• Title/Summary/Keyword: box-behnken design

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Effect of the supernatant reflux position and ratio on the nitrogen removal performance of anaerobic-aerobic slaughterhouse wastewater treatment process

  • Tong, Shuang;Zhao, Yan;Zhu, Ming;Wei, Jing;Zhang, Shaoxiang;Li, Shujie;Sun, Shengdan
    • Environmental Engineering Research
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    • v.25 no.3
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    • pp.309-315
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    • 2020
  • Slaughterhouse wastewater (SWW) is characterized as one of the most harmful agriculture and food industrial wastewaters due to its high organic content. The emissions of SWW would cause eutrophication of surface water and pollution of groundwater. This study developed a pilot scale anaerobic-aerobic slaughterhouse wastewater treatment process (AASWWTP) to enhance the chemical oxygen demand (COD) and total nitrogen (TN) removal. The optimum supernatant reflux position and ratio for TN removal were investigated through the modified Box-Behnken design (BBD) experiments. Results showed that COD could be effectively reduced over the whole modified BBD study and the removal efficiency was all higher than 98%. The optimum reflux position and ratio were suggested to be 2 alure and 100%, respectively, where effluent TN concentration was satisfied with the forthcoming Chinese discharge standard of 25 mg/L. Anaerobic digestion and ammonia oxidation were considered as the main approaches for COD and TN removal in the AASWWTP. The results of inorganic nutrients (K+, Na+, Ca2+ and Mg2+) indicated that the SWW was suitable for biological treatment and the correspondingly processes such as AASWWTP should be widely researched and popularized. Therefore, AASWWTP is a promising technology for SWW treatment but more research is needed to further improve the operating efficiency.

Optimization Condition of Astaxanthin Extract from Shrimp Waste Using Response Surface Methodology (반응 표면 분석법을 사용한 새우껍질에서 astaxanthin 추출 조건의 최적화)

  • Yoon, Chang Hwan;Bok, Hee Sung;Choi, Dae Ki;Row, Kyung Ho
    • Korean Chemical Engineering Research
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    • v.50 no.3
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    • pp.545-550
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    • 2012
  • A 17-run Box-Behnken design (BBD) was used to optimize the extraction conditions of astaxanthin from shrimp waste. Three factors such as ratio of ethanol to raw material, extraction temperature ($^{\circ}C$) and extraction time (min) were investigated. The adjusted coefficient of determination ($R^2{_{adj}}$) for the model was 0.9218, and the probability value (p=0.0003) demonstrated a high significance for the regression model. The optimum extraction conditions were found to be: optimized ratio of ethanol to raw material 29.7, extraction temperature $49.5^{\circ}C$ and extraction time 59.9 min. Under these conditions, the mean extraction yield of astaxanthin was $17.80{\mu}g/g$, which was in good agreement with the predicted model value. Under these conditions, validation experiments were done and the mean extraction yield of astaxanthin was $17.77{\mu}g/g$, which is in good agreement with the predicted model value.

A Study on the Optimal Welding Condition for Root-Pass in Horizontal Butt-Joint TIG Welding (수평자세 맞대기 TIG 초층용접에서 최적용접조건의 선정에 관한 연구)

  • Jung, Sung Hun;Kim, Jae-Woong
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.41 no.4
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    • pp.321-327
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    • 2017
  • In this study, to investigate the shape of the back bead as a weld quality parameter and to select the optimal condition of the root-pass TIG welding of a horizontal butt-joint, an experimental design and the response surface method (RSM) have been employed. Three parameters are used as input variables, which include the base current, peak current, and welding speed. The back bead width is selected as an output variable representing the weld quality, the target value of the width is 5.4 mm. Conducting the experiments according to the Box-Behnken experimental design, a $2^{nd}$ regression model for the back bead width was made, and the validation of the model was confirmed by using the F-test. The desirability function was designed through the nominal-the-best formula for the appropriate back bead width. Finally, the following optimal condition for welding was selected using the RSM: base current of 0.9204, peak current of 0.8676, and welding speed of 0.3776 in coded values. For verification, a test welding process under the optimal condition was executed and the result showed the back bead width of 5.38 mm that matched the target value well.

