• Journal of Magnetics
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• 제16권2호
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• pp.173-176
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• 2011

Fe-Cr alloys with different Cr contents were prepared by an arc melting technique. The alloys were isochronally aged in the range from $400^{\circ}C$ to $900^{\circ}C$ with $50^{\circ}C$ steps with a holding time of 100 hours. The ageing produced embrittlement in the alloys due to either the formation of a Cr-rich ${\alpha}'$ phase or a $\sigma$ phase at high temperatures. Magnetic Hysteresis Loop (MHL) and Micro-Vickers hardness were measured at each step to correlate the magnetic and mechanical properties. Coercivity and hardness of the alloys were increased and remanence decreased up to 500-$550^{\circ}C$ due to formation of a Cr-rich ${\alpha}'$ phase. Beyond 500-$550^{\circ}C$ range, the coercivity and hardness decreased and remanence increased due to the coarsening or dissolution of the Cr-rich ${\alpha}'$ phase. In the Fe-48% Cr alloy, formation of the $\sigma$ phase at $700^{\circ}C$ reduced the maximum induction of the alloy significantly.

• 한국해양공학회지
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• 제28권4호
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• pp.306-313
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• 2014

Super duplex stainless steels (sDSS) are excellent for use under severely corrosive conditions such as offshore and marine applications like pipelines and flanges. sDSS has better mechanical properties and corrosion resistance than the standard duplex stainless steel (DSS) but it is easier for a sigma phase to appear, which depresses the mechanical property and corrosion resistance, compared to DSS, because sDSS has a higher alloy element than DSS. In addition, sDSS has a feeble ductile-brittle transition temperature (DBTT) because it has a 50% ferrite microstructure. In the actual operating environment, sDSS would be thermally affected by welding and a sub-zero temperature environment. This study analyzed how precipitated sDSS behaves at a sub-zero temperature through annealing heat treatment and a sub-zero tensile test. Six types of specimens with annealing times of up to 60 min were tested in a sub-zero chamber. According to the experimental results, an increase in the annealing time reduced the elongation of sDSS, and a decrease in the tensile test temperature raises the flow stress and tensile stress. In particular, the elongation of specimens annealed for 15 min and 30 min was clearly lowered with a decrease in the tensile test temperature because of the increasing sigma phase fraction ratio.

• 대한전자공학회논문지SD
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• 제47권8호
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• pp.64-72
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• 2010

본 논문은 UWB주파수 합성기용 광대역 전압 제어 발진기로 시그마-델타 모듈레이션을 이용하여 미세한 성긴 튜닝을 구현하였다. 제안된 성긴 튜닝 방법은 위상 잡음 성능의 저하 없이 작은 유효 주파수 해상도를 제공한다. 3단계의 성긴 튜닝구조로 전압제어 발진기는 광대역과 미세 튜닝 단계를 동시에 구현한다. 본 전압 제어기를 포함한 주파수 합성기는 0.13 ${\mu}m$ CMOS공정으로 구현되었고, 5.8-6.8 GHz의 대역에 3.9 kHz의 유효 주파수 해상도를 갖는다. 측정된 위상 잡음은 1 MHz 오프셋에서 -108 dBc/Hz이고, 5.9 mW 전력 소모로 16.8 %의 튜닝 범위를 갖으며, 튜닝 범위를 갖는 Figure-of-merit(FoM)은 -181.58 dBc/Hz이다.

• 한국항해항만학회:학술대회논문집
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• 한국항해항만학회 2006년도 International Symposium on GPS/GNSS Vol.1
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• pp.535-540
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• 2006

The relationship between the observable noise model and the satellite elevation angle can be modeled quite well by an exponential function.[Jin, 1996] Noise size and dependence on the elevation angle are, however, different for each observation and receiver type. Therefore, the coefficient determination of this model is an issue, and various methods including PR-CP, single difference, and time difference have been suggested. The limitations of them are difficulty to model the carrier phase noise and to eliminate bias. To overcome these disadvantages for using Jin's model, we suggest zero baseline double difference (DD) and noise sorting algorithm. Data DD technique in zero baseline is useful to eliminate all the troublesome GPS biases, and the remaining error is the sum of GPS measurement noises from two satellites. These DD residuals for hours should be sorted by the combination of satellite elevation angles, and then variance value of the residual for each combination can be estimated. Using these values, we construct an over-determined linear equation whose solution is a set of noise variance for each satellite elevation angle. With 24hr Trimble 4000ssi data, we easily worked out the coefficients of the noise model not only for pseudorange but also for carrier phase. We estimated the standard deviation of the measurement DD using our model, and plotted 1 and 3 sigma lines for every epoch to verify the representation of the residual error. 63.3% of pseudorange residual and 65.9% of phase error did not exceed the 1 sigma lines. Additionally, 99.2% and 99.5% of them lied within 3sigma line. These figures prove that the Gaussian property of measurement noise, and that the suggested model by our algorithm corresponds to the observable noise information.

