• Title/Summary/Keyword: Size of specimen

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Synthesis of Reduced Graphene-metal Hybrid Materials via Ion-exchange Method and its Characterization (이온교환법에 의한 환원 그래핀-금속 하이브리드 소재의 합성 및 특성)

  • Park, Aeri;Kim, Sumin;Kim, Hyun;Han, Jong Hun
    • Journal of the Microelectronics and Packaging Society
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    • v.27 no.4
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    • pp.25-37
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    • 2020
  • In this study, hybridization of graphene oxide and metal was carried out by the functional groups containing oxygen and thermal treatment for reduction in order to enhance the electrical conductivity and magnetic properties of graphene materials. Graphene-metal hybrid materials were synthesized using the oxygen-containing functional groups (-OH, -COOH and so on) on the surface of graphene oxide by replacing them with metal ions via ion exchange method as well as thermal reduction. The metals used in this study were Fe, Ag, Ni, Zn, and Fe/Ag, and it was confirmed that metal particles of uniform size were well dispersed on the graphene surface through SEM, TEM, and EDS. All of the metal particles on the graphene surface had an oxide-crystalline structure. To check the electrical properties, sheet resistance of the rGO-metal hybrid sample was measured on the PET film made by the dip-coating, and the specific resistance was calculated by measuring the thickness of the specimen through SEM. As a result, the specific resistance was in the range of 2.14×10-5 and 3.5×10-3 ohm/cm.

An Experimental Study on the Evaluation of Shear Strength of Weathered Soil Containing Coarse Particles (굵은 입자가 포함된 풍화토의 전단강도 평가에 대한 실험연구)

  • Joon-Seok Kim
    • Journal of the Society of Disaster Information
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    • v.20 no.1
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    • pp.169-176
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    • 2024
  • Purpose: In this paper, an experimental study was conducted to analyze the difference in shear strength caused by the problem of excluding coarse particles due to the size of the test specimen in the direct shear test. Method: A large-scale direct shear test was conducted on three weathered soils containing coarse aggregates with a maximum diameter of 50mm. In addition, a small-scale direct shear test was performed using a sample with a maximum diameter of 5 mm, excluding coarse aggregates. Result: In the case of the small-scale direct shear test, compared to the results of the large-scale direct shear test containing large particles, the internal friction angle was about 2.3% smaller, and there was no significant difference. In terms of cohesion, compared to the large-scale direct shear test, the small-scale direct shear test derived about 80.3% smaller value, showing a relatively large difference. Conclusion: In the large-scale direct shear test, it was analyzed that the coarse particles had a greater impact on the cohesion than the internal friction angle. Therefore, granite weathered clay containing coarse particles is judged to have the same shear strength as the cohesive force that is not affected by vertical stress. In this study, it was analyzed that the small-scale direct shear test, which excludes the coarse particles that are commonly used, provides results on the safety side by excluding the effect of coarse particles.

Design and Verification of Shear Buckling Test Fixture for Composite Laminate (복합재 적층판의 전단좌굴시험을 위한 치구 설계 및 검증)

  • Park, Sung-Jun;Ko, Myung-Gyun;Kim, Dong-Gwan;Kim, Sang-Kuk;Moon, Chang-Oh;Kweon, Jin-Hwe;Choi, Jin-Ho
    • Composites Research
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    • v.27 no.4
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    • pp.158-167
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    • 2014
  • Final goal of this research is to establish the database for correlation factors which connects the test and analysis results of shear buckling allowables for composite plate. To accomplish the goal, extensive test and analysis works are required. In this paper, as the first step, a frame-type fixture for shear buckling test was designed and validated through the test and analysis. Final configuration of the fixture were determined via parametric study on the effect of specimen size, cross-sectional dimensions, and number of fastening bolts on the shear buckling load. Results of the study showed the designed frame-type fixture successfully induces the shear buckling of composite plate. However, there were deviations between the test results and analysis results for ideal case under pure shear load, which were mainly caused by the difference in plate sizes for both cases. The difference were larger in the plates with larger hole and simply supported boundary condition. It is concluded from the results that while the designed fixture can be used for the clamped plates with acceptable accuracy, it shows larger difference in the simply supported plates.

