• Title/Summary/Keyword: Spray treatment

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Preparation of Green-Light Emitting BAM:Mn Phosphor Particles by High Temperature Spray Pyrolysis (고온 분무열분해 공정에 의한 녹색 발광의 BAM:Mn 형광체 합성)

  • Ju Seo Hee;Koo Hye Young;Kim Do Youp;Kang Yun Chan
    • Korean Journal of Materials Research
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    • v.15 no.8
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    • pp.496-502
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    • 2005
  • Green-light emitting $BaMgAl_{10}O_{19}:Mn^{2+}$ (BAM:Mn) phosphor particles were prepared by spray Pyrolysis. The effect of reactor temperature and flow rate of carrier gas in the spray Pyrolysis on the morphology, crystallinity and photoluminescence characteristics under vacuum ultraviolet were investigated. The morphology of the as-Prepared Particles obtained by spray Pyrolysis had spherical shape and non-aggregation characteristics regardless of the reactor temperature. The spherical shape of the as-prepared Particles obtained by spray pyrolysis at low temperature disappeared after Post-treatment. On the other hand the as-Prepared Particles obtained by spray Pyrolysis at $1600^{\circ}C$ maintained spherical shape and non-aggregation characteristics after post-treatment at $1400^{\circ}C$ for 3 h under reducing atmosphere. The BAM:Mn Phosphor Particles Prepared by spray Pyrolysis at different reactor temperatures had pure crystal structure and high photoluminescence intensities under vacuum ultraviolet after post-treatment. BAM:Mn phosphor particles prepared by spray Pyrolysis at low How rate of carrier gas had complete spherical shape and filed morphology and high photoluminescence intensity after post-treatment under reducing atmosphere.

The Characteristics of Nano-sized Cobalt Oxide Particles Prepared by Low Pressure Spray Pyrolysis (저압 분무열분해법에 의해 합성된 나노 크기의 코발트 산화물 입자의 특성)

  • Ju, Seo-Hee;Kim, Do-Youp;Kang, Yun-Chan
    • Korean Journal of Materials Research
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    • v.16 no.9
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    • pp.538-542
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    • 2006
  • Nano-sized cobalt oxide powders were prepared by low pressure spray pyrolysis process. The precursor powders obtained by low pressure spray pyrolysis process from the spray solution with ethylene glycol had several microns size and hollow structure. The precursor powders obtained from the spray solution with optimum concentration of ethylene glycol formed the nano-sized cobalt oxide powders with regular morphology after post-treatment without milling process. On the other hand, the cobalt oxide powders obtained from the spray solution without ethylene glycol had submicron size and spherical shape before and after posttreatment. The mean size of the cobalt oxide powders formed from the spray solution with concentration of ethylene glycol of 0.7M was 180 nm after post-treatment at temperature of $800^{\circ}C$. The mean size of the powders could be controlled from several tens nanometer to micron sizes by changing the post-treatment temperatures in the preparation of cobalt oxide powders by low pressure spray pyrolysis process.

Synthesis and Properties of ITO Nano Powders by Spray Drying Process (분무건조법에 의한 ITO 나노분말의 합성과 특성)

  • 허민선;최철진;권대환
    • Journal of Powder Materials
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    • v.11 no.1
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    • pp.22-27
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    • 2004
  • The Indium Tin Oxide(ITO) nano powders were prepared by spray drying and heat treatment process. The liquid solution dissolved Indium and Tin salts was first spray dried to prepare chemically homogeneous recursor powders at the optimum spray drying conditions. Subsequently, the precursor powders were subjected to eat treatment process. The nano size ITO powders was synthesized from the previous precursor powders and the npuities also were decreased with increasing heat treatment temperature. Furthermore, the lattice parameter of TO nano powders was increased by doping Tin into Indium with increasing heat treatment temperature. The par icle size of the resultant ITO powders was about 20∼50nm and chemical composition was composed of In:Sn =86:10 wt.% at 80$0^{\circ}C$.

A Study on Surface Characteristics of High Tensile Brass with Molybdenum Flame Spray Treatment (고력황동의 몰리브덴 화염용사에 따른 표면 특성에 관한 연구)

  • Jung, Dong-Hyun;Kim, Hae-Ji
    • Journal of the Korean Society of Manufacturing Process Engineers
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    • v.17 no.6
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    • pp.38-45
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    • 2018
  • Molybdenum flame spray coatings are widely used in industrial fields to enhance the performance of mechanical component parts such as pistons, shafts and clutches. This study investigates the surface characteristics of high tensile brass with molybdenum flame spray treatment using the clutch material for small ship. The surface characteristics after molybdenum flame spray treatment in high tensile brass were quantitatively analyzed for surface composition, coating layer thickness, friction coefficient, abrasion width and phenomenon, micro-hardness, and surface roughness.

An Experimental Study on the Permeability Evaluation of Metal Spray System by Metal Spray Coating Surface Treatment (콘크리트 표면처리방법에 따른 금속용사 피막의 투수성 평가에 관한 실험적 연구)

  • Park, Jin-Ho;Jang, Hyun-O;Lee, Han-Seung
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2016.10a
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    • pp.50-51
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    • 2016
  • Ozone is a strong oxidizing materials in the advanced water treatment facilities. However, due to such a strong oxidation, Ozone eroded waterproofing/corrosion on the concrete surface and caused performance degradation. Therefore, in this study, permeability experiment of metal spraying system by concrete surface treatment was conducted.

