• Korean Journal of Materials Research
• /
• v.29 no.4
• /
• pp.241-251
• /
• 2019

There are several manufacturing techniques for developing thermionic cathodes for vacuum ultraviolet(VUV) ionizers. The triple alkaline earth metal emitters(Ca-Sr-Ba) are formulated as efficient and reliable thermo-electron sources with a great many different compositions for the ionizing devices. We prepare two basic suspensions with different compositions: calcium, strontium and barium. After evaluating the electron-emitting performance for europium, gadolinium, and yttrium-based cathodes mixed with these suspensions, we selected the yttrium for its better performance. Next, another transition metal indium and a lanthanide metal neodymium salt is introduced to two base emitters. These final composite metal emitters are coated on the tungsten filament and then activated to the oxide cathodes by an intentionally programmed calcination process under an ultra-high vacuum(${\sim}10^{-6}torr$). The performance of electron emission of the cathodes is characterized by their anode currents with respect to the addition of each element, In and Nd, and their concentration of cathodes. Compared to both the base cathodes, the electron emission performance of the cathodes containing indium and neodymium decreases. The anode current of the Nd cathode is more markedly degraded than that with In.

• Journal of Applied Biological Chemistry
• /
• v.63 no.4
• /
• pp.407-412
• /
• 2020

A simple and reliable HPLC method was developed to determine pharmacologically standard marker compounds of Ulmus parvifolia leaves. Standard markers were characterized with neochlorogenic acid (trans-5-O-caffeoylquinic acid, 5-CQA) and chlorogenic acid (trans-3-O-caffeoylquinic acid, 3-CQA) using NMR and UPLC-QTof-MS analysis. A method for qualitative/quantitative analysis of the leaves extracts were evaluated including two compounds by using HPLC. The stability test of 30% ethanolic extracts of the leaves sample and standard markers have been evaluated for six months. However, no significant changes in the content of the marker compounds of each extract was observed during the time of investigation.

• The Journal of the Korea institute of electronic communication sciences
• /
• v.16 no.1
• /
• pp.157-164
• /
• 2021

Wind and temperature were measured with a three-dimensional ultrasonic anemometer and the carbon dioxide concentration was measured using an infrared sensor in the tidal flat of Suncheon Bay. In general, as the temperature increases, the concentration of carbon dioxide increases, and as the temperature decreases, the carbon dioxide also decreases in the atmosphere. However, since photosynthesis declined immediately after the sunset, the concentration of carbon dioxide increased as the temperature decreased. In addition, near the high tide when the tidal flat is covered with seawater, the atmospheric turbulence was strong despite an increase in temperature, resulting in a decrease in carbon dioxide concentration. It is necessary to quantitatively evaluated the effects of photosynthesis, respiration and atmospheric turbulence on the change of carbon dioxide concentration over tidal flat ecosystems.

• Advances in nano research
• /
• v.10 no.2
• /
• pp.191-210
• /
• 2021

To compare the antifungal effect of two nanomaterials (NMs), nanoparticles of zinc oxide were synthesized by a chemical route and zinc oxide-based nanobiohybrids were obtained using green synthesis in an extract of garlic (Allium sativum). The techniques of X-Ray Diffraction (XRD), Infrared (IR) and Ultraviolet Visible (UV-Vis) absorption spectroscopies and Scanning (SEM) and Transmission Electron Microscopies (TEM) were used to determine the characteristics of the nanomaterials synthesized. The results showed that the samples obtained were of nanometric size (< 100 nm). To compare their antifungal capacity, their effect on Cercospora sp. was evaluated. Test results showed that both nanomaterials had an antifungal capacity. The nanobiohybrids (green route) gave an inhibition of fungal growth of ~72.4% while with the ZnO-NPs (chemical route), inhibition was ~87.1%. Microstructural studies using High Resolution Optical Microscopy (HROM) and ultra-structural analysis using TEM carried out on the treated strains demonstrated the effect of the nanofungicides on the vegetative and reproductive structures, as well as on their cell wall. To account for the antifungal effect presented by ZnO-NPs and ZnO nanobiohybrids on the fungi tested, effects reported in the literature related to the action of nanomaterials on biological entities were considered. Specifically, we discuss the electrical interaction of the ZnO-NPs with the cell membrane and the biomolecules (proteins) present in the fungi, taking into account the n-type nature of the ZnO semiconductor and the electrical behavior of the fungal cell membrane and that of the proteins that make up the protein crown.

