• Applied Science and Convergence Technology
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• v.26 no.5
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• pp.133-138
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• 2017

We investigated the interface defect engineering and reaction mechanism of reduced transition layer and nitride layer in the active plasma process on 4H-SiC by the plasma reaction with the rapid processing time at the room temperature. Through the combination of experiment and theoretical studies, we clearly observed that advanced active plasma process on 4H-SiC of oxidation and nitridation have improved electrical properties by the stable bond structure and decrease of the interfacial defects. In the plasma oxidation system, we showed that plasma oxide on SiC has enhanced electrical characteristics than the thermally oxidation and suppressed generation of the interface trap density. The decrease of the defect states in transition layer and stress induced leakage current (SILC) clearly showed that plasma process enhances quality of $SiO_2$ by the reduction of transition layer due to the controlled interstitial C atoms. And in another processes, the Plasma Nitridation (PN) system, we investigated the modification in bond structure in the nitride SiC surface by the rapid PN process. We observed that converted N reacted through spontaneous incorporation the SiC sub-surface, resulting in N atoms converted to C-site by the low bond energy. In particular, electrical properties exhibited that the generated trap states was suppressed with the nitrided layer. The results of active plasma oxidation and nitridation system suggest plasma processes on SiC of rapid and low temperature process, compare with the traditional gas annealing process with high temperature and long process time.

• Transactions of Materials Processing
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• v.15 no.3 s.84
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• pp.232-240
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• 2006

Magnesium alloys are expected to be widely used fur the parts of structural and electronic appliances due to their lightweight and EMI shielding characteristics. While the die casting has been mainly used to manufacture the parts from the magnesium alloys, the press forming is considered as an alternative to the die casting for saving the manufacturing cost and improving the structural strength of the magnesium alloy parts. However, the magnesium alloy has low formability at room temperature and therefore, in many cases, forming at elevated temperatures is necessary to obtain the required material flow without failure. In the present study, square cup deep drawing tests using the magnesium alloy AZ31 sheet were experimentally conducted at various elevated temperatures as well as room temperature, and the corresponding finite-element simulations, which calculated the damage evolution based on the Oyane's criterion, were conducted using the stress-strain relations from the tensile tests at various temperatures. The formability predictability by the finite-element analysis was investigated by comparing the predicted damage distributions over the deformed AZ31 sheet at elevated temperatures with the corresponding experimental deformations with failures.

• Journal of the Korean Society of Visualization
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• v.17 no.3
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• pp.12-18
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• 2019

Direct numerical simulation of a fully developed turbulent plane Couette-Poiseuille flow with a two-dimensional (2-D) rod-roughened wall is performed to investigate the impacts of the surface roughness. It is shown that the logarithmic region in the mean velocity profile over the rough wall Couette-Poiseuille flow is significantly shortened by the surface roughness compared to that over a turbulent Couette-Poiseuille flow with smooth wall. The Reynolds shear stress over the rough wall Couette-Poiseuille flow is decreased compared to that for a smooth case in the outer layer. These results are attributed to weakened turbulence activity or roll-cell mode over the rough wall Couette-Poiseuille flow near the channel centerline due to suppressed development of u'-structure on the top wall, as documented through spanwise energy spectra of the streamwise velocity fluctuations. Inspection of congregation motion near the bottom wall and time evolution of u'-structure reveal weakened co-supporting cycle for the rough wall case.

• The Korean Journal of Rheology
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• v.9 no.1
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• pp.6-15
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• 1997

계면활성제용액에 서로 다른 기능을 하는 두 종류의 첨가제를 투입하여 미셀의 미 세구조 전이현상을 규명하였다. 양이온 계면활성제는 CMC 이상의 농도에서 2단계의 미세 구조 전이거동을 나타낸다. 우선 구형 미셀은 첨가제의 투입에 의하여 표면에서의 친수성기 간의 반발력이 감소됨으로써 실린더형 또는 디스크형미셀로 전이가 일어난다. 더욱 농도가 증가하면 이방성을 가지는 실린더형 미셀간의 중첩 또는 hooking 현상에 의한 두 번째 전 이가 일어난다. 이때 미셀 용액은 흔히 점탄성을 나타내거나 확연한 비뉴톤성 유체거동을 나타낸다. 본 연구에선 heptanol의 화확구조적 차이가 물성에 나타내는효과를 규명하고 wormlike 미셀을 형성하는 MaSal에 의한 점탄성 거동을 살펴보았다. Heptanol의 화학구조 의 영향을 보면 약친수성기인 OH기가 알킬그룹과 나란하게 존재하여 밀집된 구조를 가지 기 쉬운 primary heptanol이 가장효과적으로 미세구조 전이를 유도함을 관찰하였다. 다른 이성질 hetanol의 경우 secondary heptanol이 teriary heptanol에 비하여 효과적임을 보이지 만 화학재할수 있는 농도범위가 매우 좁아 대부분 영역에서 비뉴톤성거동을 나타냄을 확인 하였다. 즉 NaSal를 사용한 경우 실린더형 미셀이 존재할 수 있는농도범위가 매우 좁아 대 부분 영역에서 비뉴톤성 거동을 나타냄을 확인하였다. 즉 NaSal 이 첨가된 용액은 선형점탄 성거동을 보이며 몰비가 증가함에 따라 scission 과정이 관찰되었다. 또한 몰농도비에 따라 항복응력과 shear thickening 특징을 보이는데 이는 흐름장의 세기에 따라 미세구조 변화가 일어나기 때문이다.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2005.10a
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• pp.122-125
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• 2005

