/Summary/Keyword: 재료물성시험

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Mechanical Properties of Carbon Fiber/Si/SiC and Carbon Fiber/C/SiC Composites (탄소섬유/Si/SiC 및 탄소섬유/탄소/SiC 복합재의 기계적 물성)

  • 신동우;박삼식;김경도;오세민
    • Composites Research
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    • v.12 no.3
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    • pp.8-16
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    • 1999
  • Carbon woven fabric/C/SiC composites were fabricated by multiple impregnations of carbon woven fabric/carbon preform with the polymer precursor of SiC, i.e., polycarbosilane. In addition, two kinds of low density carbon/carbon preforms which had different fiber volume fraction and fiber orientation, i.e., a carbon woven fabric(${\thickapprox}$55 vol%)/carbon and a chopped carbon fiber${\thickapprox}$40 vol%)/carbon composites, were reaction-bonded with a silicon melt at 1$700^{\circ}C$ in a vacuum to fabricate dense carbon fiber/Si/SiC composites. The reaction-bonding process increased the density to ~2.1 g/$cm^3$ from 1.6 g/$cm^3$ and 1.15 g/$cm^3$ of a carbon woven and a chopped carbon preforms, respectively. All of the composites fractured with extensive fiber pull-out. The higher the density the higher the stiffness and proportional limit stress. The mechanical properties obtained from a three-point bend and tension tests were compared. The ratios of the peak tensile stresses to the bending strengths of a carbon woven and a chopped carbon composites were about one-third, respectively. The carbon woven fabric/Si/SiC composites with density of 2.06 g/$cm^3$ showed ~120 MPa of ultimate strength and ~80 MPa of proportional limit in bend testing.

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A study of feasibility of using compressed wood for LNG cargo containment system (압축목재를 사용한 LNG 화물창 단열시스템의 적합성 평가에 관한 연구)

  • Kim, Jong-Hwan;Ryu, Dong-Man;Park, Seong-Bo;Noh, Byeong-Jae;Lee, Jae-Myung
    • Journal of Advanced Marine Engineering and Technology
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    • v.40 no.4
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    • pp.307-313
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    • 2016
  • When liquefied natural gas (LNG) is stored in a tank, it is necessary to maintain low temperature. It is very important that insulation techniques are applied to the LNG cargo because of this extreme environment. Hence, laminated wood, especially plywood, is widely used as the structural member and insulation material in LNG cargo containment systems (CCS). However, fracture of plywood has been reported recently, owing to sloshing effect. Therefore, it is necessary to increase the strength of the structural member for solving the problem. In this study, compressed wood, which is used as a support in LNG independent type B tanks, was considered as a substitute for plywood. Compression and bending tests were performed on compressed wood under ambient and cryogenic temperatures to estimate the mechanical behaviors and fracture characteristics. In addition, the direction normal to the laminates surface was considered as an experimental variable. Finally, the feasibility of using compressed wood for an LNG CCS was evaluated from the test results.

Experimental Study on the Fire Performance of PC Slab by the Bearing Length (걸침길이에 따른 PC 슬래브의 화재성능에 관한 실험적 연구)

  • Park, Siyoung;Kang, Thomas H.K.;Lee, Ho-Wook;Gwak, Si-Young;Park, Jun-Kyu
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.26 no.6
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    • pp.14-22
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    • 2022
  • In this study, a fire test was conducted to evaluate the fire performance of precast concrete (PC) slabs in an outdoor environment in response to the increase in fire incidents caused by the growth of warehouses. Prior to the field fire test, the tensile yield strength of the tendon at elevated temperatures was tested to analyze the mechanical properties. Also, by referring to previous studies, the thermal properties of tendon and the mechanical and thermal properties of concrete were investigated. A field fire test was conducted to analyze the structural and fire performance of two identical slabs with 50 and 150 mm bearing length. As the bearing length increased, deflection and horizontal displacement decreased. The fire test lasted for 200 minutes without the collapse of slabs, validating current codes. Based on the structural performance which maintained even with concrete spalling and rupture of some tendons, the bonded method is assumed to be practical in pre-tensioned PC slabs. The results of fire test are expected to be utilized in evaluating the fire performance of PC slabs in warehouses.

