• Title/Summary/Keyword: heating temperature and time

Search Result 1,375, Processing Time 0.028 seconds

Temperature Calibration of a Specimen-heating Holder for Transmission Electron Microscopy

  • Kim, Tae-Hoon;Bae, Jee-Hwan;Lee, Jae-Wook;Shin, Keesam;Lee, Joon-Hwan;Kim, Mi-Yang;Yang, Cheol-Woong
    • Applied Microscopy
    • /
    • v.45 no.2
    • /
    • pp.95-100
    • /
    • 2015
  • The in-situ heating transmission electron microscopy experiment allows us to observe the time- and temperature-dependent dynamic processes in nanoscale materials by examining the same specimen. The temperature, which is a major experimental parameter, must be measured accurately during in-situ heating experiments. Therefore, calibrating the thermocouple readout of the heating holder prior to the experiment is essential. The calibration can be performed using reference materials whose phase-transformation (melting, oxidation, reduction, etc.) temperatures are well-established. In this study, the calibration experiment was performed with four reference materials, i.e., pure Sn, Al-95 wt%Zn eutectic alloy, NiO/carbon nanotube composite, and pure Al, and the calibration curve and formula were obtained. The thermocouple readout of the holder used in this study provided a reliable temperature value with a relative error of <4%.

An Analytic Study on Early aged Freezing Damage Prevention and Thermal Crack Control of Concrete in Cold-Weathering Mat Foundation Construction (동절기 매트기초공사시 콘크리트의 초기동해방지 및 온도충격제어에 관한 해석적 연구)

  • 이도범;김효락;박지훈;최일호
    • Proceedings of the Korea Concrete Institute Conference
    • /
    • 2001.05a
    • /
    • pp.807-812
    • /
    • 2001
  • This study is peformed for checking the limitation and application of each curing/heating methods on cold-weathering mat foundation construction, considering temperature control, early strength security and temperature declination range limit, by means of concrete material properties and thermal analysis technique that were published previously. In the result of this analysis, we checked the open air temperature and mat depth that are possible to apply each curing/heating methods on cold-weathering construction and found curing/heating time of each methods that is able to prevent early aged freezing damage and thermal crack

  • PDF

Electrical Property Evaluation of Printed Copper Nano-Ink Annealed with Infrared-Lamp Rapid Thermal Process (적외선 램프를 이용하여 소결한 구리 나노잉크의 전기적 특성 평가에 관한 연구)

  • Han, Hyun-Suk;Kim, Changkyu;Yang, Seung-Jin;Kim, Yoon-Hyun
    • Korean Journal of Materials Research
    • /
    • v.26 no.4
    • /
    • pp.216-221
    • /
    • 2016
  • A sintering process for copper based films using a rapid thermal process with infrared lamps is proposed to improve the electrical properties. Compared with films produced by conventional thermal sintering, the microstructure of the copper based films contained fewer internal and interfacial pores and larger grains after the rapid thermal process. This high-density microstructure is due to the high heating rate, which causes the abrupt decomposition of the organic shell at higher temperatures than is the case for the low heating rate; the high heating rate also induces densification of the copper based films. In order to confirm the effect of the rapid thermal process on copper nanoink, copper based films were prepared under varying of conditions such as the sintering temperature, time, and heating rate. As a result, the resistivity of the copper based films showed no significant changes at high temperature ($300^{\circ}C$) according to the sintering conditions. On the other hand, at low temperatures, the resistivity of the copper based films depended on the heating rate of the rapid thermal process.

A Study on the External Wall Heating Temperature Distribution According to Opening Size in Building (건물의 개구부 크기에 따른 외벽 수열온도분포에 관한 연구)

  • Jung, Ui-In;Hong, Sang-Hun;Kim, Bong-Joo
    • Journal of the Korea Institute of Building Construction
    • /
    • v.20 no.3
    • /
    • pp.261-267
    • /
    • 2020
  • This study used a real-scale model experiment to reproduce internal fires in residential buildings such as a multi-dwelling unit, in order to prevent damage caused by tens of thousands of fires witnessed each year and to take measures to cope with them. For experimental conditions, different opening sizes were applied to measure and analyze the heating temperature of the exterior wall. Results drawn are as following: when the experiment was conducted with opening sizes(horizontal length) each at 2,000mm, 1,600mm, and 1,400mm, the flashover occurred at 630 seconds, 505 seconds and 510 seconds, respectively. Also, the total heating time, in proportion to this, came to 815 seconds, 713 seconds and 721 seconds. The maximum heating temperature of the exterior wall by the opening size reached 282.4℃ at 2,000mm, 382.9℃ at 1,600mm, and 423.8℃ at 1,400mm. This represented that as the opening size gets smaller, the heating temperature of the exterior wall by fire spread becomes higher.

