Lim, Se Hwan;Lee, Hyosung;Shin, Eun-Jung;Han, Seok Kyu;Hong, Soon-Ku
Korean Journal of Materials Research
/
v.22
no.10
/
pp.539-544
/
2012
We have grown AlN nanorods and AlN films using plasma-assisted molecular beam epitaxy by changing the Al source flux. Plasma-assisted molecular beam epitaxy of AlN was performed on c-plane $Al_2O_3$ substrates with different levels of aluminum (Al) flux but with the same nitrogen flux. Growth behavior of AlN was strongly affected by Al flux, as determined by in-situ reflection high energy electron diffraction. Prior to the growth, nitridation of the $Al_2O_3$ substrate was performed and a two-dimensionally grown AlN layer was formed by the nitridation process, in which the epitaxial relationship was determined to be [11-20]AlN//[10-10]$Al_2O_3$, and [10-10]AlN//[11-20]$Al_2O_3$. In the growth of AlN films after nitridation, vertically aligned nanorod-structured AlN was grown with a growth rate of $1.6{\mu}m/h$, in which the growth direction was <0001>, for low Al flux. However, with high Al flux, Al droplets with diameters of about $8{\mu}m$ were found, which implies an Al-rich growth environment. With moderate Al flux conditions, epitaxial AlN films were grown. Growth was maintained in two-dimensional or three-dimensional growth mode depending on the Al flux during the growth; however, final growth occurred in three-dimensional growth mode. A lowest root mean square roughness of 0.6 nm (for $2{\mu}m{\times}2{\mu}m$ area) was obtained, which indicates a very flat surface.
Seungmin Lee;Seong Cheol Jang;Ji-Min Park;Soon-Gil Yoon;Hyun-Suk Kim
Korean Journal of Materials Research
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v.33
no.11
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pp.491-496
/
2023
As the demand for p-type semiconductors increases, much effort is being put into developing new p-type materials. This demand has led to the development of novel new p-type semiconductors that go beyond existing p-type semiconductors. Copper iodide (CuI) has recently received much attention due to its wide band gap, excellent optical and electrical properties, and low temperature synthesis. However, there are limits to its use as a semiconductor material for thin film transistor devices due to the uncontrolled generation of copper vacancies and excessive hole doping. In this work, p-type CuI semiconductors were fabricated using the chemical vapor deposition (CVD) process for thin-film transistor (TFT) applications. The vacuum process has advantages over conventional solution processes, including conformal coating, large area uniformity, easy thickness control and so on. CuI thin films were fabricated at various deposition temperatures from 150 to 250 ℃ The surface roughness root mean square (RMS) value, which is related to carrier transport, decreases with increasing deposition temperature. Hall effect measurements showed that all fabricated CuI films had p-type behavior and that the Hall mobility decreased with increasing deposition temperature. The CuI TFTs showed no clear on/off because of the high concentration of carriers. By adopting a Zn capping layer, carrier concentrations decreased, leading to clear on and off behavior. Finally, stability tests of the PBS and NBS showed a threshold voltage shift within ±1 V.
Journal of the Korea institute for structural maintenance and inspection
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v.15
no.6
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pp.156-165
/
2011
This study investigates the horizontal shear behavior of an interface between precast concrete (PC) and topping concrete(RC), and evaluates the horizontal based on the investigations by the experimental. Horizontal shear strength in connected surface is determined by the roughness an interface and the shear reinforcement or not. In this study, the main experimental parameters are the shear reinforcement types in the shape of loop-type and lattice-type, rebar spacing. A total of four specimens were shear strength tested and manufactured. As a result, the horizontal shear strength of reinforced connected surface was found to be controlled by deformation in vertical direction. Comparison of reinforcement shape, the mean initial crack load loop type specimens, the average maximum load and the junction of the average in terms of initial stiffness, respectively 33.7%, 45.9% and 55.2% were large enough. Evaluation results for shear strength equation of existing standard domestic, the loop-type reinforced 2.32 to 4.23 times, lattice-type reinforced 1.65 to 3.06 times appears to be higher. Behavior of interface or strength of structural design criteria was fairly safe side. It does not have any problems in the applied field is considered.
