• Journal of the Korean institute of surface engineering
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• v.51 no.3
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• pp.164-171
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• 2018

In this study, we have fabricated pure titanium (Ti)/hydroxyapatite (HA) double layer coating on medical grade PEEK from magnetron sputtering system, an investigation was performed whether the surface can be had more improve bio-active for orthopedi/dental applications than that of non-coated one. Pure Ti and HA coating layer were obtained by a radio-frequency and direct current power magnetron sputtering system. The microstructures surface, mechanical properties and wettability of the pure Ti/HA double layer deposited on the PEEK were analyzed by scanning electron microscopy (SEM), energy dispersive X-ray spectroscopy (EDS), X-ray diffraction (XRD), nano-indentation, and contact angle test. According to the EDS and XRD results, the composition and crystal structure of pure Ti and HA coated surface were verified. The elastic modulus and hardness value were increased by pure Ti and HA coating, and the pure Ti/HA double layer coating surface has the highest value. The contact angle showed higher value for pure Ti/HA double layered coating specimens than that of non-coated (PEEK) surface.

• Journal of the Korean institute of surface engineering
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• v.46 no.5
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• pp.181-186
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• 2013

We performed plasma spraying for 2001 (Bi:Cu = 2:1), 0212 (Sr:Ca:Cu = 2:1:2) oxide powders. $Bi_2Sr_2CaCu_2Ox$ (2212) superconductor has been prepared by PMP-AT (partial melting process-annealing treatment). The 2212 phase is synthesized between Sr-Ca-Cu oxide coating layer (0212) and Bi-Cu oxide coating layer (2001) by movement of partial melted Bi on 2001 layer and the diffusion reaction (Cu, Sr, Ca) after PMP-AT. There are two different coating layers on joining process. The one is ABAB coating layers and the other is BAAB coating layers by arrangement of 2001 (A), 0212 (B) layers. We performed heat treatment these two different coating layers processes under same PMP-AT conditions. We obtained Bi-2212 superconducting layers at each experimental condition, and the result of MPMS, the critical temperature was showed about 78 K. But the microstructure images and result of EDS as each experimental variable were showed about the qualitatively different Bi-2212 superconducting phases. We also deduced the generation mechanism of Bi-2212 superconducting layer as a result of these experimental data, microstruc ture images, EDS data and phase diagram.

• Journal of Advanced Marine Engineering and Technology
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• v.24 no.1
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• pp.49-58
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• 2000

Thermal spraying is one of the most common surface coating techniques to be used for many applications and flame spraying covers a wide range of different materials which can be coated onto various substrates. The purpose of this study is to investigate the effects of mixed ratio in composite coatings on the mechanical and anti-corrosion properties. The five different types of composite coatings were made with $Al_2O_3$ ceramic and Ni-alloy powder on the mild steel substrate by flame spraying method. The mechanical properties such as microhardness, adhesive strength and erosion resistance and corrosion resistance were tested for the sprayed coating specimens. The results obtained are summarized as follows; 1. The composite coating layers greatly improve the microstructure, erosion resistance and adhesive strength by increasing the content of Ni-Al alloy. 2. Microhardness of the compsite coating layer is decreased by increasing the content of Ni-Al alloy. 3. The anti-corrosion properties is considerably improved by increasing the compsite rate of Ni-Al alloy.

• Journal of the Korean Society of Manufacturing Process Engineers
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• v.13 no.6
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• pp.1-7
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• 2014

Gas turbines for generation are operated under high temperatures, high pressures and in corrosive environments for long periods of time. This environment causes serious damage to these parts. Therefore, the material, coating, and cooling technology used with a gas turbine are important factors with regard to turbine blade development. One method that can be used to protect a product from harsh conditions is the coating technology. A turbine blade undergoes very aggressive thermal stress and experiences high-temperature fatigue. In order to reduce the surface temperature of the components and protect the blade from high-temperature flames, a thermal barrier coating (TBC) is applied to its substrate. This study confirms the applicability of an inspection system for the turbine blade coating layer using an artificial heat source.

• Journal of the Korean institute of surface engineering
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• v.53 no.6
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• pp.360-368
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• 2020

Wear resistance of cutting tools is one of the most important requirements in terms of the durability of cutting tool itself as well as the machining accuracy of the workpiece. Generally, tungsten carbide ball end mills have been processed with hard coatings for high durability and wear resistance such as diamond coating and tetrahedral amorphous carbon(ta-C) coating. In this study, we developed multilayer ta-C coatings whose wear resistance is comparable to that of diamond coating. First, we prepared single layer ta-C coatings according to the substrate bias voltage and Ar gas flow, and the surface microstructure, raman characteristics, hardness and wear characteristics were evaluated. Then, considering the hardness and wear resistance of the single layer ta-C, we fabricated multilayer coatings consisting of hard and soft layers. As a result, it was confirmed that the wear resistance of the multilayer ta-C coating with hardness of 51 GPa, and elastic recovery rate of 85% improved to 97% compared to that of the diamond coated ball end mill.

