• Journal of the Korean Institute of Electrical and Electronic Material Engineers
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• v.28 no.10
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• pp.652-657
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• 2015

We have investigated the properties of Al-doped ZnO (AZO) thin films as functions of atomic layer deposition (ALD) oxidants. AZO transparent conducting oxides (TCOs) layer was deposited by ALD with adding trimethylaluminum (TMA) and diethylzinc (DEZn). AZO films were deposited at low temperature with $H_2O$ and $O_3$ as oxidants. Electrical, optical and structural properties of AZO thin films were investigated by 4-point probe, Hall effect measurement, UV-VIS, and AFM. Microstructure and atomic bonding states were investigated by HRXRD and XPS. The resistivity of AZO films grown using $H_2O$ was lower than the films grown using $H_2O$ and $O_3$, by approximately two orders of magnitude. The differences in oxygen vacancy peak intensity of AZO films were correlated to the optical and electrical properties.

• Steel and Composite Structures
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• v.34 no.2
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• pp.189-213
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• 2020

Stainless-clad (SC) bimetallic steels that are manufactured by metallurgically bonding stainless steels as cladding metal and conventional mild steels as substrate metal, are kind of advanced steel plate products. Such advanced composite steels are gaining increasingly widespread usage in a range of engineering structures and have great potential to be used extensively for large civil and building infrastructures. Unfortunately, research work on the SC bimetallic steels from material level to structural design level for the applications in structural engineering field is very limited. Therefore, the aim of this paper is to investigate the material behaviour of the SC bimetallic steels under the cyclic loading which structural steels usually could encounter in seismic scenario. A number of SC bimetallic steel coupon specimens are tested under monotonic and cyclic loadings. The experimental monotonic and cyclic stress-strain curves of the SC bimetallic steels are obtained and analysed. The effects of the clad ratio that is defined as the ratio of the thickness of cladding layer to the total thickness of SC bimetallic steel plate on the monotonic and cyclic behaviour of the SC bimetallic steels are studied. Based on the experimental observations, a cyclic constitutive model with combined hardening criterion is recommended for numerical simulation of the cyclic behaviour of the SC bimetallic steels. The parameters of the constitutive model for the SC bimetallic steels with various clad ratios are calibrated. The research outcome presented in this paper may provide essential reference for further seismic analysis of structures fabricated from the SC bimetallic steels.

• Korean Journal of Metals and Materials
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• v.50 no.10
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• pp.775-783
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• 2012

The effect of thermal annealing on the in-situ growth characteristics of intermetallics (IMCs) and the mechanical strength of Cu pillar/Sn-3.5Ag microbumps are systematically investigated. The $Cu_6Sn_5$ phase formed at the Cu/solder interface right after bonding and grew with increased annealing time, while the $Cu_3Sn$ phase formed at the $Cu/Cu_6Sn_5$ interface and grew with increased annealing time. IMC growth followed a linear relationship with the square root of the annealing time due to a diffusion-controlled mechanism. The shear strength measured by the die shear test monotonically increased with annealing time. It then changed the slope with further annealing, which correlated with the change in fracture modes from ductile to brittle at a critical transition time. This is ascribed not only to the increasing thickness of brittle IMCs but also to the decreasing thickness of the solder, as there exists a critical annealing time for a fracture mode transition in our thin solder-capped Cu pillar microbump structures.

• Geomechanics and Engineering
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• v.18 no.2
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• pp.179-188
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• 2019

This paper presents an experimental study to evaluate the effect of palm oil on the selected basic physical-chemical and geotechnical properties of kaolin. The experimental findings are further compared with literature outcomes investigating similar properties of fine grained soils subjected to contamination by different types of oils. To this end, palm oil was mixed with oven dried kaolin samples-aiding oil's interaction (coating) with dry particles first, in anticipation to emphasize the effect of oil on the properties of kaolin, which would be difficult to achieve otherwise. Oil content was limited to 40% by dry weight of kaolin, supplemented at intervals of 10% from clean kaolin samples. Observations highlight physical particle-to-particle bonding resulting in the formation of pseudo-silt sized clusters due to palm oil's interaction as evinced in the particle size distribution and SEM micrographs. These clusters, aided by water repellency property of the oil coating the kaolin particles, was analyzed to show notable variations in kaolin's consistency-measured as liquid and plastic limits. Furthermore, results from compaction tests indicates contribution of oil's viscosity on the compaction behavior of kaolin - showing decrease in the maximum dry unit weight (${\gamma}_{d,max}$) and optimum moisture content ($w_{opt}$) values with increasing oil contents, while their decrease rates were directly and inversely proportional in ${\gamma}_{d,max}$ and $w_{opt}$ values with oil contents respectively. Comparative study in similar terms, also validates this lower and higher decrease rates in ${\gamma}_{d,max}$ and $w_{opt}$ values of the fine grained soils respectively, when subjected to contamination by oil with higher viscosity.