• 열처리공학회지
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• 제19권2호
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• pp.103-108
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• 2006

Microstructural evolution of Pt-aluminide coated Ni-based superalloy has been investigated with ductilization heat treatment. The Pt coat was prepared on the superalloy and then aluminide coating was conducted using a pack cementation process. Samples were heat-treated at $1050^{\circ}C$ for 2 hrs and the microstructure and element analysis were preformed. A various precipitated compounds were observed within the coating layer and the diffusion region in the Pt-aluminide coating and heat treatment, indicating that the bi-phase compounds of $PtAl_2$ and NiAl were performed during the Pt-aluminide coating, whereas $M_{23}C_6$, MC, $Ni_3Al$ and ${\sigma}$ phases were precipitated in the inter-diffusion region. The bi-phase compounds of $PtAl_2$ and NiAl were transformed into the single phase compound of $PtAl_2$ with the heat treatment, increasing the amount of carbide and ${\sigma}$ phase.

• The Plant Pathology Journal
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• 제29권3호
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• pp.323-329
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• 2013

The stationary-phase sigma factor, RpoS, influences the expression of factors important in survival of Pseudomonas chlororaphis O6 in the rhizosphere. A partial proteomic profile of a rpoS mutant in P. chlororaphis O6 was conducted to identify proteins under RpoS regulation. Five of 14 differentially regulated proteins had unknown roles. Changes in levels of proteins in P. chlororaphis O6 rpoS mutant were associated with iron metabolism, and protection against oxidative stress. The P. chlororaphis O6 rpoS mutant showed increased production of a pyoverdine-like siderophore, indole acetic acid, and altered isozyme patterns for peroxidase, catalase and superoxide dismutase. Consequently, sensitivity to hydrogen peroxide exposure increased in the P. chlororaphis O6 rpoS mutant, compared with the wild type. Taken together, RpoS exerted regulatory control over factors important for the habitat of P. chlororaphis O6 in soil and on root surfaces. The properties of several of the proteins in the RpoS regulon are currently unknown.

• 한국식품영양학회지
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• 제24권2호
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• pp.258-267
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• 2011

14-3-3 is a highly conserved, ubiquitously expressed protein family. It associates with diverse cellular proteins through its specific phosphoserine/phosphothreonine-binding activity and thus contributes to the regulation of crucial cellular processes such as metabolism, signal transduction, cell-cycle control, apoptosis, protein trafficking, transcription and stress responses. This study aims to determine changes in levels of 14-3-3 isoforms and 14-3-3 - associated proteins in Helicobacter pylori(H. pylori)-infected gastric epithelial AGS cells. AGS cells were stimulated with H. pylori(NCTC 11637) at the ratio of 300:1(bacterium:cell). Western blot analysis revealed that 14-3-3 $\sigma$ was elevated at 3 hr after H. pylori treatment. Other isoforms were not significantly affected by H. pylori infection. Using immunoprecipitation to 14-3-3 $\sigma$, followed by proteomic analysis, we found that S phase kinase associated protein isoform 2 bound to 14-3-3 $\sigma$ has increased. In contrast, three proteins (DEAD-box polypeptide 3, heterogeneous nuclear ribonucleoprotein H2 and WD repeat-containing protein isoform 1) bound to 14-3-3 decreased by H. pylori infection. Our results suggest that 14-3-3 may play an important regulatory role in H. pylori-induced signal transduction in gastric epithelial cells.