Won Mi-Kyoung;Park Chan-Jin;Chang Kyoung-Soo;Kim Chang-Whe;Kim Yung-Soo;Isa Zakiahbt Mohd;Ariffin Yusnidar Tajul
The Journal of Korean Academy of Prosthodontics
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v.41
no.6
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pp.720-731
/
2003
Statement of problem. The importance of fixture design and surface treatment. Purpose. The clinical success of dental in plants is affected by many factors such like as degree of osseointegration, the effective load dispersion for the prostheses, and a lot of attempts have been made to overcome the difficulties. In this study, efforts were made to find the possibility of clinical acceptance of the dental implants of newly designed surface and resorbable blast media surcace. Materials and methods. In this study, two groups of custom-made, screw-shaped implants were prepared. The first with the consisting of Branemark clone design and the other with the new design. These implants were divided into four groups according to the kinds of surface treatment. Four implants($AVANA^{(R)}$, Osstem, Busan, Korea)of each group were installed in twenty rabbits. Group A was consisted of Branemark done implant left as machined, Group B with Branemark clone implants with RBM(Resorbable blast media) surface, Group C with newly designed implants left as machined and Group D with newly designed implants with RBM surface. One of the twenty rabbits died from inflammation and the observation was made for six weeks. Specimens from four groups were observed using scanning electron microscopy with 40, 100, 1000 magnification power and microsurface structures were measured by white-light scanning interferometry for three dimensional surface roughness measurements(Accura $2000^{(R)}$, Intek-Plus, Korea.). Removal torque was measured in 17 rabbits using digital torque gauge(MGT 12R, Mark-10 corp., NY, U.S.A.) immediately after the sacrifice and two rabbits were used for the histologic preparation(EXAKT $310^{(R)}$, Heraeus Kulzer, wehrheim, Germany) of specimens and observed under light microscope. Resonance frequency measurement($Osstell^{(R)}$) was taken with the 19 rabbits at the beginning of the implant fixation and immediately after the sacrifice. Results. Following results were taken from the experiment. 1. The surface of the RBM implants as seen with SEM had rough and irregular pattern with reticular formation compared to that of fumed specimens showing different surface topographies. 2. The newly designed implant with RBM surface had high removal torque value among four groups with no statistical significance. The average removal torque was $49.95{\pm}6.70Ncm$ in Group A, $51.15{\pm}4.40Ncm$ in Group B, $50.78{\pm}9.37Ncm$ in Group C, $51.09{\pm}4.69Ncm$ in Group D. 3. The RFA values were $70.8{\pm}4.3Hz$ in Group A, $71.8{\pm}3.1Hz$ in Group B, $70.9{\pm}2.5Hz$, $72.7{\pm}2.5Hz$ in Group D. Higher values were noted in the groups which had surface treatment compared to the untreated groups with no statistical significance. 4. The results from the histomorphometric evaluation showed a mean percentage of bone-to-implant contact of $45{\pm}0.5%$ in Group A, $55{\pm}3%$ in Group B, $49.5{\pm}0.5%$ in Group C, and $55{\pm}3%$ in Group D. Quite amount of newly formed bone were observed at the surface RBM-treated implants in bone marrow space.
This experiment was conducted to investigate the effect of some soil conditioners, such as polyvinylalcohol(PVA), zeolite and perlite, on the changes of soil physical properties and on tobacco growth in paddy-upland rotated field. Soil conditioners were treated at the rates of 120kg in PVA, 500kg in zeolite and perlite per l0a, respectively. Ratio of soil aggregates formed from the treated plots tended to. be higher than those from the control in the order of PVA > perlite > zeolite. The wet aggregate stability, mean weight diameter, moisture retention and air permeability from the treated plots tended to be higher than those from the control. Amounts of water-stable aggregates of PV A-treated soil increased with higher soil moisture showing a peak at 50% of moisture content. But with respect to particle of size aggregate formed for crop growth and workability in field, it was presumed that 40% of soil moisture content would be most desirable. Visual characters of soil surface throughout the experiment clearly showed that treated soils were maintaining better surface roughness and porosity than control, but difference in water stable aggregates among treated plots tended to be narrowed. The growths of tobacco, espacially its root zone were better in conditioner treated plots than in non-treated plot showing best in PVA-treated soil.
This study was conducted to evaluate the tensile bond strength by bonding the dental bracket with Super-bond after treating the surface of dental Nickel-Chromium alloy with sandblasting, sandblasting & tin-plating, respectively, and tin-plating. 10 pieces of Nickel-Chromium alloys with brackets bonded with Super-bond without their surface treatment were sampled as a control group, 20 pieces of Nickel-Chromium alloy brackets bonded with Super-bond after treating them with sandblasting as group I, 20 pieces of Nickel-Chromium alloys tin-plated and bonded with Super-bond after sandblasting as group II, and then 20 pieces of alloys with brackets bonded with Super-bond after tin-plating as group III. The result of those examination and comparison is summarized as follows: 1. Group I showed the mean tensile bond strength of $14.41{\pm}2.24MPa$ which was highest among 4 groups, followed by group III($13.59{\pm}.51MPa$), group II($12.27{\pm}.45MPa$), and control group($10.50{\pm}1.57MPa$), respectively. However, it was shown that there was no statistically significant difference between group I and III, group III and II, and group II and control group(p>0.05). 2. The main failure pattern of those brackets showed that $70\%$ of the control group had an adhesive failure at the bracket-Superbond interface, and $30\%$ at the Nickel-Chromium alloy-Superbond interface, while other groups did the adhesive failure at the bracket-Superbond interface. 3. When examined under SEM, it was shown that adhesives were mostly attached to the surface of the Nickel-Chromium alloy for all groups while a considerable quantity of adhesives were attached to the bracket base. Then, those samples treated only with sandblasting showed the most even and remarkable roughness of their surface.
