• Korean Journal of Materials Research
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• v.24 no.11
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• pp.573-577
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• 2014

The existing metal getters are invariably covered with thin oxide layers in air and the native oxide layer must be dissolved into the getter materials for activation. However, high temperature is needed for the activation, which leads to unavoidable deleterious effects on the devices. Therefore, to improve the device efficiency and gas-adsorption properties of the device, it is essential to synthesize the getter with a method that does not require a thermal activation temperature. In this study, getter material was synthesized using palladium oxide (PdOx) which can adsorb $H_2$ gas. To enhance the efficiency of the hydrogen and moisture absorption, a porous layer with a large specific area was fabricated by an etching process and used as supporting substrates. It was confirmed that the moisture-absorption performance of the $SiO_2/Si$ was characterized by water vapor volume with relative humidity. The gas-adsorption properties occurred in the absence of the activation process.

• Journal of the Korean Vacuum Society
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• v.14 no.1
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• pp.1-6
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• 2005

Getters are invariably covered with thin layers of oxides even in air. For the getter to function properly it is necessary to activate them by heating in vacuum during which the oxide layer is removed exposing clean surface. The so-called activation temperature is an important parameter along with gas sorption capacity since it determines the maximum temperature of a device in which a getter can be installed. Nevertheless, no standard method to measure activation temperature has been documented yet. In this study, a relatively simple method to measure the activation temperature based on the ultimate pressure measurement was suggested. The activation temperature of TiZrV alloy measured by the method was between 100℃～200℃.

• Journal of the Korean Magnetics Society
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• v.18 no.3
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• pp.109-114
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• 2008

The samples were synthesized by using a solid state reaction. The X-ray diffraction pattern for $Ti_{0.96}Co_{0.02}Fe_{0.02}O_2$ showed a pure rutile phase with tetragonal structure, Mixtures of the proper proportions of the elements sealed in evacuated quartz ampoule were heated at $870{\sim}930^{\circ}C$ for one day and then slowly cooled down to room temperature at a rate of $10^{\circ}C$/h. In order to obtain single phase material, it was necessary to grind the sample after the first firing and to press the powders into pellets before annealing them for a second time in evacuated and sealed quartz ampoule. Magnetic properties have been investigated using the vibrating sample magnetometer (VSM). Room temperature magnetic hysteresis (M-H) curve showed an obvious ferromagnetic behavior and the magnetic moment per Fe atom under the applied of 0.8 T was estimated to be about $1.5\;{\mu}_B$/CoFe. But the magnetic moment per Fe atom under the applied of 0.8 T was estimated to be about $0.02\;{\mu}_B$/CoFe without Ti-getter. Size of particles is about $1\;{\mu}m$ using the transmission electron microscope (TEM). The ingredients of sample are distributed irregular in particles. Only Fe get shown on the surface of particles.

• 한국정보디스플레이학회:학술대회논문집
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• 2006.08a
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• pp.1063-1066
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• 2006

We report the transparent getter performance of $POCl_3$ and amine based system by using the acid-base reaction in the fastest chemical reaction for top emitting OLEDs. OLED device including synthesized getter component exhibited stable current-voltage curve after 500 hours under $60^{\circ}C$, 90% RH storage condition and showed stable surface performance until 520 hours.

• Journal of the Korean Magnetics Society
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• v.17 no.1
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• pp.43-46
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• 2007

The samples were synthesized by using a solid state reaction. The X-ray diffraction pattern for $Ti_{0.96}Co_{0.02}Fe_{0.02}O_2$ showed a pure rutile phase with tetragonal structures. Mixtures of the proper proportions of the elements sealed in evacuated quartz ampoule were heated at $870{\sim}930^{\circ}C$ for one day and then slowly cooled down to room temperature at a rate of $10^{\circ}C/h$. In order to obtain single phase material, it was necessary to grind the sample after the first firing and to press the powders into pellets before annealing them for a second time in evacuated and sealed quartz ampoule. Magnetic properties have been investigated using the vibrating sample magnetometer(VSM). Room temperature magnetic hysteresis(M-H) curve showed an obvious ferromagnetic behavior and the magnetic moment per Fe atom under the applied of 0.8T was estimated to be about $1.3{\mu}_B/CoFe$. But the magnetic moment per Fe atom under the applied of 0.8T was estimated to be about $0.02{\mu}_B/CoFe$ without Ti-getter.

