• Title/Summary/Keyword: Slurries

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Physical Properties of Microencapsulated Phase Change Material Slurries (미립잠열슬러리의 물성에 관한 실험적 연구)

  • 이효진;홍재창;이재구
    • Korean Journal of Air-Conditioning and Refrigeration Engineering
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    • v.12 no.9
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    • pp.860-869
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    • 2000
  • The thermal conductivity and density of slurries entrained with the particles of Micro-PCM are measured with respect to its temperatures as well as concentrations. For the thermal conductivity of slurries, a device made from P.A. Hilton (Model No. H470) is adopted. There is a well-scaled 0.3 mm gap between shells into which the slurry is injected. The temperatures of the slurry are changed to $5~25^{\circ}C$ , for which it is controled by the supplied voltage and cooling water circulated around the outer shell. The concentrations of Micro-PCM slurries are varied from 5 wt% to 50 wt%. Some general equations such as Maxwell's equation, are evaluated for their applicability with Micro-PCM slurry. As a result, it happens to be some 20% discrepancy between the experiment and the applied equations. The density measurements of Micro-PCM slurry to its temperature and concentration are peformed by hydrometer. For the experiment, tetradecane encapsulated slurry (($t_m≒6^{\circ}C$) and a mixed wax ($t_m≒50^{\circ}C$) are tested. The temperature changes of tetradecane are applied for $0^{\circ}C\;to\;$20^{\circ}C$and a mixed wax for $20^{\circ}C\;to\;$60^{\circ}C$ and its concentrations are changed from 5 wt% to 30 wt%. The results are compared with a general equation and the referenced data. For the conclusion, the experimental result and a general equation are well agreed.

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Use of Ultra Fine Cement Particles as Crack Repair Materials (균열주입재로서 초미립자 시멘트의 이용)

  • 이종열;정연식;이웅종;양승규;채재홍
    • Proceedings of the Korea Concrete Institute Conference
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    • 2000.10b
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    • pp.1205-1210
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    • 2000
  • In this research we made the mean cement particle size 4 $\mu\textrm{m}$ which can penetrate even minor cracks based on the theory of J.K. Michel who reported particles can penetrate the crack of width up to 3 times of maximum particle size. The cement slurries were produced by adding super plasticizer. The slurries were tested with slurry characterization methods and its rheological properties were characterized. The early hydrated phenomena of ultra fine cement were observed by SEM, XRD and DSC during 24 hours. Mechanical properties of hardened slurry with JIS molds were also tested in 3, 7 and 28 days. The cracked specimens which were repaired with slurries produced various conditions were tested after 3, 7 and 28 days curing in the air and adhesion properties were characterized.

Optimization of Removal Rates with Guaranteed Dispersion Stability in Copper CMP Slurry

  • Kim Tae-Gun;Kim Nam-Hoon;Kim Sang-Yong;Chang Eui-Goo
    • Transactions on Electrical and Electronic Materials
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    • v.5 no.6
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    • pp.233-236
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    • 2004
  • Copper metallization has been used in high-speed logic ULSI devices instead of the conventional aluminum alloy metallization. One of the key issues in copper CMP is the development of slurries that can provide high removal rates. In this study, the effects of slurry chemicals and pH for slurry dispersion stability on Cu CMP process characteristics have been performed. The experiments of copper slurries containing each different alumina and colloidal silica particles were evaluated for their selectivity of copper to TaN and $SiO_{2}$ films. Furthermore, the stability of copper slurries and pH are important parameters in many industries due to problems that can arise as a result of particle settling. So, it was also observed about several variables with various pH.

Preparation of Ceria Coated Silica Abrasive by Hydrothermal Treatment and Polishing Rate on Oxide Film (수열처리에 의한 세리아가 코팅된 실리카 연마재의 제조 및 Oxide Film의 연마특성)

  • Ryu Dae Sun;Kim Dae Sung;Lee Seung-Ho
    • Korean Journal of Materials Research
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    • v.15 no.12
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    • pp.818-823
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    • 2005
  • Sub-micron colloidal silica particles coated with nano-sized ceria were prepared by mixing of its silica and cerium salts hydrolysis, and modified by hydrothermal reaction. By using the slurries with and without hydrothermal modification containing above particles, oxide film coated on silicon wafer was polished. The modified slurries had higher polish rate due to increase of ceria fraction to silica through hydrothermal reaction. They revealed higher stability in wide range of pH $2\~10$ than ceria coated silica slurries without its modification.

Adsorption and Oxidation Reaction Rate of $SO_2$ in Slurries of Activated Carbon (활성탄 슬러리를 이용한 $SO_2$ 가스의 흡착 및 산화반응 속도)

  • 최용택;신창섭;이태희
    • Journal of Korean Society for Atmospheric Environment
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    • v.3 no.1
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    • pp.41-46
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    • 1987
  • Adsorption and reaction studies were made for the catalytic oxidation in aqueous slurries of activated carbon at room temperature and atmospheric pressure. In order to analyze the reaction rate, the mechanism was assumed by the steps of nonhomogeneous catalytic reaction. The experimental result show that oxidation rate was controlled by the reaction between adsorbed molecular oxygen and sulfur dioxide on the catalyst surface. Ar room temperature, the equat5ion of reaction rate was given as $ro_2 = 2.49 \times 10^{-7} P_O_2^{0.604}$.