• Journal of the Korean Society of Manufacturing Process Engineers
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• v.18 no.2
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• pp.1-6
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• 2019

With the increase in number of the athletic population and elderly demographic, the demand for orthopedic splints, which are used to support a damaged body, has rapidly increased. Current splints mainly consist of inner and outer parts, which are multiple fabrics covered with polyurethane and nonwoven fabrics, respectively. However, the laminated materials with directly applied pre-polymer coating lead to a high defect rate because of the uneven thickness on the surface. Thus, this study proposes an indirect coating method using a precise clearance controller, which enables the even application of the coating material on multiple inner parts while maintaining a constant thickness. In addition, a roll-to-roll (R2R) technique is applied instead of the sewing mechanism to bond the inner and outer materials together and enhance the productivity in the final stage. In the advanced methods, there is a storage tank that contains polyurethane, a clearance controller, and pairs of rollers in the upper and lower rows. To improve the quality of the products and optimize the equipment, three controllable factors are determined: the viscosity of polyurethane, angle of the gap controller and number of pairs of rollers in the R2R system.

• Steel and Composite Structures
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• v.51 no.5
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• pp.509-527
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• 2024

Bonding carbon fiber-reinforced polymer (CFRP) laminates have been extensively employed in the restoration of steel constructions. In addition to the mechanical properties of the CFRP, the bond strength (P_U) between the CFRP and steel is often important in the eventual strengthened performance. Nonetheless, the bond behavior of the CFRP-steel (CS) interface is exceedingly complicated, with multiple failure causes, giving the P_U challenging to forecast, and the CFRP-enhanced steel structure is unsteady. In just this case, appropriate methods were established by hybridized Random Forests (RF) and support vector regression (SVR) approaches on assembled CS single-shear experiment data to foresee the P_U of CS, in which a recently established optimization algorithm named Aquila optimizer (AO) was used to tune the RF and SVR hyperparameters. In summary, the practical novelty of the article lies in its development of a reliable and efficient method for predicting bond strength at the CS interface, which has significant implications for structural rehabilitation, design optimization, risk mitigation, cost savings, and decision support in engineering practice. Moreover, the Fourier Amplitude Sensitivity Test was performed to depict each parameter's impact on the target. The order of parameter importance was t_c> L_c > E_A > t_A > E_c > b_c > f_c > f_A from largest to smallest by 0.9345 > 0.8562 > 0.79354 > 0.7289 > 0.6531 > 0.5718 > 0.4307 > 0.3657. In three training, testing, and all data phases, the superiority of AO - RF with respect to AO - SVR and MARS was obvious. In the training stage, the values of R² and VAF were slightly similar with a tiny superiority of AO - RF compared to AO - SVR with R² equal to 0.9977 and VAF equal to 99.772, but large differences with results of MARS.

• Journal of Korean Home Economics Education Association
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• v.26 no.1
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• pp.69-80
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• 2014

The purpose of this study was to investigate the relation among family strength and self-efficacy. This subjects were the 576 middle school students living in Gwangju. Data were analyzed with SPSS 20.0 program. The major findings were as follows; First, middle school students' family strength scores were higher than median(3.00). Family respect and affection scores were highest and communication and family bonding scores were lowest. Also, self-efficacy scores were higher than median(3.00). Second, family strength and the self-efficacy showed significant correlation. Third, the male middle school students' self-efficacy was influenced by Family respect and affection. And the male middle school students' self-efficacy was explained about 29% by this variable. The Female middle school students' self-efficacy was influenced by Family respect and affection and Financial stability. And the female middle school students' self-efficacy was explained about 32% by these variables.

