• Transactions of the Korean Society of Mechanical Engineers
• /
• v.14 no.1
• /
• pp.157-171
• /
• 1990

The heat transfer problem associated with pulse technique for measuring thermal diffusivity was solved by means of Green function. The obtained general solution was discussed so as to apply for all possible cases; kinds of boundary condition and heat source, irradiation positions of heat pulse, radius of heat pulse, one-and two-dimensional heat flow, finite pulse time effects and radiation heat loss systems. Experimentally, the laser flash lamp was used as heat source for measuring thermal diffusivity of low carbon, aluminium chilled steel plate, which was heavily rolled in order to measure the variation of thermal diffusivity in the temperature range from room temperature through 500.deg. C. The derived results are (1) materials produced from same furnace showed a somewhat different thermal diffusivity values. (2) the thermal diffusivity value of rolled material was smaller than unrolled material and the difference decreased as increasing temperature. (3) the thermal diffusivity value of an annealed and temper rolled material was larger than the value of a cold rolled material, even thought smaller than unrolled material. (4) In case of heavy rolled material, there was no consistent relationships between the thermal diffusivity and the reduction in thickness.

• Transactions of the Korean Society of Mechanical Engineers B
• /
• v.22 no.8
• /
• pp.1073-1082
• /
• 1998

When thermal diffusivity is measured by laser flash method, the thermal diffusivity call be calculated front the assumption of the uniformly heated whole surface of the specimen. It has been known that the approximate 5% error is made by the non-uniform energy distribution on the specimen surface of laser pulse heat source. In this study, to obtain the highly-uniformed laser beam, which has both the low non-uniform heating error from non-uniform laser beam and the energy loss, research was carried out on no transmitting loss by optical fiber and high repetitions. In addition, heating error and thermal diffusivity were measured as the measuring positions were varied and compared with the results using the uniform and the non-uniform laser beams. In addition, dole to using the uniformalized laser beam, the whole surface of the specimen was heated uniformly and as a result, it was the thought that this was very effective to reduce the variations of the errors of the thermal diffusivity as the measuring positions were varied. It can be obtained that when the thermal diffusivity of POCO-AXM-5Q1 of SRM in NBS was measured with both the uniform and the non-uniform laser beams, the dispersion error of the former was from 2 to 2.5%, which was more improved than that of the latter.

• Transactions of the Korean Society of Mechanical Engineers B
• /
• v.27 no.9
• /
• pp.1220-1228
• /
• 2003

The mirage technique is proved to be powerful in measuring the thermal diffusivity of materials. In particular, its contactless nature makes it suitable for delicate samples and microscale structures. In this study, thermal-wave-coupling method is developed in a general form for both thermally thin and thick samples. In the suggested measuring scheme, the probe beam can be positioned close to the pump beam and the absolute position need not be measured. Therefore the new scheme provides a relatively simple yet effective way to determine the thermal diffusivity of thermally thick samples. Thermal diffusivities of bulk samples like Ni and Al were measured and the characteristics of mirage signal for a thin film were observed by using the mirage experimental setup. The apparent thermal diffusivity was measured by varying such parameters as probe beam height, size of pump beam, power of pump beam, and surface condition of sample. From the practical standpoint, it is shown that the size of the pump beam is the most important factor for accurate thermaldiffusivity measurement. Experiments using thin-film samples show that the thermal diffusivity of a substrate covered with thin film can be measured by photothermal mirage signals.

• Proceedings of the KSME Conference
• /
• 2003.04a
• /
• pp.1395-1400
• /
• 2003

This paper introduces a novel scheme for determining the thermal diffusivity of solids using the photothermal mirage technique. The suggested scheme extends the thermal-wave coupling method, employing the solution to the heat conduction equation in close proximity to the pump beam. Therefore, determination of thermal diffusivity is possible by detecting the mirage signal with small separation between the probe and pump beams, with enhanced intensity of the mirage signal. Though the method requires information about the probe-beam height, the absolute transverse position of the probe beam need not be known as it is automatically evaluated by the iterative-computation procedure. The thermal diffusivity of Ni is measured by the proposed scheme and the result demonstrates good agreement with the literature value to within 5 %.

• Transactions of the Korean Society of Mechanical Engineers B
• /
• v.26 no.12
• /
• pp.1747-1755
• /
• 2002

A complete theoretical treatment of the photothermal displacement technique has been performed for thermal diffusivity measurement in semi-infinite solid materials. The influence of the parameters, such as radius and modulation frequency of the heating beam and the thermal diffusivity, was studied. Usually, thermal diffusivity was determined by the deformation angle and phase angle as the relative position between the heating and probe beams. In this study, we proposed the simple analysis method based on the real part of deformation gradient as the relative position between two beams. It is independent in the parameters such as power of heating beam, absorption coefficient, reflectivity, Poisson's ratio, and thermal expansion coefficient.