• Journal of the Korea Convergence Society
• /
• v.13 no.4
• /
• pp.287-292
• /
• 2022

In this paper, the stochastic distribution of the springback amount is investigated for the stamping process of a U-channel shaped-product with ultra-high strength steel. Using the reliability-based design optimization technique (RBDO), stochastic distribution of process parameters is considered in the analysis including material properties and process variation. Quantification of the springback scatters is carried out with the statistical analysis method according to the material strength. It is found that the scattering amount of springback decreases while the amount of springback increases as the tensile strength of the blank material increases, which is investigated by analyzing the strain and stress distribution of the punch and die shoulder. It is noted that the proposed scheme is capable of predicting and responding to the unavoidable scattering of springback in the sheet metal forming process.

• Computers and Concrete
• /
• v.30 no.3
• /
• pp.175-183
• /
• 2022

To study the working mechanism and size effect of an innovative dovetail UHPC joint originated from the 5th Nanjing Yangtze River Bridge, a large-scale testing subject to negative bending moment was conducted and compared with the previous scaled specimens. The static responses, i.e., the crack pattern, failure mode, ductility and stiffness degradation were analyzed. It was found that the scaled specimens presented similar working stages and working mechanism with the large-scale ones. However, the post-cracking ductility and relative stiffness degradation all decrease with the enlarged length/scale, apart from the relative stiffness after flexural cracking. The slab stiffness at the flexural cracking stage is 90% of the initial stiffness while only 24% of the initial stiffness reserved in the ultimate stage. Finite element model (FEM) was established and compared with the experiments to verify its effectiveness in exploring the working mechanism of the innovative joint. Based on this effective method, a series of FEMs were established to further study the influence of material strength, pre-stressing level and ratio of reinforcement on its deflection-load relationship. It is found that the ratio of reinforcement can significantly improve its load-carrying capacity among the three major-influenced factors.

• Journal of Advanced Navigation Technology
• /
• v.26 no.5
• /
• pp.358-364
• /
• 2022

The Inter Communication System for avionics is in charge of processing all voice signals that internal calls between Pilot and Co-pilot, internal calls between Pilots and Crews, external calls through communication equipment such as Ultra/Very High Frequency Receiver/Transmitter(U/VHF RT), audio signal monitoring for navigation and mission equipment such as VHF Omnidirectional Range/Instrument Landing System(VOR/ILS), Tactical Air Navigation(TACAN), audio signal output for voice recording to Flight Data Recorder(FDR) and Data Transfer System(DTS), and warning/caution audio signal generate about the status and threat of aircraft. Because Inter Communication System for avionics is sensitive to noise in the case of analog audio signals, a redundant design that can protect audio signal from electromagnetic noise inside/outside of aircraft is required for the mission of pilots and crews. In this paper, Normal/Back-up operation mode and redundancy design plan based on digital method for the redundancy of the digital Inter Communication System for avionics and manufacturing, verification results are described.