Comparison of the Mechanical Properties between Bulk-fill and Conventional Composites (Bulk-fill 복합레진과 전통적 복합레진의 물성비교)

  • Noh, Taehwan;Song, Eunju;Park, Soyoung;Pyo, Aeri;Kwon, Yonghoon;Kim, Jiyeon;Kim, Shin;Jeong, Taesung
    • Journal of the korean academy of Pediatric Dentistry
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    • v.43 no.4
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    • pp.365-373
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    • 2016
  • Composites are the most useful restorative material. However, composites have some disadvantages such as polymerization shrinkage, long working time, and susceptibility to water and contamination, which are stood out more especially when treating children. To solve these problems, bulk-fill composites have been developed. The aim of this study is to compare mechanical properties of bulk-fill and conventional composites. Bulk-fill composites (SureFil SDR flow (SDR), Tetric N-Ceram bulk fill (TBF)) and conventional composites (Filtek Z-350 (Z-350), Unifil Flow (UF), Unifil Loflo Plus (UL)) were used. The Vickers hardness tester was used to measure the microhardness of materials, and Fourier transform infrared spectroscopy was used to measure the degree of conversion. Polymerization shrinkage was measured by using a linometer. Flexural and compressive properties were measured by using the universal testing machine. Data were statistically analyzed by ANOVA and Scheffe's post hoc test. The level of significance was set to p < 0.05. Most conventional composites showed higher microhardness than bulk-fill composites. However, bulk-fill composites showed a higher top/bottom microhardness ratio than conventional composites. Bulk-fill composites showed a higher top/bottom degree of conversion ratio than conventional composites. The polymerization shrinkage was highest in UL and lowest in Z-350. The polymerization shrinkage of flowable composites was higher than that of non flowable composites. The compressive properties were highest in Z-350 and lowest in SDR and UL. In terms of flexural properties, Z-350 was the highest. However, none of the bulk-fill composites exhibited mechanical properties as good as those of conventional composites. Nonetheless, the ratio of microhardness and degree of conversion, which are important properties of bulk filling, were higher in bulk-fill composites. Therefore, the bulk-fill composites might be considered suitable restorative materials in pediatric dentistry.

Comparison of the mechanical properties and microstructures of fractured surface for Co-Cr alloy fabricated by conventional cast, 3-D printing laser-sintered and CAD/CAM milled techniques (주조, 3-D printing을 활용한 laser sintered 및 CAD/CAM milled 기법을 이용하여 제작된 코발트-크롬 합금의 물리적 성질 및 파절 단면 관찰 비교 연구)

  • Choi, Yun-Jung;Koak, Jai-Young;Heo, Seong-Joo;Kim, Seong-Kyun;Ahn, Jin-Soo;Park, Dong-Soo
    • The Journal of Korean Academy of Prosthodontics
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    • v.52 no.2
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    • pp.67-73
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    • 2014
  • Purpose: The purpose of present study is to compare mechanical properties and microstructural characteristics of fractured surface for cast, 3-D printing laser sintered and CAD/CAM milled cobalt-chromium (Co-Cr) alloy specimens and to investigate whether laser sintered technique is adequate for dental applications. Materials and methods: Thirty six flat disc shape Co-Cr alloy specimens were fabricated for surface hardness test and divided into three groups according to the manufacturing methods; 12 specimens for casting (n=12), 12 specimens for laser sintered technology (n=12) and 12 specimens for milled technology (n=12). Twelve dumbbell shape specimens for each group were also fabricated for a tensile test. Statistical comparisons of the mechanical properties for the alloys were performed by Kruskal-Wallis test followed by Mann-Whitney and Bonferroni test. The microstructural characteristics of fractured surfaces were examined using SEM. Results: There were significant differences in the mean Vickers hardness values between all groups and the cast specimen showed the highest (455.88 Hv) while the CAD/CAM milled specimen showed the lowest (243.40 Hv). Significant differences were found among the three groups for ultimate tensile strength, 0.2% yield stress, elongation, and elastic modulus. The highest ultimate tensile strength value (1442.94 MPa) was shown in the milled group and the highest 0.2% yield strength (1136.15 MPa) was shown in the laser sintered group. Conclusion: Different manufacturing methods influence the mechanical properties and microstructure of the fractured surfaces in Co-Cr alloys. The cast Co-Cr alloy specimens showed the highest Vickers hardness, and the CAD/CAM milled specimens revealed the highest tensile strength value. All alloys represent adequate mechanical properties satisfying the ISO standards of dental alloy.