Optimization of As Bioleaching by Herbaspirillum sp. GW103 Coupled with Coconut Oil Cake

  • Govarthanan, Muthusamy;Praburaman, Loganathan;Kim, Jin-Won;Oh, Sae-Gang;Kamala-Kannan, Seralathan;Oh, Byung-Taek
    • Journal of Soil and Groundwater Environment
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    • v.20 no.2
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    • pp.47-54
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    • 2015
  • The objective of this study was to optimize the experimental conditions for bioleaching of arsenic (As) using Herbaspirillum sp. GW103 and to understand the interaction between bacteria and As during bioleaching. Five variables, temperature, time, CaCO3, coconut oil cake, and shaking rate, were optimized using response surface methodology (RSM) based Box-Behnken design (BBD). Maximum (73.2%) bioleaching of As was observed at 30℃, 60 h incubation, 1.75% CaCO3, 3% coconut oil cake, and 140 rpm. Sequential extraction of bioleached soil revealed that the isolate Herbaspirillum sp. GW103 significantly reduced 28.6% of water soluble fraction and increased 38.8% of the carbonate fraction. The results of the study indicate that the diazotrophic bacteria Herbaspirillum sp. could be used for bioleaching As from mine soil.

Optimization of Color Sorting Process of Shredded ELV Bumper using Reaction Surface Method (반응표면법을 이용한 폐자동차 범퍼 파쇄물의 색채선별공정 최적화 연구)

  • Lee, Hoon
    • Resources Recycling
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    • v.28 no.2
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    • pp.23-30
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    • 2019
  • An color sorting technique was introduced to recycle End-of-life automobile shredded bumpers. The color sorting is a innovate method of separating the differences in the color of materials which are difficult to separate in gravity and size classification by using a camera and an image process technique. Experiments were planned and optimal conditions were derived by applying BBD (Box-Behnken Design) in the reaction surface method. The effects of color sensitivity, feed rate and sample size were analyzed, and a second-order reaction model was obtained based on the analysis of regression and statistical methods and $R^2$ and p-value were 99.56% and < 0.001. Optimum recovery was 94.1% under the conditions of color sensitivity, feed rate and particle size of 32%, 200 kg/h, and 33 mm respectively. The recovery of actual experiment was 93.8%. The experimental data agreed well with the predicted value and confirmed that the model was appropriate.

Development of Carbon-based Adsorbent for Acetylene Separation Using Response Surface Method (반응 표면 분석법을 활용한 Acetylene 분리용 탄소기반 흡착제 개발)

  • Choi, Minjung;Yoo, Kye Sang
    • Applied Chemistry for Engineering
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    • v.30 no.1
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    • pp.29-33
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    • 2019
  • Carbon nanotubes, nanofibers and powders were used for acetylene adsorption experiments. A total of 15 different experiments were designed by 3-level of Box-Behnken Design (BBD) with 3 factors including the Pd concentration of 0 to 5%, adsorption temperature of 30 to $80^{\circ}C$ and $C_2H_2/CO_2$ of 3 to 10. Based on those data, a second order polynomial regression analysis was used to derive the adsorption amount prediction equation according to operating conditions. The adsorption temperature showed the greatest influence index while the $C_2H_2/CO_2$ ratio showed the smallest according to the F-value measurement of the ANOVA analysis. However, there was little interaction between major factors. In the adsorption optimization analysis, a 22.0 mmol/g was adsorbed under the conditions of Pd concentration of 3.0%, adsorption temperature of $47^{\circ}C$ and $C_2H_2/CO_2$ of 10 with 95.9% accuracy.

Optimization for Preparation of Malic acid-catalyzed Ginsenoside Rg3 by Response Surface Methodology (반응 표면 분석법을 이용한 홍삼 사포닌으로부터의 사과산 활용 진세노사이드 Rg3 전환 최적화)

  • Ki Seong Kim;Junseong Park
    • Journal of the Society of Cosmetic Scientists of Korea
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    • v.49 no.4
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    • pp.375-383
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    • 2023
  • Malic acid-catalyzed transformation has been developed to produce ginsenoside Rg3 which is increasingly in demand as a functional ingredient. The optimization of the conversion of red ginseng saponin (RGS) to ginsenoside Rg3 by acid catalyzed transformation was carried out using Box-Behnken design (BBD) based on Response Surface Analysis (RSM). The main independent variables were malic acid concentration, temperature, and reaction time. Conversion of ginsenoside Rg3 was performed according to BBD model and optimization conditions were analyzed. The concentration of the converted ginsenoside Rg3 ranged from 1.548 mg/L to 4.558 mg/L, and the highest production was obtained under the condition of reacting 1% malic acid, 50 ℃ and 9h. Consequently, The independent variables affecting the production of ginsenoside Rg3 were identified in the following order: malic acid concentration, reaction time and temperature. In addition, it was confirmed that the interaction between malic acid concentration and reaction time had a greater influence than the temperature.

