• 한국전기전자재료학회논문지
• /
• 제32권6호
• /
• pp.516-521
• /
• 2019

The top seeded solution growth (TSSG) method is an alternative technique to grow high-quality SiC crystals that has been actively studied for the last two decades. However, the TSSG method has different issues that need to be resolved when compared to the commercial SiC crystal growing method, i.e., physical vapor transport (PVT). A particular issue of the TSSG method of results from the presence of liquid droplets on the grown crystal that can remain even after crystal growth; this induces residual stress on the crystal surface. Hence, the residual droplet causes several unwanted effects on the crystal such as the initiation of micro-cracks, micro-pipes, and polytype inclusions. Therefore, this study investigated the formation of the residual droplet through multiphysics simulations and lead to the development of a liquid droplet removal method. As a result, we found that although residual liquid droplets significantly apply residual stress on the grown crystal, these could be vaporized by adopting thermal annealing processes after the relevant crystal growing steps.

• 한국전기전자재료학회논문지
• /
• 제21권7호
• /
• pp.599-602
• /
• 2008

Growth of well-aligned ZnO nanostructures on various substrates such as GaN, ITO/glass, and sapphire was realized via a simple aqueous solution method at low temperature of $90^{\circ}C$. Morphology of ZnO nanostructures grown on various substrates as function of substrate was studied. It was found that ZnO nanostructures is a strong function of substrate. It was clearly observed that the morphology of ZnO nanostructures could be varied by change of substrate. Morphology, crystallinity, and crystal characteristics were carried out by FE-SEM, synchrotron x-ray scattering measurements, and high-resolution electron microscopy, respectively.

• 한국결정성장학회:학술대회논문집
• /
• 한국결정성장학회 2000년도 Proceedings of 2000 International Nano Crystals/Ceramics Forum and International Symposium on Intermaterials
• /
• pp.243-248
• /
• 2000

Effect of NiO addition on microstructure, stability of tetragonal phase and mechanical properties was investigated. (Y, Ni)-TZP solid solution was obtained by pressureless sintering. The fracture toughness was increased by solid solution of NiO. Neither reaction phase nor glassy phase was observed at the grain boundaries. From these results, it was determined that solid solution of NiO was destabilized tetragonal phase of Y-TZP. Y-TZP/Ni nanocomposite that contained nano-sized Ni particles was also fabricated by internal reduction method. Some evaluations and discussions were carried out for both (Y, Ni)-TZP solid solution and Y-TZP/Ni nanocomposite.

• 한국안전학회지
• /
• 제21권1호
• /
• pp.15-20
• /
• 2006

The finite element alternating method is a convenient and efficient method to analyze three-dimensional cracks embedded in an infinite or a finite body because the method has the property that the uncracked body and cracks can be modeled independently. In this paper the method was applied for fatigue crack growth simulation. A surface crack in a cylinder was considered as an initial crack and the crack configurations and stress intensity factors during the crack growth were obtained. In this paper the finite element alternating method proposed by Nikishkov, Park and Atluri was used after modification. In the method, as the required solution for a crack in an infinite body, the symmetric Galerkin boundary element method formulated by Li and Mear was used. And a crack was modeled as distribution of displacement discontinuities, and the governing equation was formulated as singularity-reduced integral equations.

• 한국전기전자재료학회논문지
• /
• 제22권11호
• /
• pp.987-991
• /
• 2009

We report growth of vertically well-aligned zinc oxide (ZnO) nanorods on indium-tin oxide (ITO)/glass substrates using a simple aqueous solution method at low temperature via control of the ZnO seed layer morphology. ZnO nanoparticles acting as seeds are pre-coated on ITO-coated glass substrates. by spin coating to control distribution and density of the ZnO seed nanoparticles. ZnO nanorods were synthesized on the seed-coated substrates in a dipping process into a main growth solution. It was found that the alignment of ZnO nanorods can be effectively manipulated by the spin-coating speed of the seed layer. A grazing incidence X-ray diffraction pattern shows that the ZnO seed layer prepared using the higher spin-coating speed is of uniform seed distribution and a flat surface, resulting in the vertical growth of ZnO nanorods aligned toward the [0001] direction in the main growth process.