• Journal of Mechanical Science and Technology
• /
• v.18 no.10
• /
• pp.1712-1721
• /
• 2004

A method of measuring the thermal diffusivity of semi-infinite solid material at room temperature using photothermal displacement is proposed. In previous works, within the constant thickness of material, the thermal diffusivity was determined by the magnitude and phase of deformation gradient as the relative position between the pump and probe beams. In this study, however, a complete theoretical treatment of the photothermal displacement technique has been performed for thermal diffusivity measurement in semi-infinite solid materials. The influence of parameters, such as, radius and modulation frequency of the pump beam and the thermal diffusivity, was studied. We propose a simple analysis method based on the zero -crossing position of real part of deformation gradient and the minimum position of phase as the relative position between two beams. It is independent of parameters such as power of pump beam, absorption coefficient, reflectivity, Poisson's ratio, and thermal expansion coefficient.

• Korean Journal of Materials Research
• /
• v.30 no.9
• /
• pp.474-479
• /
• 2020

The effect of precipitation and dissolution of Si on the thermal diffusivity in the Al-Si alloy system is reported in this study and solution heat treatment followed by aging treatment is carried out to determine the effects of heat treatment on the thermal characteristics. The solution treatment is performed at 535 ℃ for 4 and 10 h and then the specimens are cooled by rapid quenching. The samples are aged at 300 ℃ for 4 h to precipitate Si solute. The addition of 9 wt% silicon contents makes the thermal diffusivity decrease from 78 to 74 mm/s² in the cases of solid solution treated and quenched samples. After quenching and aging, the Si solute precipitates on the Al matrix and increases the thermal diffusivity compared with that after the quenched state. In particular, the increase of the thermal diffusivity is equal to 10 mm/s² without relation to the Si contents in the Al-Si alloy, which seems to corresponded to solute amount of Si 1 wt% in the Al matrix.

• Korean Journal of Materials Research
• /
• v.30 no.8
• /
• pp.435-440
• /
• 2020

The relationship between the precipitation of secondary phase and the thermal properties of Al-4.5%Cu alloy (in wt.%) after various heat treatments has been studied. Solid solution treatment of alloy was performed at 808 K for 6 hours, followed by warm water quenching; then, the samples were aged in air at 473 K for different times. The thermal diffusivity of the Al-4.5%Cu alloy changed with the heat treatment conditions of the alloy at temperatures below 523 K. The as-quenched specimen had the lowest thermal diffusivity, and as the artificial aging time increased, the thermal diffusivity of the specimen increased in the temperature range between 298 and 523 K. For the specimen aged for five hours, the thermal conductivity was 12% higher than that of the as-quenched specimens at 298 K. It is confirmed that the thermal diffusivity and thermal conductivity of the Al-4.5%Cu alloy significantly depend on their thermal history at temperatures below 523 K. The precipitation and dissolution of the Al₂Cu phase were confirmed via DSC for the alloys, and the formation of coefficient of thermal expansion peaks in TMA was caused by precipitation. The precipitation of supersaturated solid solution of Al-4.5%Cu alloys had an additional linear expansion of ≈ 0.05 % at 643 K during thermal expansion measurement.

• Journal of the Korean Society of Safety
• /
• v.22 no.4
• /
• pp.13-19
• /
• 2007

An numerical method to estimate thermal diffusivity has been developed for one-dimensional unsteady heat conduction problem, when the temperatures are know at two positions in a semi-infinite body. Using the closed form solution which has already derived an explicit solution for the inverse problem for one-dimensional transient heat conduction using Laplace transform technique, we first estimate the surface temperature. The thermal diffusivity can be estimated by using the estimated surface temperature and measured temperatures, which include some uncertainties. The estimated surface heat flux and thermal diffusivity are found to be in good agreement with those of the experimented conditions. This method will be extended to the simultaneous measurement of thermal diffusivity and thermal conductivity.

• Journal of the Korean Ceramic Society
• /
• v.22 no.4
• /
• pp.40-46
• /
• 1985

Thermal diffusivities of zirconia samples partially or fully stabilized by MgO and $Y_2O_3$ were measured b laser-flash method up to 140$0^{\circ}C$ The values of thermal diffusivity decreased as the contents of MgO and $Y_2O_3$ increased due to the phonon scattering effect of defect structure of cubic phase formed. The temperature dependence of thermal diffusivity showed that the thermal diffusivity values decreased due to phono-phonon scattering as the temperature increased. The difference in thermal diffusivity was observed on cooling after heating up to 140$0^{\circ}C$ for magnesia stabi-lized zirconia samples but not for yttria stabilized zirconia samples.