• Journal of Dental Rehabilitation and Applied Science
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• v.27 no.1
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• pp.1-13
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• 2011

The aim of this study was to evaluate shear bond strength of pressed reinforced composite resin ($TESCERA^{TM}$ ATL) veneering to zirconia with various surface treatments. Forty sintered zirconia specimens and forty pockmarked zirconia specimens were fabricated. All the materials were categorized as Group 1 (Control : porcelain veneering on zirconia surface), Group 2 ( $TESCERA^{TM}$ ATL dentine veneering after bonding agent application on zirconia surface), Group 3 ($TESCERA^{TM}$ ATL dentine veneering on pockmarked zirconia surface), Group 4 ($TESCERA^{TM}$ ATL dentine veneering after bonding agent application on pockmarked zirconia surface), Group 5 (Thermocycling on Group 1), Group 6 (Thermocycling on Group 2), Group 7 (Thermocycling on Group 3), and Group 8 (Thermocycling on Group 4). SBS(Shear bond strength) of 8 groups was determined with an Instron Universal Testing Machine. Also fractured surface of specimens were observed with a scanning electron microscope. There were no significant differences in the initial SBS between Group 1(control group), Group 3, and Group 4. (p>0.05) Group 2 presented the lowest SBS values. There was a no significant difference between just as 24hour water storage and simulated aging on pockmarked zirconia groups. (p>0.05) A formation of pockmarked irregularities on zirconia surface as mechanically pitted surface was reliable method for establishing a stronger bond between $TESCERA^{TM}$ ATL and zirconia-based material.

• Journal of the korean academy of Pediatric Dentistry
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• v.34 no.1
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• pp.62-72
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• 2007

The purpose of present study was to determine whether different kinds of curing lights can alter microtensile bond strength(MTBS) of class I cavity pulpal and axial wall specimens in primary molar. Thirty clean mandibular 2nd primary molar's occlusal enamel were removed and class I cavity, size of $2{\times}4{\times}2mm$ was prepared. Dentin bonding agent was applied according to manufacturer's manual. Each group was cured with Halogen Curing Unit, Plasma Curing Unit and LED Curing Unit. Composite resin was bulk filled and photo cured with same curing unit. MTBS specimens which size is $0.7{\times}0.7{\times}4mm$ were prepared with low speed saw. Specimens were coded by their curing lights and wall positions (Halogen - Axial wall group, Halogen - Pulpal wall group, Plasma - Axial wall group, Plasma - Pulpal wall group, LED - Axial wall group, LED - Pulpal walt group). MTBS were tested at 1 mm/min cross Head speed by Universal Testing Machine. Fractured surface and bonding surface was observed with SEM. T-test between axial and pulpal specimens in each curing lights, one-way ANOVA among different curing light specimens in each wall positions were done. Weibull distribution analysis was done. The results were as follows : Mean MTBS of pulpal wall specimens were significantly greater than that of axial wall specimens at each curing units(p<.05). There was no significant difference in the MTBS among three curing units at axial wall and pulpal wall. In Weibull distribution, pulpal wall specimens were more homogeneous than axial wall specimens.

• The korean journal of orthodontics
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• v.34 no.5 s.106
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• pp.439-447
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• 2004

The purpose of this study was to investigate the influence of water, saliva and blood contamination on the bonding strength of metal brackets with a self-etching primer/adhesive to enamel. Ninety-six extracted human teeth were divided into four groups. The brackets were bonded to enamel with a self- etching primer (3M/Unitek Dental Products. Monorovia California) according to one of four protocols. The teeth were bonded in a dry condition (group D) or in contamination with distilled water (group W), artificial saliva (group S). or fresh human blood (group B) Shear bond strengths were tested using an Instron Universal testing machine. After debonding. bracket and tooth surfaces were examined with a stereomicroscope. In each group, four samples were selected and examined with a Scanning electron microscope of the prepared enamel surface and resin-enamel interlace. The results obtained were summarized as follows: Shear bond Strength if group D $(15.22{\pm}2.86MPa)$ and W $(15.20{\pm}3.85 MPa)$ Were higher than in group B$(12.56{\pm}2.94MPa)$ (p<0.05). There were no statistical differences in the shear bond strengths between groups D. W and S (p>0.05). There was a tendency to have less residual adhesive remaining on the enamel surfaces of group B than group D. The SEW morphology of group D and W showed a more roughened etching pattern than group S and B. Water or saliva contamination on bending of orthodontic brackets with Transbond plus self etching primer had almost no influence on bond strength In this study, the blood contaminated group showed the lowest bond strength, but it was above the clinically acceptable bond strength (5.9-7.8 MPa, Reynold, 1975). The results of this study suggest that acceptable clinical bond strengths can be obtained in wet conditions when self-etching adhesives are used.