• Proceedings of the KWS Conference
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• 2005.11a
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• pp.262-264
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• 2005

$Bi_{2}Sr_{2}CaCu_{2}O_{x}$(Bi-2212) and $Bi_{2}Sr_{2}Ca_{2}Cu_{3}O_{y}$(Bi-2223) high-$T_{c}$ superconductor(HTS) coating have been prepared by plasma spraying and heaat treatment. The Bi-2212 HTS coating later is synthesized through the peritectic reaction between Sr-Ca-Cu oxide coating layer and Bi-Cu oxide coating later, and $Bi_{2}Sr_{2}CaCu_{2}O_{y}$(Bi-2212) superconducting phase grow by partial melting process. The superconducting characteristic depends strongly on the conditions of the partial melting process. the Bi-2212 HTS layer consists of the whiskers grown in the diffusion direction. Above the 2212 layer, Bi-2223 phase and secondary phase was observed. The secondary phase is distributed uniformly over the whole surface. This is caused to the microcrack on the coatings surface. Despite everything, the film shows superconducting with an onset $T_{c}$ of about 115K. There are two changes steps. One changes (1step) at 115K is due to the diamagnetism of the Bi-2223 phase and the other changes (2step) at 78K is due to the diamagnetism of the Bi-2212 phase.

• 보존과학연구
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• s.29
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• pp.65-90
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• 2008

This study examines the status and the physical features of Paraloid B-72 layers with examination of microstructure and analysis of organic matters. Paraloid B-72 layers were coated on samples from the colour layer of outer wall painting in Mireuk hall in Geumsan temple. On the basis of the previous examination result, it has made the samples which are similar to outer wall in Mireuk hall in Geumsan temple. The samples can be divided into two, one; 5% Paraloid B-72 coating and another is without coating. Then samples have been experimented under the compulsive environments of infrared radiation and immersion, thereafter compared the results of the damages and physical features between two samples. As a result of the comparison, the sample with Paraloid B-72 had more serious cracks, exfoliations and peeling layers than that of without Paraloid B-72. Otherwise, in the examination of ultraviolet radiation, the sample with Paraloid B-72 coating showed weaker physical properties, less density in structure of colour layer and less hardness in surface of colour layer than the sample without coating. The percentage of moisture content after the ultraviolet radiation was higher in the sample without Paraloid B-72 than the sample with Paraloid B-72 coating. Observing the conditions before the ultraviolet radiation, the sample with Paraloid B-72 coating demonstrated lower rate in moisture evaporation rate than the sample without Paraloid B-72. As a consequence, in examination of this samples, the change of physical features are increased in the sample with Paraloid B-72 coating than that without Paraloid B-72 when compulsive environment of heat, moisture and ultraviolet rays for a short term are imposed.

• Proceedings of the KIEE Conference
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• 1998.07d
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• pp.1340-1342
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• 1998

The diamond-like carbon(DLC) film, as an antireflection layer, is coated on a commerically used Ge window. DLC films are deposited by using an rf(13.56 MHz) plasma CVD. The optimal value of thickness and refractive index of DLC layer has been determined from the computer simulation. IR-transmittances of DLC-coated Ge windows are estimated by measuring FTIR spectra in the wavelength range of$ 2.5{\sim}25{\mu}m$. By coating the DLC film on one side of the Ge window, the transmittance measured at a wavelength of $10{\mu}m$ is about 60 %, while that of the bare Ge is lower than 50 %. Also, a higher transmittance up to about 90 % is obtained by coating the DLC film on both sides of the window. It may be suggested that the further improvement of the IR-transmittance can be achieved by more precisely controlling the thickness and the refractive index of DLC layer and also by adopting various muliti-layer antireflection structures.

• Journal of the Korean Institute of Telematics and Electronics
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• v.21 no.6
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• pp.64-69
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• 1984

We found that the maximum efficiency of Al-MIS (p-Si) solar ceil was shown at 80$\AA$ thickness of Al-film which was deposited with slower velocity than 0.6$\AA$/sec. It was coated with ZnS and SiO for Anti-Reflecting. In single coating, ZnS and SiO film had maximum Isc at 570 and 690 A thickness, respectively. We confirmed that these results agreed well with the quarter coating condition; n1d1=λ/4. In double coating, we held the one layer with its optimum thickness in single coating and controlled the other layer. The maximum value of Isc in this case was almost the same with it in single coating but was maintained its value in so wide range of thickness. Keeping the relation; n1d1=n2d2 as another way, we made the total thickness of film thinner to 70-90% of the sum of each optimum thickness in single coating. In this case Isc was higher value than 20% of it in any other previous case and was retained so wide range of thickness.

• New Physics: Sae Mulli
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• v.68 no.11
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• pp.1208-1214
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• 2018

The one-step spin coating method is reported as an excellent thin film process because it can be easily used to fabricate high-quality methyl-ammonium lead tri-iodide ($MAPbI_3$) perovskite layers. One of the important things in the one-step spin coating method towards obtaining high-quality $MAPbI_3$ layers is the anti-solvent (AS) engineering, which consists of an one-step deposition of the $MAPbI_3$ film and dripping of the AS. The properties of the $MAPbI_3$ layer were found to be strongly influenced by the amount, dispensing speed, and spraying time of the AS solution. The $MAPbI_3$ solution was prepared by dissolving lead iodide and methyl-ammonium iodide in N,N-dimethylformamide and adding N,N-dimethyl sulfoxide. Diethyl ether (DE) was used for the AS solution. The results indicate that a $MAPbI_3$ layer appropriately sprayed with DE is beneficial for improving film quality and device efficiency because nucleation of $MAPbI_3$ layer is affected by the characteristics of DE, which affect the film's crystallinity, density, and surface morphology. The $MAPbI_3$ layer, which was optimized by using 0.7 mL of DE, a 3.03 mL/sec dispensing speed, and a 7 second time to spray after spinning showed the best efficiency of 13.74%, which was reproducible.