• 한국세라믹학회지
• /
• 제46권6호
• /
• pp.596-601
• /
• 2009

Double-layered ZnO nanostructures have been synthesized by aqueous solution method on (001) plane of ZnO nanorod. A stepwise changing of aqueous solution concentration gave rise to a new nano-structured layer consisting of either multiple of nanorods or nanowires with much smaller radii than that of the ZnO nanorod on which the new layer was grown. As the first step the ZnO nanorods have been grown to have the (001) preferential orientation in the aqueous solution consisting of 0.1M zinc nitrate and 0.1 M HMT. This preferentially aligned ZnO nanorods have been regrown in either a less diluted solution of 0.01M zinc nitrate and 0.01 M HMT or a more diluted solution of 0.005M zinc nitrate and 0.01 M HMT. A new nano-layer consisting of numerous aligned nanorods or nanowires has been produced on the (001) planes of ZnO nanorods. The growth mechanism for this double layered ZnO nanostructure is ascribed to the (001) polar surface energy instability and inhibition of (001) plane growth due to the step-wise change of aqueous solution concentration; ZnO nuclei formed on the (001) plane grow preferentially in (010) plane instead of (001) plane to reduce the total surface energy. Surface area of ZnO nanostructure can be increased in orders of magnitudes by forming a new layer consisting of smaller nanorods/nanowires on (001) plane of ZnO nanorods.

• 대한기계학회논문집
• /
• 제6권4호
• /
• pp.377-383
• /
• 1982

Acoustic emission (AE) of a high strength steel (SCM-4) was measured under stress corrosion cracking(SCC) test at a constant displacement in 3.5% artificial NaCl solution of 18.deg.C, 45.deg.C and 60.deg.C, respectively. The results are as follows; During the SCC test, AE is detected and AE count rate is approximately proportional to the crack growth rate. Even though crack is not propagated macroscopically, AE is detected. The crack growth rate of SCC and the AE count rate are higher for the solution of higher temperature, 45.deg.C and 60.deg.C, than for the solution of lower temperature, 18.deg.C. In the early stage of SCC, AE total counts mostly depend on crack growth. In the later stage, however, AE mostly depends on the film fracture and the dissolution of anode.

• Korean Journal of Mathematics
• /
• 제18권3호
• /
• pp.277-288
• /
• 2010

We consider the nonlinear biharmonic equation with coefficient exponential growth term and Dirichlet boundary condition. We show that the nonlinear equation has at least one bounded solution under the suitable conditions. We obtain this result by the variational method, generalized mountain pass theorem and the critical point theory of the associated functional.

• 생물환경조절학회지
• /
• 제10권2호
• /
• pp.101-105
• /
• 2001

팽연화왕겨 배지는 펄라이트와 수분특성이 달라서 펄라이트는 과채류 재배용 스티로폼베드에서 재배할 경우 1일 1.5~2.0L씩의 급액량을 1일 16회로 분할하여 급액한 처리에서 가장 좋은 생육을 보였으나 팽연화왕겨는 1일 16~24회로 분할 급액할 경우 높은 수량성을 보였다. 또한 토마토 재배시 정식 후 25일간 급액 EC를 높여줌으로써 우수한 생육 및 수량을 얻을 수 있었으며 초기 부숙이 급속히 진행되는 과정에서 발생되는 NO$_3$의 부족을 보완할 수 있을 것으로 판단된다.

• Journal of Microbiology and Biotechnology
• /
• 제9권5호
• /
• pp.554-561
• /
• 1999

A novel estimation method was investigated for determining the concentrations of residual biomass, poly-3-hydroxybutyrate (PHB), and main nutrients including carbon and nitrogen sources, phosphate, and mineral ions from the supplied amount of ammonia solution used for a pH-control solution and nitrogen source in a PHB fermentation. The estimation equations for a batch culture and a fed-batch culture were derived from the relationship between the growth rate of residual biomass and the feed rate of the pH-control solution, and then were applied to the batch culture and the fed-batch cultures of Alcaligenes latus. This method was successfully applied to estimate the concentrations of residual biomass, PHB, and nutrients.