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Effect of an temperatures of post-spray heat treatment on wear behavior of $8%Y_2O_3-ZrO_2$ coating

  • Chae, Y.H.;Kim, S.S.
    • Proceedings of the Korean Society of Tribologists and Lubrication Engineers Conference
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    • 2002.10b
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    • pp.181-182
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    • 2002
  • Most recent, Plasma ceramic spray is used on parts of tribosystem, has been investigated on the tribological performance. The application of ceramic coatings by plasma spray has become essential in tribosystems to produce better wear resistance and longer life in various conditions. The purpose of this work was to investigate the wear behavior of $8%Y_2O_3-ZrO_2$ coating due to temperatures of post-spay heat treatment. The plasma-sprayed $8%Y_2O_3--Zirconia$ coating was idiscussed to know the relationship between phase transformations and temperatures of post- spray heat treatment. Wear tests was carried out with ball on disk type on normal load of 50N, 70N and 90N under room temperature. The transformation of phase and the value of residual stress were measured by X-ray diffraction method(XRD). Tribological characteristics and wear mechanisms of coatings was observed by SEM. The tribologieal wear performance was discussed a point of view for residual stress. Consequently. post-spray heat treatment plays an important role in decreasing residual stress. Residual stress in coating system has a significant influence on the wear mechanism of coating.

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Sliding Wear Characteristics of plasma Sprayed $8\%Y_{2}O_3-ZrO_2$ Coating for Post-spray Heat Treatment

  • Chae Young-Hun;Kim Seock-Sam
    • KSTLE International Journal
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    • v.6 no.2
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    • pp.45-50
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    • 2005
  • Plasma ceramic spray that is applied on a machine part under severe work conditions has been investigated for tribological behavior. The application of ceramic coatings by plasma spray has become essential in tribosystems to produce wear resistance and long life in severe conditions. The purpose of this study was to investigate the wear characteristics of $8\%Y_{2}O_3-ZrO_2$ coating, in view of the effect of post-spay heat treatment. The plasma-sprayed $8\%Y_{2}O_3-ZrO_2$ coating was studied to know the relationship between phase transformations and wear behavior related to post-spray heat treatment. Wear test was carried out with ball on disk type on normal loads of 50N,70N and 90N under room temperature. The phase transformation of phase and the value of residual stress were measured by X-ray diffraction method(XRD). Tribological characteristics and wear mechanisms of coatings were observed by SEM. The tribological wear performance was discussed in the focusing of residual stress. Consequently, post-spray heat treatment plays an important role in decreasing residual stress. Residual stress in the coating system has a significant influence on the wear mechanism of coating.

Development of Alginate-based Spray-type Hydrogel and Evaluation of Technical Compatibility for Container Application (알지네이트 기반 분사형 하이드로겔 개발 및 용기 적용에 대한 기술적합성 평가)

  • Yong Joon, Joo;Hee Kyung, Jeon;Jeong Yeon, Choi;Gyeong Sik, Hong
    • Journal of Biomedical Engineering Research
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    • v.44 no.1
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    • pp.64-72
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    • 2023
  • Initial burn wound care is one of the important factors in the outcome of burn treatment. In this study, we tried to develop spray-type alginate hydrogel dressing with advantages such as promoting wound healing, reducing pain, and increasing ease of use for emergency burn treatment. Spray implementation, physical properties, and cytotoxicity of the newly developed spray-type alginate hydrogel dressing were evaluated. As a result, a new functional spray-type hydrogel dressing with excellent physical properties and biocompatibility was developed along with the development of spray able containers, and it was confirmed that it could be applied as a treatment for skin regeneration in the future.

Evaluation of Plasma Spray Hydroxy Apatite coatings on Metallic Materials

  • Take, S.;Mitsui, K.;Kasahara, M.;Sawai, R.;Izawa, S.;Nakayama, M.;Itoi, Y.
    • Corrosion Science and Technology
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    • v.6 no.6
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    • pp.286-290
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    • 2007
  • Biocompatible Hydroxy apatite (HAp) coatings on metallic substrate by plasma spray techniques have been developed. Long-term credibility of plasma spray HAp coatings has been evaluated in physiological saline by electrochemical measurements. It was found that the corrosion resisitance of SUS316L based HAp/Ti conbined coatings was excellent even after more than 10 weeks long-term immersion. It was shown that postal heat treatment improved both the crystallinity and corrosion resistance of HAp. By lowering cooling rate during heat treatment process, less cracks produced in HAp coating layer, which lead to higher credibility of HAp during immersion in physiological saline. The ICP results showed that the dissolution level of substrate metallic ions was low and HAp coatings produced in this research can be acceptable as biocompatible materials. Also, the concentration of dissolved ions from HAp coatings with postal heat treatment was lower compared to those from samples without postal heat treatment. The adherence of HAp coatings with Ti substrate and other mechanical properties were also assessed by three-point bending test. The poor adhesion of HAp coating to titanium substrate can be improved by introducing a plasma spray titanium intermediate layer.

Recent Study of Thermal Spray for Green Automotive Industry (친환경 자동차산업의 용사(Thermal spray)에 대한 최신 연구동향)

  • Yoo, Ho-Cheon
    • Journal of Welding and Joining
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    • v.32 no.3
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    • pp.43-52
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    • 2014
  • Recent developing tendency of thermal spray for green automotive industry are studied by searching of NDSL, KIPRIS, ScienceDirect and so on. Spraying techniques such as plasma spray, microwave treatment, dry-ice blasting, HVOF thermal spray, cold spraying, aerosol deposition are introduced, further more spraying materials such as nano particles, intermetallic compound, TiAlN, TiC, Si-Al alloys are investigated.