• Geomechanics and Engineering
• /
• v.29 no.2
• /
• pp.113-131
• /
• 2022

A rockburst is a common disaster in deep-tunnel excavation engineering, especially for high-geostress areas. An anomalously low friction effect is one of the most important inducements of rockbursts. To elucidate the correlation between an anomalously low friction effect and a rockburst, we establish a two-dimensional prediction model that considers the discontinuous structure of a rock mass. The degree of freedom of the rotation angle is introduced, thus the motion equations of the blocks under the influence of a transient disturbing force are acquired according to the interactions of the blocks. Based on the two-dimensional discontinuous block model of deep rock mass, a rockburst prediction model is established, and the initiation process of ultra-low friction rockburst is analyzed. In addition, the intensity of a rockburst, including the location, depth, area, and velocity of ejection fragments, can be determined quantitatively using the proposed prediction model. Then, through a specific example, the effects of geomechanical parameters such as the different principal stress ratios, the material properties, a dip of principal stress on the occurrence form and range of rockburst are analyzed. The results indicate that under dynamic disturbance, stress variation on the structural surface in a deep rock mass may directly give rise to a rockburst. The formation of rockburst is characterized by three stages: the appearance of cracks that result from the tension or compression failure of the deformation block, the transformation of strain energy of rock blocks to kinetic energy, and the ejection of some of the free blocks from the surrounding rock mass. Finally, the two-dimensional rockburst prediction model is applied to the construction drainage tunnel project of Jinping II hydropower station. Through the comparison with the field measured rockburst data and UDEC simulation results, it shows that the model in this paper is in good agreement with the actual working conditions, which verifies the accuracy of the model in this paper.

• Structural Engineering and Mechanics
• /
• v.81 no.3
• /
• pp.305-316
• /
• 2022

Externally bonded ultrahigh performance fiber-reinforced concrete (UHPFRC) is commonly used as a strengthening material for reinforced concrete (RC) structures. This study reports the results of an experimental program investigating the bonding behavior between concrete and prefabricated UHPFRC plates. The overall experimental program is consisting of five RC specimens, which are strengthened using the different lengths and widths of prefabricated UHPFRC plates. These specimens were analyzed using the pull-pull double-shear test. The performance of each strengthened specimen is presented, discussed and compared in terms of failure mode, maximum load, load-slip relationship, fracture energy and strain distribution. Specimen C-25-160-300 which bonded along the whole width of 160 mm recorded the highest maximum load (109.2 kN) among all the analysed specimens. Moreover, a 3D numerical finite element model (FEM) is proposed to simulate the bond behavior between concrete and UHPFRC plates. Moreover, this study reviews the analytical models that can predict the relationship between the maximum bond stress and slip for strengthened concrete elements. The proposed FEM is verified against the experimental program and then used to test 36 RC specimens strengthened with prefabricated UHPFRC plates with different concrete grades and UHPFRC plate widths. The obtained results together with the review of analytical models helped in the formation of a design equation for estimating the bond stress between concrete and prefabricated UHPFRC plates.

• Analytical Science and Technology
• /
• v.34 no.4
• /
• pp.160-171
• /
• 2021

Synthetic azo dyes are used extensively in herbal medicines to render the medicines more visually attractive to consumers. This study developed and validated a rapid high-performance liquid chromatography (HPLC) method to determine whether synthetic colorants such as Tartrazine, Auramine O, Metanil yellow, Sunset yellow, and Orange II are used extensively in Typha orientalis. To increase the recovery of the synthetic dyes, this method employed containing 50 mM ammonium acetate in 70 % methanol at first extraction and 100 mM HCl in 70 % methanol at second extraction. Five synthetic pigments in Typha orientalis were separated by gradient elution with a mobile phase consisting of acetonitrile and 50 mM ammonium acetate in distilled water at ultra-violet (UV) detection 428 nm or 500 nm. Additionally, this study established the liquid chromatography tandem mass spectrometry (LC-MS/MS) method to confirm positive samples suspected by HPLC results. The HPLC-UV method had good linearity, indicating r²> 0.999. The recoveries of the samples spiked with three different concentration ranged from 73.8~91.5 %, and relative standard deviation values indicated 0.2~5.2 %. The established LC-MS/MS could successfully identify the synthetic pigments in herbal medicine samples. The study demonstrates that Typha orientalis adulterated by yellowish synthetic dyes can be successfully distinguished when using the HPLC-UV method.