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A Development of Recycling Technology of Solar Cell Wafering Slurry (태양전지 Wafering Slurry 재생기술 개발에 관한 연구)

  • Na, Won-Shik;Lee, Jae-Ha
    • Journal of Advanced Navigation Technology
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    • v.14 no.3
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    • pp.426-431
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    • 2010
  • 68% of the manufacturing costs of solar cell wafer can be attributed to the slurry. The recycling of slurries is mandatory for reducing the costs of manufacturing wafering production, and the disposal of industrial waste, as well as for cutting down pollution levels. Slurries are currently being recycled using the centrifuge(decanter) method. However, this method is less than optimal as it does not completely remove the fine particles, leading to low quality. Also, be cause of the incomplete separation from the oil, it causes the impurities in the dried slurries. This study aims to develope a new recycling technology that overcomes the flaws of the centrifuge by utilizing chemicals. It will provide a total solution to the crucial process of recycling slurries in the making of solar cell wafer, by increasing the efficiency and renewable rate.

Influence of Ice Recrystallization on Rheological Characteristics of Ice Slurries and Physicochemical Properties of Concentrated Milk

  • Park, Sung-Hee;Kim, Jee-Yeon;Hong, Geun-Pyo;Kwak, Hae-Soo;Min, Sang-Gi
    • Food Science and Biotechnology
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    • v.15 no.5
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    • pp.756-762
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    • 2006
  • Freeze concentration of milk was carried out through the controlled recrystallization of ice in a multi-stage freeze concentrator. Rheological characteristics of ice slurries were analyzed to determine efficient concentration levels for the freeze concentration process. It was determined that efficient concentration level was 17% of total solids in the first and 27% in the second stage. Physicochemical properties were compared between freeze concentrated and evaporated milk. Freeze concentrated milk was more similar in color appearance to control milk than was evaporated milk. pH significantly decreased in evaporated milk than in freeze concentrated milk. pH of freeze concentrated milk resulted in similar value to control. These results indicated the advantages of freeze concentration as a non-thermal milk processing technology in terms of physicochemical properties. Consequently, we investigated the influence of ice recrystallization on the rheological characteristics of ice slurries and physicochemical properties of freeze concentrated milk.

Effect of pH level and slurry particle size on the chemical mechanical planarization of langasite crystal wafer (pH level 및 slurry 입도가 langasite wafer의 chemical mechanical planarization에 미치는 영향)

  • Cho Hyun
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.15 no.1
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    • pp.34-38
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    • 2005
  • Effects of pH level and slurry particle size on material removal rate and planarization of langasite single crystal wafer have been examined. Higher material removal rate was obtained with lower pH level slurries while the planarization was found to be determined by average particle size of colloidal silica slurries. Slurries containing 0.045 ㎛ amorphous silica particles showed the best polishing effect without any scratches on the surface. Effective particle number has a strong effect on the surface planarization and the removal rate, so that the lower effective particle numbers produced low removal rate but the better planarization results.

Rheological Properties and Particle Size Distribution of Northeast Mixed Hardwood for Enzymatic Saccharification Processing with High Substrates Loading

  • Um, Byung-Hwan
    • Journal of the Korean Wood Science and Technology
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    • v.36 no.5
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    • pp.56-65
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    • 2008
  • In this paper experimental results are presented for the rheological behavior of high-solids saccharification of mixed northeast hardwood as a model feedstock. The experimental determination of the viscosity, shear stress, and shear rate relationships of the 10 to 20 percent slurry concentrations with constant enzyme concentrations were performed under variable rotational speed of a viscometer (2.0 to 200 RPM) at combined temperatures (50 to $30^{\circ}C$) for the initial four hours. The viscosities of saccharification slurries observed were in the ranges of 0.024 to 0.028, 0.401 to 0.058, and 0.840 to 0.087 Pa s for shear rates up to 100 reciprocal seconds at 10, 15, and 20 percent initial solids (w/v) respectively. The fluid behavior of the suspensions was modeled using the power-law, the Herschel-Bulkley, the Casson, and the Bingham model. The results showed that broth slurries were pseudoplastic with a yield stress. The model slope increased and the model intercept decreased with increasing fermentation time at shear rates normal for the fermentor. The broth slurries exhibited Newtonian behavior at high and low shear rates during initial saccharification process. The solid particle size ranged from 57.8 to $70.0{\mu}m$ for $40^{\circ}C$ and from 44.0 to 57.5 11m for combined temperatures at 10, 15, and 20 percent initial solids (w/v) respectively.

Dispersion Behavior of Transparent Dielectric Glass Frits in the Multi-Solvent and Ammonium-Type Dispersant System (다성분 용매와 암모늄계 분산제가 적용된 투명 유전체 프릿트 슬립의 분산거동)

  • Kim, Joo-Won;Chun, Young-Hwan;Hwang, Jong-Hee;Lee, Sang-Jin
    • Journal of the Korean Ceramic Society
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    • v.43 no.10 s.293
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    • pp.635-639
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    • 2006
  • Dispersion behavior of the slurries consisted of Pb or Bi-based glass frits, which are used for the fabrication of green sheet as PDP front panel transparent dielectric, was examined in non-aqueous solvent system. Measurements of sedimentation height and viscosity were conducted to determine proper dispersion condition in the various solvent and dispersant system. Azotropic compound and ethyl acetate were used as the solvent and ammonium-type dispersant was applied to the slurries. All slurries were dispersed well in azotropic solvent system involving 20$\sim$50 vol% ethyl acetate at 2$\sim$3 wt% dispersant content. Especially, dispersion behavior was notably improved in the addition of ethyl acetate in the Bi-based frit slurry.