• 한국주조공학회지
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• 제29권4호
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• pp.181-186
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• 2009

The interrelationship between new parameter ${\sigma}$ and maximum diameter $D_{max}$ is elaborated and discussed in comparison with four other glass forming ability (GFA) parameters, i.e. (1) super-cooled liquid region ${\Delta}T_x (=T_x - T_g)$, (2) reduced glass transition temperature $T_{rg} (=T_g/T_l)$, (3) K parameter $K (=[T_x-T_g]/[T_l -T_x])$, and (4) gamma parameter ${\gamma}(=[T_x]/[T_l+T_g])$ in Ca-based bulk metallic glass (BMG) systems. The ${\sigma}$ parameter, defined as ${\Delta}T^*{\times}P^'$, has a far better correlation with $D_{max}$ than the GFA parameters suggested so far, clearly indicating that the liquid phase stability and atomic size mismatch dominantly affect the GFA of Ca-based BMGs. Thus, it can be understood that the GFA of BMGs can be properly described by considering structural aspects for glass formation as well as thermodynamic and kinetic aspects for glass formation.

• 대한전자공학회논문지SD
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• 제47권12호
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• pp.75-82
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• 2010

본 논문은 다중대역 송수신기 CMOS RFIC 단일 칩을 위한 광대역 델타시그마 분수분주형 주파수합성기에 관한 것이다. 광대역 VCO의 LC Tank에 6-bit Switched Capacitor Array Bank를 작용하여 2340~3940 MHz의 출력주파수 범위를 가지도록 하였으며, 위상동기 전 Capacitor Bank Code를 선택하기위한 VCO Frequency Calibration 회로는 전체 주파수대역에서 $2{\mu}s$이하로 보정을 마치는 뛰어난 성능을 보여준다. 광대역 VCO로부터 T-DMB/DAB/FM Radio의 LO 신호를 생성하기 위해 선택 가능한 다중분주비 ${\div}2$, ${\div}16$, ${\div}32$를 가지는 LO 신호 발생기는 L-Band (1173 ~ 1973 MHz), VHF-III (147 ~ 246 MHz), VFH-II (74~123 MHz)에서 I/Q신호를 생성한다. Integrated Phase Noise는 전체 대역에서 0.8 degree RMS 이하로 측정되어 매우 낮은 위상잡음을 보여주었다. 또한, VCO Frequency Calibration 시간을 포함하는 주파수합성기의 전체 동기시간은 $50{\mu}s$ 이하로 측정되었다. 이 광대역 델타시그마 분수분주형 주파수합성기는 $0.13{\mu}m$ CMOS공정으로 제작되었으며, 1.2 V 전원전압에서 15.8 mA의 전류를 소모한다.

• 전자공학회논문지
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• 제54권5호
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• pp.24-32
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• 2017

본 논문에서는 생체 신호 처리를 위한 12비트 이상의 고 해상도를 갖는 저 전력 CMOS 4차 델타-시그마 변조기를 설계하였다. 제안하는 4차 델타-시그마 변조기는 시간 분할 기법을 이용하여 회로를 시간에 따라 재구성해 4개의 연산증폭기가 필요한 회로를 1개의 연산증폭기만으로 구동 시켰다. 이를 통하여 일반적인 구조보다 전력소모를 75% 감소시킬 수 있다. 또한 kT/C 잡음과 칩 면적을 고려하여 변조기의 입력단과 출력 단의 커패시터들을 안정적으로 구동하기 위하여 적분기내 가변되는 증폭기를 설계하였다. 첫 번째와 두 번째 클럭 위상에서는 2단 연산 증폭기가 동작하고, 세 번째와 네 번째 위상에서는 1단 연산 증폭기가 동작한다. 이로 인하여 두 가지 위상 조건에서 연산증폭기의 위상여유가 60~90도 이내에 존재하게 하므로서 변조기의 안정성을 크게 향상시켰다. 제안한 변조기는 $0.18{\mu}m$ CMOS N-well 1 poly 6 metal 공정을 이용하여 제작되었으며, 1.8V의 공급전압에서 $354{\mu}W$의 전력소모가 측정되었다. 256kHz의 동작주파수, 128배의 오버샘플링 비율 조건에서 250Hz의 입력 신호를 인가하였을 때, 최대 SNDR은 72.8dB, ENOB은 11.8 비트로 측정되었다. 또한 종합 성능 평가지수인 FOM(Walden)은 49.6pJ/step, FOM(Schreier)는 154.5dB로 측정되었다.