Warpage of Flexible OLED under High Temperature Reliability Test (고온 신뢰성 시험에서 발생된 플렉서블 OLED의 휨 변형)

  • Lee, Mi-Kyoung;Suh, Il-Woong;Jung, Hoon-Sun;Lee, Jung-Hoon;Choa, Sung-Hoon
    • Journal of the Microelectronics and Packaging Society
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    • v.23 no.1
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    • pp.17-22
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    • 2016
  • Flexible organic light-emitting diode (OLED) devices consist of multi-stacked thin films or layers comprising organic and inorganic materials. Due to thermal coefficient mismatch of the multi-layer films, warpage of the flexible OLED is generated during high temperature process of each layer. This warpage will create the critical issues for next production process, consequently lowering the production yield and reliability of the flexible OLED. In this study, we investigate the warpage behavior of the flexible OLED for each bonding process step of the multi-layer films using the experimental and numerical analysis. It is found that the polarizer film and barrier film show significant impact on warpage of flexible OLED, while the impact of the OCA film on warpage is negligible. The material that has the most dominant impact on the warpage is a plastic cover. In order to minimize the warpage of the flexible OLED, we estimate the optimal material properties of the plastic cover using design of experiment. It is found that the warpage of the flexible OLED is reduced to less than 1 mm using a cover plastic of optimized properties which are the elastic modulus of 4.2 GPa and thermal expansion coefficient of $20ppm/^{\circ}C$.

Computational Modal Analyses for the Propellant Tank and Small-Scaled First-Stage Models of Liquid-Propulsion Launch Vehicles (우주 발사체 추진제 탱크 및 축소 1단 모델의 전산 모드 해석 연구)

  • Sim, Chang-Hoon;Kim, Geun-Sang;Kim, Dong-Goen;Kim, In-Gul;Park, Soon-Hong;Park, Jae-Sang
    • Journal of Aerospace System Engineering
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    • v.12 no.3
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    • pp.18-25
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    • 2018
  • This research aims to establish the finite-element modeling techniques for computational modal analyses of liquid propellants and flange joints of launch-vehicle structures. MSC.NASTRAN is used for the present computational modal analyses of the liquid-propellant tank and the small-scaled first-stage model. By means of the correlation between the measured and computed natural frequencies, the finite modeling techniques for liquid propellants and flange joints of launch-vehicle structures are established appropriately. This modal analysis using the virtual-mass method predicts well the bell mode of the liquid-propellant tank containing liquid. In addition, the present computation using RBE2 elements for modeling of flange joints predicts the first and second bending-mode frequencies within a relative error of 10%, which is better than the measured frequencies obtained from the modal test, for the small-scaled first-stage model containing liquid.

Autogenous Shrinkage Mock-up Test of High Performance Concrete by Emulsified Refined Cooking Oil (유화처리 정제식용유를 사용한 고성능 콘크리트의 자기수축 Mock-up 실험)

  • Jo, Man-Ki;Han, Cheon-Goo
    • Journal of the Korean Recycled Construction Resources Institute
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    • v.4 no.3
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    • pp.307-315
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    • 2016
  • The aim of this research is analyzing the fundamental properties and autogenous shrinkage reducing performance of 70 and 100MPa grade high performance concrete including emusified refined cooking oil(ERCO) under the mock-up conditions. As a results of experiment, the mixture contained 0.5% of ERCO showed slightly decreased slump flow while the slump was increased and segregation resistance performance was improved as 2.5 of EIS. For air content, all mixtures satisfied target air content with increased unit weight and delayed setting time with ERCO addition. In the case of compressive strength, when ERCO was added 0.5%, the result of approximately 5 to 10% of increased compressive strength was observed. For the autogenous shrinkage, ERCO contributed on 20-30% of shrinkage reducing performance comparing to Plain mixture without ERCO. It is considered that capillary pore filling action of soap particles occurred by the reaction of ERCO in cement paste between fatty aicd and calcium hydroxide contributed the shrinkage reducing performance. Based on these mock-up test results, application of the high performance concrete mixture with ERCO on CFT actual structure was decided.

Effect of Adhesive Shear Strength of CFRP/Ni-Cr Alloy Under Severe Environmental Condition (가혹 환경이 복합재/Ni-Cr 합금 접착전단강도에 미치는 영향 연구)