Magnesium alloys are expected to be widely used for the parts of structural and electronic applications due to their lightweight and EMI shielding characteristics. While the die casting has been mainly used to manufacture the parts from the magnesium alloys, the press forming is considered as an alternative to the die casting for saving the manufacturing cost and improving the structural strength of the magnesium alloy parts. However, the magnesium alloy has low formability at room temperature and therefore, in many cases, forming at elevated temperatures is necessary to obtain the required material flow without failure. In the present study, square cup deep drawing tests using the magnesium alloy AZ31 sheet were experimentally conducted at various elevated temperatures as well as room temperature, and the corresponding finite-element simulations, which calculated the damage evolution based on the Oyane's criterion, were conducted using the stress-strain relations from the tensile tests at various temperatures. The formability predictability by the finite-element analysis was investigated by comparing the predicted damage distributions over the deformed AZ31 sheet at elevated temperatures with the corresponding experimental deformations with failures.

• Korean Journal of Materials Research
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• v.9 no.9
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• pp.900-904
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• 1999

The effects of Tio$_2$addition on the microstructural evolution and mechanical properties of alumina ceramics were studied. Bulk density decreased with an increase of the amount of TiO$_2$. Apparent porosity decreased with an increase of the amount of TiO$_2$ up to 7wt%. But beyond 9wt% of TiO$_2$powders, apparent porosity increased. In the compression test, the modulus increased with an increase of the amount of TiO$_2$addition. In the three point bending test, the stress at yield decreased with an increase of the amount of TiO$_2$ addition. The addition. The addition of TiO$_2$ promoted the grain growth of alumina ceramics.

• Journal of Powder Materials
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• v.13 no.2 s.55
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• pp.124-128
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• 2006

In recent years, equal channel angular pressing (ECAP) has been the subject of intensive study due to its capability of producing fully dense samples having a ultrafine grain size. In this paper, the ECAP process was applied to metallic powders in order to achieve both powder consolidation and grain refinement. In the ECAP process for solid and powder metals, knowledge of the internal stress, strain and strain rate distribution is fundamental to the determination of the optimum process conditions for a given material. The properties of the ECAP processed solid and powder materials are strongly dependent on the shear plastic deformation behavior during ECAP, which is controlled mainly by die geometry, material properties, and process conditions. In this study, we investigated the consolidation, plastic deformation and microstructure evolution behaviour of the powder compact during ECAP.

• Fibers and Polymers
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• v.6 no.2
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• pp.131-138
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• 2005

A theoretical model is proposed in order to investigate rheological behavior of bubble suspension with large deformation. Theoretical constitutive equations for dilute bubble suspensions are derived by applying a deformation theory of ellipsoidal droplet [1] to a phenomenological suspension theory [2]. The rate of deformation tensor within the bubble and the time evolution of interface tensor are predicted by applying the proposed constitutive equations, which have two free fitting parameters. The transient and steady rheological properties of dilute bubble suspensions are studied for several capillary numbers (Ca) under simple shear flow and uniaxial elongational flow fields. The retraction force of the bubble caused by the interfacial tension increases as bubbles undergo deformation. The transient and steady relative viscosity decreases as Ca increases. The normal stress difference (NSD) under the simple shear has the largest value when Ca is around 1 and the ratio Of the first NSD to the second NSD has the value of 3/4 for large Ca but 2 for small Ca. In the uniaxial elongational flow, the elongational viscosity is three times as large as the shear viscosity like the Newtonian fluid.

• Journal of the Korean Institute of Electrical and Electronic Material Engineers
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• v.15 no.2
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• pp.119-126
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• 2002

The mica/epoxy composite used in generator(rated 22 kV and 500 MW) stator windings was aged at 180$\^{C}$ for up to 1000 hours in air and hydrogen. The degradation mechanism was investigated through the defect of evolution and microstructural analysis by performing SEM(Scanning Electron Microscope). As the thermal aging time increases, the number of voids per unit volume increases at the mica/epoxy interface of generator stator windings. The aged specimens in hydrogen showed retarded generation and growth of voids. Accelerated aging tests were conducted using the combination of thermal and electrical aging in air and hydrogen. The aging was carried out at a combined stress such as thermal aging at 110$\^{C}$, electrical aging at 5.5 kV/mm and frequencies 420 Hz in air, and electrical aging at 5.5 kV/mm and frequencies 420 Hz in hydrogen (pressure 4 kg/㎠). Thermal and electrical aging generates large voids at the mica/epoxy interface in air. Electrical aging in hydrogen also generates small voids, delaminations and cracks in mica tapes.

• Corrosion Science and Technology
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• v.2 no.3
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• pp.155-160
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• 2003

Plasma spraying technique was used to fabricate functionally graded coating (FGC) of NiCrAIY/YSZ 8wt%$Y_2O_3-ZrO_2$ on a Co-base superalloy (HAYNES 188) substrate. Six layers were coated on the substrate for building up compositionally graded architecture. Conventional thermal barrier coating (TBC) of NiCrAIY/SZ with sharp interface was also fabricated. As-coated FGC and TBC samples were exposed at the temperature of $1100^{\circ}C$ for 10, 50, 100 hours in air. Microstructural change of thermally exposed samples was examined. Pores and microcracks were formed in YSZ layer due to evolution of thermal internal stress at high temperature. The amount of pores and microcracks in YSZ layer were increased with increasing exposure time at high temperature. High temperature oxidation of coatings occurred mainly at the NiCrAIY/YSZ interface. In comparison with the case of TBC. the increased area of the NiCrAIY/YSZ interface in FGC is likely to attribute to forming the higher amount of oxides.