• Proceedings of the Korean Radioactive Waste Society Conference
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• 2003.11a
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• pp.117-123
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• 2003

In succession to the previous paper, the tritium injection system and the regeneration system of the tritium handling system are presented. Both systems should be placed inside glove boxes since there can be potential leakage of tritium from these systems. The tritium injection system should be capable of measuring the exact amount of the injected tritium to keep track of the tritium inventory. The tritium injection system is designed to recover the remaining tritium from the system after injection for the minimization of tritum release to the environment as well as for the recovery of precious resource. TRS equipment such as MS, Ni catalyst bed, and metal getter are regenerated with a standalone regeneration system. Unlike other equipments which can be regenerated by heating and purging with appropriate gas, regeneration of the metal getter used to recover tritium is somewhat complicated.

• Proceedings of the Korean Vacuum Society Conference
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• 2012.08a
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• pp.261-261
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• 2012

This paper presents the understandings carried out for the installation of the hydrogen reservoir of the multi-gap pseudospark switch under developing for the accelerator applications. As a cold cold cathode switch, the pseudospark switch could replace the thyratron switch which has hot cathode and being used well currently in the high power field such as laser and accelerator applications. Especially in the klystron modulator, the key component is a switch which mostly defines the jitter and the instability of the modulator system. To get the less jitter and the instability, we need to find proper range of the pressure for the gas discharge inside gas switch. This could be achieved by the understanding of the characteristic of the nonevaporable getter (NEG) which is used as a hydrogen reservoir for the switch. Therefore we verified the characteristics of the NEG (St 172, Saes) and its installation in the switch. Finally we controlled the getter to find best pressure point for the pseudospark switch.

• Korean Journal of Materials Research
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• v.15 no.2
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• pp.79-84
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• 2005

The lowest activation temperature of a commercial vacuum getter reported so far in literature was about $400^{\circ}C$. Recently, $Ti_{0.3}Zr_{0.2}V_{0.5}$ alloy has been reported to exhibit the activation temperature lower than $200^{\circ}C$ when they are prepared as thin film. In this study, the alloy was prepared as bulk form and its activation temperature and hydrogen sorption properties were investigated in compliance with a standard method. The alloy powder was prepared by arc melting and subsequent HDH(Hydride-DeHydride) process. The activation temperature of the alloy was estimated from the ultimate pressure-temperature curve and located between $150^{\circ}C\;and\;200^{\circ}C$. The hydrogen sorption speed measured by an orifice method was 0.895 liter/sec which is comparable to thin film of same composition.

• Journal of the Korean Institute of Illuminating and Electrical Installation Engineers
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• v.23 no.5
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• pp.29-35
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• 2009

Field emission displays(FED) are currently being study as a potential flat technology. The purpose of this project shows the research result of vacuum packaging technology for the development of FED. For FED vacuum packaging, the bonding of glass/glass, the exhaust of vacuum and getter technology have been studied for vacuum packaging technology The simulation and vacuum sealing, and glass/glass bonding are also extensively studied. The glass/glass bonding is formed by using the frit glass and the Inside pressure of complete panel showed of $2{\times}10^{-5}$[Torr]. As a getter result, the increase of pressure has been showed the decrease of outgassing effect by using thin film getter.

• Korean Journal of Materials Research
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• v.16 no.2
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• pp.116-122
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• 2006

The effects of milling time in argon and hydrogen atmospheres on the hydrogen sorption speed of a getter alloy, $Zr_{57}V_{36}Fe_{7}$, was studied. The hydrogen sorption speed of milled alloys was evaluated at room temperature. In argon, as the oxygen content increased with milling time, the hydrogen sorption speed decreased accordingly. In hydrogen, on the other hand, the oxygen content decreased at first with milling time but started increasing after 5 hrs of milling time. Similar to the case of argon, however, the hydrogen sorption speed changed exactly in the opposite direction with the oxygen content, exhibiting the maximum rate at 5 hrs. These results suggest that in both atmospheres the hydrogen sorption speeds are inversely related with the oxygen contents.