  • Cho, Hyeon-Tae;Park, Seong-Min;Kim, Min-Jun;Hoang, Van-Tho;Kim, Hak-Inn;Son, Myung-Sook;Ahn, Jong-Kee;An, Ji-Min;Choi, Jin-Ho;Nam, Young-Woo;Kweon, Jin-Hwe
    • Composites Research
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    • v.33 no.5
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    • pp.275-281
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    • 2020
  • The mechanical property related to lap shear strength of the joint structure between carbon fiber reinforced polymer (CFRP) composite and metal (Ni-Cr Alloy) under varying environmental conditions (temperature and humidity) was studied in order to apply to the aircraft fan blade. Room temperature dry (RTD), elevated temperature wet (ETW), and cold temperature dry (CTD) environmental conditions were chosen for investigation based on the flight conditions of aircraft. Lap shear strength tests were conducted according to ASTM Standard D3528 to evaluate the shear strength. The microstructure characteristic of failure zone was analyzed by SEM images to check the adhesive shear strength with the three environmental conditions. In comparison with shear strength for the RTD condition, the shear strength in the ETW condition was reduced by 72.8% while those for the CTD condition increased by 56.5%. The moisture absorption and high temperature in ETW condition strongly had an affect on mechanical property of adhesive, while cold temperature could enhance the adhesive shear strength due to the higher brittleness.

Analysis on Foaming Properties of the PANI added MWNT/PU Films (PANI 첨가 MWNT/PU 필름의 발포특성)

  • Ma, Hye-Young;Choi, La-Hee;Park, Mi-Ra;Kim, Seung-Jin
    • Proceedings of the Korean Society of Dyers and Finishers Conference
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    • 2012.03a
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    • pp.63-63
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    • 2012
  • 전자제품 패키지에 요구되는 쿠션성과 정전방전 기능을 갖는 폴리우레탄 발포 필름의 제조기술을 확립하게 되면 IT산업용에 적용 가능한 필름제품이 개발되어 ESD(정전방전, Electrostatic Dissipation) 성능을 발휘하게 됨으로서 정전기 쇼크에 의한 각종 전자제품의 오작동이나 파손 방지가 가능하게 되어 포장재, 자동차 전자제품의 하우징 등으로 사용될 수 있게 된다. 전도성 고분자인 Polyaniline (PANI)은 다른 여러 고분자와 비교하여 볼 때 다른 유형의 전도성 고분자보다 합성하기가 쉽고 높은 전기전도도를 보임은 물론 열적 및 대기 안정성이 우수하며 가격이 저렴한 장점을 가지고 있다. 본연구는 CNT 나노기술을 응용한 IT산업용 적층간지용 ESD PU발포필름의 제조 가공기술 및 상품화 개발을 수행하고자 방수, 투습방수성을 가지는 유연재료인 폴리우레탄(PU)의 1액형 PU와 DMF에 PANI의 함량을 5, 10, 15, 20, 25, 30wt%로 변화시켜 제조한 PANI/DMF 분산용액과 IPA/MWNT 3wt% 분산용액의 혼용비에 변화를 주어 $120^{\circ}C$에서 2분 건조시켜 그라운드 필름을 제조하였다. 그리고 2액형 PU와 IPA/MWNT 3wt% 분산용액과 발포제를 사용하여 발포온도 $150^{\circ}C$에서 5분간 건조시켜 발포필름을 제조하였으며 이들의 전기적 특성과 역학적 특성을 조사하였다. 제조된 필름의 전기전도성은 전기저항측정기 KEITHLEY 8009를 사용하여 부피저항과, 표면저항을 각각 측정하여 확인하였으며, 필름의 마찰 대전압은 E.S.T-7 마찰 대전압 시험기를 이용하여 표면 마찰 대전압을 측정하여 확인하고, 필름의 물리적 특성은 인장시험기를 이용하여 breaking stress, breaking strain을 측정하였다. 필름단면의 CNT 발포특성은 주사전자현미경(SEM)을 사용하여 측정하여 발포특성과 물성과의 연관성을 확인하였다. 그 결과 필름의 전기적 특성은 PANI가 30% 함량일 때 전반적으로 낮은 저항값이 측정되었으며, 마찰대전압을 측정한 결과 대부분의 시료가 0에 가까운 낮은 값을 가졌다. 필름의 물리적 인장특성은 PANI가 10wt%의 함량일 때 가장 높은 절단강도를 가졌으며 분산용액의 혼용비에 따른 경향성은 나타나지 않았다. 필름의 단면형상을 확인하여 발포특성을 분석한 결과 PANI의 함량에 따라 발포 cell의 크기는 뚜렷한 경향성을 보이지 않았으나 30wt%의 PANI/DMF 분산용액 20part(gr)와 3wt% IPA/MWNT 분산용액 40part(gr)로 제조한 시료의 cell이 가장 균일하고 고르게 발포되었으며, 3.90E+06ohm으로 가장 낮은 표면저항 값으로 측정되어 가장 좋은 전기전도성을 가짐을 확인하였다.

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