Delamination Detection of Retrofitted Concrete Using Horn Antenna (Horn Antenna를 이용한 콘크리트 보강재의 박리탐사 실험)

  • Rhim, Hong-Chul;Cho, Young-Sik
    • Journal of the Korean Society for Nondestructive Testing
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    • v.27 no.5
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    • pp.409-416
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    • 2007
  • In accordance with the increased usage of reinforcing materials such as carbon fibers and glass fibers, delamination detection between concrete and the reinforcing material is needed as such delaminations may be a major cause for strength reduction or failure of a structure. In this work, 15 GHz center frequency with 10 GHz band width horn antenna was used to detect delamination between concrete and carbon fibers or glass fibers. The specimens measured $600\;(length)\;{\times}\;600\;(width)\;{\times}\;100\;(thickness)\;mm$, and glass fibers and carbon fibers with a thickness of 1.5 mm were attached on the specimens' surfaces using epoxy. In addition, artificial delaminations of size $50\;(length)\;{\times}\;50\;(width)\;mm$ were placed in the middle of the specimen with thickness of 2, 4, 6 mm respectively together with a 2 mm delamination projecting upwards from the surface of the concrete. Therefore a total of 8 specimens were used, 4 specimens for glass fiber reinforced concrete and 4 for carbon fiber reinforced concrete, containing delaminations as described above. The experiment results were derived by using the difference of area under the curved graph. According to experimental results artifical delaminations were identified in both fiber reinforced and carbon reinforced specimens and these results could contribute to further development of delamination detection technology.

The suggestion of Steel Plate-Concrete Composite Beam Shape with Bolts (볼트 체결형 강판-콘크리트 합성보의 형상 제안)

  • Cho, Tae-Gu;Choi, Byong-Jeong
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.19 no.7
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    • pp.305-314
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    • 2018
  • The steel-plate concrete composite beam is composed of a steel plate, concrete and a shear connector to combine the two inhomogeneous materials. In general, the steel plate is assembled by welding an existing composite beam. In this study, a new steel-plate concrete composite (SPCC) beam was developed to reduce the size of the shear connector and improve its workability. The SPCC beam was composed of folded steel plates and concrete, without any shear connector. The folded steel plate was assembled with high strength bolts instead of welding. To improve the workability in field construction, a hat-shaped cap was attached in the junction with the slab. Monotonic two-point load testing was conducted under displacement control mode. The flexural strength of the SPCC beam specimen was calculated to be 76% of that of the complete composite beam by using the plastic stress distribution method and strain compatibility method. The cap acted as the stud and accessory. The synthesis rate could be increased by controlling the gap of the cap, and the bending performance could be evaluated by using the strain fitting method considering the synthesis rate of the SPCC beam.

Microstructure and plasma resistance of Y2O3 ceramics (Y2O3 세라믹스의 미세구조 및 플라즈마 저항성)

  • Lee, Hyun-Kyu;Lee, Seokshin;Kim, Bi-Ryong;Park, Tae-Eon;Yun, Young-Hoon
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.24 no.6
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    • pp.268-273
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    • 2014
  • $Y_2O_3$ ceramic specimens were fabricated from the granular powder, obtained by spray drying process from the slurry. The slurry was prepared by mixing PVA binder, NaOH for Ph control, PEG and $Y_2O_3$ powder. The $Y_2O_3$ specimen was shaped in size of ${\phi}14mm$ and then sintered at $1650^{\circ}C$. The characteristics, microstructure, densities and plasma resistance of the $Y_2O_3$ specimens were investigated with the function of forming pressure and sintering time. $Y_2O_3$ specimens were exposed under the $CHF_3/O_2/Ar$ plasma, the dry etching treatment of specimens was carried out by the physical reaction etching of $Ar^+$ ion beam and the chemical reaction etching of $F^-$ ion decomposed from $CHF_3$. With increasing sintering time, $Y_2O_3$ specimens showed relatively high density and strong resistance in plasma etching test.

Resonance Frequency Analysis of A Baseball Bat by Impact Angle (가진 각도에 따른 야구배트의 공진주파수 분석)