Floor Heating Characteristics of Latent Heat Storage - Bioceramic Ondol - Focused on Theoretical Analysis - (잠열 축열 - 바이오 세라믹 온돌의 난방 특성 - 이론적 분석을 중심으로 -)

  • 송현갑;유영선
    • Proceedings of the Korea Society for Energy Engineering kosee Conference
    • /
    • 1995.05a
    • /
    • pp.213-222
    • /
    • 1995
  • Korean traditional Ondol with the sensible heat storage medium has been for a long time used as residential heating system, in these days the concrete Ondol without the heat storage medium was realized as the heating system in the private houses and the apartments. This floor heating system is good for our health. But the concrete Ondol is not desirable for the energy saving and for the maintenance of comfortable room temperature because the heat storage medium is not employed in the concrete Ondol. And as the hot water circulating pipes ate buried under the the concrete floor, the concrete Ondol system has some kind of problems to be improved. Therefore the new type of Ondol system was developed in this study. And the new Ondol was consisted of latent heat storage material as heat storage medium with a great heat capacity and bioceramics as medium to maintain comfortable room temperature. In this study, the heat transfer characteristics of latent heat storage-bioceramic Ondol was analyzed theoretically.

  • PDF

Catch-fire Temperature and Amount of Combustion-Heat on the Fuel of Miscanthus type (참억새(Miscanthus)燃料의 着火溫度 및 燃燒熱量)

  • Kim, Kwan-Soo;In-Soo Jang;Jae-Soon Lee
    • The Korean Journal of Ecology
    • /
    • v.18 no.4
    • /
    • pp.483-491
    • /
    • 1995
  • This study examined the relationship among catch-fire, burning, maximum temperature (MT), amount of combustion-heat (ACH), and combustive time (CT) in heating temperature treated with the same amount of each organ of Miscanthus. In the survey sites, about 19% of the areaswere covered by Miscanthus types, and the dry weight of Miscanthus and debris on the ground were 1,164 and 178 g/㎡, respectively. At 350℃ and 400℃, the rise of temperature by Culm type (culms and ears) and Leaf type (leaves and debris) were 90℃ and 82℃, respectively. At 350℃, durning time (BT) of culms-200, ears-200, ears-200, leaves-200 and debris-200 was 0-10’30”, 0-07’40”, 0-04’20”and 0-02’40”, and that at 400℃ was 0-01’20”, 0-00’50” 0-00’35”and 0-00’30”, respectively. BT was shorter at higher temperatures, and BT of Leaf type was shorter than that of Culm type. The amount of samples consumed was as follows: Culm type (culms-200 and ears-200) was 14.6g and 12.6g more than Leaf type (leaves-200 and debris-200) at 350℃ and 400℃, respectively. The total amount of combustion-heat (TACH) of samples was 5,859.7 kcal. The amount of mean combustion-heat generated from sample at 350℃ and 400℃ differed little: 727.6 kcal (24.9%) at 350℃ and 737.3 kcal (26.0%) at 400℃.

  • PDF

Effect of heating temperature to remove NOx by sludge pellet (Sludge Pellet의 NOx제거특성에 미치는 온도의 영향)