Analysis of Characteristics and Optimization of Photo-degradation condition of Reactive Orange 16 Using a Box-Behnken Method (실험계획법 중 Box-Behnken(박스-벤켄)법을 이용한 반응성 염료의 광촉매 산화조건 특성 해석 및 최적화)

  • Cho, Il-Hyoung;Lee, Nae-Hyun;Chang, Soon-Woong;An, Sang-Woo;Yonn, Young-Han;Zoh, Kyung-Duk
    • Journal of Korean Society of Environmental Engineers
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    • v.28 no.9
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    • pp.917-925
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    • 2006
  • The aim of our research was to apply experimental design methodology in the optimization of photocatalytic degradation of azo dye(Reactive orange 16). The reactions were mathematically described as a function of parameters amount of $TiO_2(x_1)$, and dye concentration($x_2$) being modeled by the use of the Box-Behnken method. The results show that the responses of color removal(%)($Y_1$) in photocatalysis of dyes were significantly affected by the synergistic effect of linear term of $TiO_2(x_1)$ and dye concentration($x_2$). Significant factors and synergistic effects for the $COD_{Cr}$, removal(%)($Y_2$) were the linear term of $TiO_2(x_1)$ and dye concentration($x_2$). However, the quadratic term of $TiO_2(x_1^2)$ and dye concentration($x_2^2$) had an antagonistic effect on $Y_1$ and $Y_2$ responses. Canonical analysis indicates that the stationary point was a saddle point for $Y_1$ and $Y_2$, respectively. The estimated ridge of maximum responses and optimal conditions for $Y_1:(X_1,\;X_2)$=(1.11 g/L, 51.2 mg/L) and $Y_2:(X_1,\;X_2)$=(1.42 g/L, 72.83 mg/L) using canonical analysis was 93% and 73%, respectively.

The Shape Optimal Design of Shaft Serration Using Design of Experiment and Finite Element Method (실험계획법과 유한요소법을 이용한 주축계의 세레이션 형상 최적설계)

  • Kim, Eui-Soo;Kim, Byung-Min
    • Journal of the Korean Society for Precision Engineering
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    • v.25 no.8
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    • pp.72-79
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    • 2008
  • To meet demand of big capacity and high speed rotation for washing machine, more stress from bending and twisting are complexly loaded onto the shaft supporting the horizontal drum, causing problems in fracture strength and fatigue life. Shafting system is mainly divided into flange and shaft. Shaft and flange connected by inserting shaft serration into flange on the process of die casting. When the system is operating, the gap is formed between serration and flange. But, Serration has various design factors and the optimal values can't be easily determined. Using a design of experiment (DOE) based on the FEM (Finite Element Method), this study was performed investigating the interaction effect between the various design factors as well as the main effect of the each design factor under bending, twist and vibration and proposed optimum design using box-behnken method among response surface derived from regression equation of simulation-based DOE.

Statistical Characteristics of Diazinon Degradation using E-beam (전자빔을 이용한 통계적 Diazinon 분해특성 연구)

  • Lee, Sijin
    • Journal of the Korean GEO-environmental Society
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    • v.14 no.5
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    • pp.57-63
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    • 2013
  • In this study, the characteristics of degradation and mineralization of diazinon using a statistical approach based on Box-Behnken design (BBD, one of response surface method) was investigated in an E-beam process, and also the main factors with diazinon concentration ($X_1$), irradiatin intensity ($X_2$) and pH ($X_3$) which consisted of 3 levels in each factor was set up to determine the effects of factors and optimization. At first, effects of pH and diazinon concentration were investigated to determine the proper range of application on response surface method(RSM). In statistical approach, the regression analysis and analysis of variance (ANOVA) were applied to evaluate the quantitative comparison of each factors in order to obtain the effects were irradiation intensity>diazinon concentration>pH. The regression model predicted the optimization point using the response optimizer to consider the effects of operation conditions were $Y_1=81.73-5.58X_1+23.69X_2-14.23X{_2}^2+4.22X{_3}^2(R^2=99.7%)$, $Y_2=35.23-3.01X_1+10.79X_2-7.58X_2{^2}(R^2=97.9%)$ and 95.7% of diazinon degradation, 41.8% of TOC reduction at 12.75mg/L and 4.26kGy, respectively. The pH condition was not significantly affects on E-beam process than other advanced oxidation processes (AOPs).