  • Park, Sun-Hyang;Chung, Woo-Yang;Jung, Hwan-Hee;Lee, Sang-Joon
    • Journal of the Korean Wood Science and Technology
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    • v.43 no.6
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    • pp.777-783
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    • 2015
  • Wood is an anisotropic material that shows the changes in hardness, quality and dimensions depending on the types of cells on three cross sections, size, array and so on. It can also be used in different ways according to its use, which requires a meticulous research, in order to maximize the utilization by understanding the nature and use; and by clarifying the theory and technologies. The research on relationship among wood's physical properties, density, and elasticity of modulus have been studied in Korea and abroad, but those studies were based on correlation gained through standardized specimen. Rather, the study on complete product is rare. Moreover, the previous reports are mostly concentrating on vibration mode and batting, though the wood's physical properties as a material have not been in the main focus. Therefore, this study will carried out for analyzing MOE through figuring material property out and comparing frequency adapting to the Canadian HardMaple bat. For comparison of material properties, we studied the annual ring and density of the bat; calculated the MOE with resonance frequency and formula (ASTM C1259); and verified the repulsive force of this material. As a result, the relevance of the resonance frequency and annual ring is weak, and in comparison in the grain direction in wood, the MOE value is higher when the grain direction in wood is excited horizontally than when is excited vertically, because the material is repulsive when grain direction is horizontal.

Detectability of Pore Defect in Wind Turbine Blade Composites Using Image Correlation Technique (이미지 상관 기법을 이용한 풍력 발전 블레이드용 복합재료의 기공 결함 검출능)

  • Kim, Jong Il;Huh, Yong Hak;Lee, Gun Chang
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.37 no.10
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    • pp.1201-1206
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    • 2013
  • Defects that occur during the manufacturing process or operation of a wind turbine blade have a great influence on its life and safety. Typically, defects such as delamination, pore, wrinkle and matrix crack are found in a blade. In this study, the detectability of the pores, a type of defect that frequently occur during manufacturing, was examined from the full field strain distribution determined with the image correlation technique. Pore defects were artificially introduced in four-ply laminated GFRP composites with $0^{\circ}/{\pm}45^{\circ}$ fiber direction. The artificial pores were introduced in consideration of their size and location. Three different-sized pores with diameter of 1, 2 and 3 mm were located on the top and bottom surface and embedded. By applying static loads of 0-200 MPa, the strain distributions over the specimen with the pore defects were determined using image correlation technique. It was found the pores with diameter exceeding 2 mm can be detected in diameter.

An Experimental Study on Seismic Performance Evaluation of Retrofitted Column of FRP Seismic Reinforcement that can be Emergency Construction (긴급시공이 가능한 FRP 내진보강재로 보강된 기둥의 내진성능평가 실험)

  • Kim, Jin-Sup;Kwon, Min-Ho;Seo, Hyun-Su;Lim, Jeong-Hee;Kim, Dong-Young
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.17 no.6
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    • pp.21-30
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    • 2013
  • As increasing number of large-size earthquake, the social interest of seismic retrofitting of RC structure is growing. Especially, the RC columns that are not reflected seismic design can not resist lateral loads by the earthquake. The brittle fracture of Non-seismic designed columns lead to full collapse of the building. Thus, the emergency columns reinforcement method is needed. That have a fast construction time, do not cause damage to the column. In the past, cross-sectional expansion method, a steel plate reinforcing method is applied mainly, but in recent years, carbon fiber sheet taking advantage of FRP (Fiber Reinforced Polymer) is widely used. In this study, retrofitting effect of seismic performance of FRP seismic reinforcement, which is possible to emergency construction, was examined. Reinforced concrete specimens were constructed to experimental study. The seismic performence of specimes retrifitted with FRP seismic reinforcement were evaluated. As a result, the seismic performance of specimen reinforced with FRP seismic reinforcement has been improved.

Application of Waste Concrete Powder as Silica Powder of Cement Extruding Panel (시멘트 압출패널의 규사분말 대체재로서 폐콘크리트 미립분의 활용)

  • Kim, Jin-Man;Kim, Kee-Seok;La, Jung-Min;Choi, Duck-Jin
    • Journal of the Korean Recycled Construction Resources Institute
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    • v.6 no.1
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    • pp.88-94
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    • 2011
  • To make recycling aggregate, quantity of fine particles increase due to multi-crushing. Though this particles were mixed with recycling aggregate, those have to be disparted from aggregate in the high quality recycling aggregate, because of the cause of low quality. Considering reactivity, fine particles is better than coarse one. Therefore, it needs to develop suitable usage. We try to make cement extruding material by using the fine particles from concrete recycling, as a silicious replacement. Test results are as follows ; 1) Waste concrete powder has major ingredients such as $SiO_2$ and CaO, its density is $2.45g/cm^3$ being similar to silica powder, its diameter is range 13 to $141{\mu}m$. 2) Considering to strength properties according to particle size, specimen was made using small particles is higher strength than large one. 3) Despite of exception in the autoclaved curing, when the replacement of waste fine particle increase, strength of extruding panel shows almost same level.

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