Kim, Hee-Young;Park, Kyung-Ae;Kwak, Byeong-Dae;Joo, Hui-Tae;Lee, Joon-Soo
Journal of the Korean earth science society
/
v.43
no.5
/
pp.604-617
/
2022
Sea surface temperature (SST) is a key variable that can be used to understand ocean-atmosphere phenomena and predict climate change. Satellite microwave remote sensing enables the measurement of SST despite the presence of clouds and precipitation in the sensor path. Therefore, considering the high utilization of microwave SST, it is necessary to continuously verify its accuracy and analyze its error characteristics. In this study, the validation of the microwave global precision measurement (GPM)/GPM microwave imager (GMI) SST around the Northwest Pacific and Korean Peninsula was conducted using surface drifter temperature data for approximately eight years from March 2014 to December 2021. The GMI SST showed a bias of 0.09K and an average root mean square error of 0.97K compared to the actual SST, which was slightly higher than that observed in previous studies. In addition, the error characteristics of the GMI SST were related to environmental factors, such as latitude, distance from the coast, sea wind, and water vapor volume. Errors tended to increase in areas close to coastal areas within 300 km of land and in high-latitude areas. In addition, relatively high errors were found in the range of weak wind speeds (<6 m s-1) during the day and strong wind speeds (>10 m s-1) at night. Atmospheric water vapor contributed to high SST differences in very low ranges of <30 mm and in very high ranges of >60 mm. These errors are consistent with those observed in previous studies, in which GMI data were less accurate at low SST and were estimated to be due to differences in land and ocean radiation, wind-induced changes in sea surface roughness, and absorption of water vapor into the microwave atmosphere. These results suggest that the characteristics of the GMI SST differences should be clarified for more extensive use of microwave satellite SST calculations in the seas around the Korean Peninsula, including a part of the Northwest Pacific.
Microclimatic data were measured, and the human thermal sensation was analyzed at 10 local climate zones based on the major land cover classification to investigate the thermal environment of urban areas during summer nighttime. From the results, the green infrastructure areas (GNIAs) showed an average air temperature of 1.6℃ and up to 2.4℃ lower air temperature than the gray infrastructure areas (GYIAs), and the GNIAs showed an average relative humidity of 9.0% and up to 15.0% higher relative humidity. The wind speed of the GNIAs and GYIAs had minimal difference and showed no significance at all locations, except for the forest location, which had the lowest wind speed owing to the influence of trees. The local winds and the surface roughness, which was determined based on the heights of buildings and trees, appeared to be the main factors that influenced wind speed. At the mean radiant temperature, the forest location showed the maximum value, owing to the influence of trees. Except at the forest location, the GNIAs showed an average decrease of 5.5℃ compared to GYIAs. The main factor that influenced the mean radiant temperature was the sky view factor. In the analysis of the human thermal sensation, the GNIAs showed a "neutral" thermal perception level that was neither hot nor cold, and the GYIAs showed a "slightly warm" level, which was a level higher than those of the GNIAs. The GNIAs showed a 3.2℃ decrease compared to the GYIAs, except at the highest forest location, which indicated a half-level improvement in the human thermal environment.
We measured sputtering yield of RF $O_2-plasma$ treated MgO protective layer for AC-PDP(plasma display panel) using a Focused ion Beam System(FIB). A 10 kV acceleration voltage was applied. The sputtering yield of the untreated sample and the treated sample were 0.33 atoms/ion and 0.20 atoms/ion, respectively. The influence of the plasma-treatment of MgO thin film was characterized by XPS and AFM analysis. We observed that the binding energy of the O 1s spectra, the FWHM of O 1s spectra and the RMS(root-mean-square) of surface roughness decreased to 2.36 eV, 0.6167 eV and 0.32 nm, respectively.
Kim, Young-Soon;Shin, Jiho;Kim, Hyung-Il;Cho, Joong-Hee;Seo, Hyung-Ki;Kim, Gil-Sung;Shin, Hyung-Shik
Korean Chemical Engineering Research
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v.43
no.4
/
pp.495-502
/
2005
Copper was plated on the tungsten substrate by use of a direct copper electroless plating. The optimum deposition conditions were found to be with a concentration of $CuSO_4$ 7.615 g/L, EDTA of 10.258 g/L, and glyoxylic acid of 7 g/L, respectively. The solution temperature was maintained at $60^{\circ}C$. The pH was varied from 11.0 to 12.8. After the deposition, the properties of the copper film were investigated with X-ray diffractometer (XRD), Field emission secondary electron microscope (FESEM), Atomic force microscope (AFM), X-ray photoelectron spectroscope (XPS), and Rutherford backscattering spectroscope (RBS). The best deposition condition was founded to be the solution pH of 11.8. In the case of 10 min deposition at the pH of 11.8, the grain shape was spherical, Cu phase was pure without impurity peak ($Cu_2O$ peak), and the surface root mean square roughness was about 11 nm. The thickness of the film turned out to be 140 nm after deposition for 12 min and the deposition rate was found to be about 12 nm/min. Increase in pH induced a formation of $Cu_2O$ phase with a long rectangular grain shape. The pH control seems to play an important role for the orientation of Cu in electroless deposition. The deposited copper concentration was 99 atomic percent according to RBS. The resulting Cu/W film yielded a good adhesive strength, because Cu/W alloy forms during electroless deposition.
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