  • Kim, Young-Ju;Park, Jae-Yoon;Park, Hong-Jae;Song, Won-Seob;Park, Sang-Hyun;Bae, Myung-Whan
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
    • /
    • 2002.07b
    • /
    • pp.922-926
    • /
    • 2002
  • In this paper, in order to investigate the catalytic effect of the sludge exhausted from waterworks as heating temperature for NOx removal, we measure NO, $NO_2$ concentration as increasing temperature of sludge pellets and applying high voltage to sludge pellets in a quartz-glass reactor at the same time. NO initial concentration is 100ppm balanced with air gas in a mixing chamber. The gas flow is 5[l/min] and the heating temperature of sludge pellets in a quartz-glass reactor is adjusted from $200[^{\circ}C]$ $400[^{\circ}C]$ to investigate the effect of sludge pellets for removal NOx$(NO+NO_2)$ as increasing temperature. $BaTiO_3$ pellets is filled in a packed-bed reactor for corona discharge to measure how much NOx$(NO+NO_2)$ is removed after generating $NO_2$ from the packed-bed reactor. AC[60Hz] voltage is supplied to the reactor for discharge. In the result, $NO_2$ concentration is decreased by sludge pellets without heating temperature for sludge pellets in case of sludge pellets done heat treatment, however NO concentration is almost the same to be compared NO initial concentration. As increasing heating temperature for sludge pellets, $NO_2$ adsorbed on the sludge surface done heat treatment is converted to NO by the thermal energy, so NO concentration is extremely increased by reduction decomposition of $NO_2$. Finally, We think the sludge is possible to use for reduction catalysts, however we need to study more about the possibility and endurance of sludge as catalysts for NOx removal.

  • PDF

Numerical Study of Double Diffusive Convection of a Stratified Fluid in an Annulus Due to Lateral Heating (환형밀폐용기내 성층화된 유체의 옆면가열에 의한 이중확산대류에 관한 수치해석)

  • 강신형;전창덕;이진호
    • Transactions of the Korean Society of Mechanical Engineers
    • /
    • v.19 no.7
    • /
    • pp.1720-1730
    • /
    • 1995
  • Finite-difference analysis was conducted to study the natural convection of a stably stratified salt-water solution in an annulus due to lateral heating. The main purpose of this study is to examine in detail the multi-layered flow structure. Calculation was thus made for R $a_{\eta}$=2*10$^{5}$ and 6.5*10$^{5}$ . Formation of layered flow structure, merging process of layers, the corresponding temperature and concentration distributions, Nusselt number variations with time are examined. Numerical results show that in each layer, the temperature profile looks 'S`-shaped and the concentration profile is uniform due to the convective mixing. The formation of the roll and the layer is governed by natural convection due to the temperature gradient and the merging process of the layer by diffusion of the concentration.ation.

PREDICTION OF AERODYNAMIC HEATING ON A SUPERSONIC MISSILE (초음속 유도탄 공력가열 예측)

  • Sun, Chul;Ahn, C.S.
    • 한국전산유체공학회:학술대회논문집
    • /
    • 2007.04a
    • /
    • pp.134-137
    • /
    • 2007
  • Aero-Heating phenomenon is one of the severe problems occurring in high speed missile flight. in the high speed flight, not only stagnation point but also aft body parts encounter high temperature related structural problems. But the phenomenon is not easy to predict accurately because unsteady calculation according to a flight trajectory is needed, and takes much time. In this Paper, a fast and precise scheme is introduced, which calculates heat flow and temperature by simple pressure field prediction on a missile.

  • PDF

NUMERICAL ANALYSIS FOR UNSTEADY THERMAL STRATIFIED FLOW WITH HEAT TRACING IN A HORIZONTAL CIRCULAR CYLINDER

  • Jeong, Ill-Seok;Song, Woo-Young;Park, Man-Heung
    • Proceedings of the Korean Nuclear Society Conference
    • /
    • 1997.05a
    • /
    • pp.304-309
    • /
    • 1997
  • A method to mitigate the thermal stratification flow of a horizontal pipe line is proposed by heating external bottom of the pipe with electrical heat tracing. Unsteady two dimensional model has been used to numerically investigate an effect of the external Denting to the thermally stratified flow. The dimensionless governing equations are solved by using the control volume formulation and SIMPLE algorithm. Temperature distribution, streamline profile and Nusselt numbers of fluids and pipe walls with time are analyzed in case of externally heating condition. no numerical result of this study shows that the maximum dimensionless temperature difference between the hot and the cold sections of pipe inner wall is 0.424 at dimensionless time 1,500 ann the thermal stratification phenomena is disappeared at about dimensionless time 9,000. This result means that external heat tracing can mitigate the thermal stratification phenomena by lessening $\Delta$ $T_{ma}$ about 0.1 and shortening the dimensionless time about 132 in comparison with no external heat tracing.rnal heat tracing.

  • PDF