• 제목/요약/키워드: Sample pre-treatment

검색결과 224건 처리시간 0.027초

전처리조건에 따른 냉풍감압건조 복숭아의 이화학적 및 항산화 활성 (Effect of Different Pre-treatments on the Physicochemical and Antioxidant Activities of Cold-Vacuum Dried Peaches)

  • 권기만;김재원;윤광섭
    • 한국식품과학회지
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    • 제45권4호
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    • pp.466-472
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    • 2013
  • 전처리 방법에 따른 냉풍감압건조 복숭아의 이화학적 및 기능적 특성을 조사한 결과 수분함량은 0.3% NaCl 처리에서 유의적인 낮은 수분함량을 나타내었다. pH의 경우 전처리 구에서 낮아지는 경향을 보였고, 당도 및 당산비는 0.1% Vit-C 처리에서 높은 값을 나타내었다. 색도는 전반적으로 건조가 진행될수록 밝기를 나타내는 L 값은 감소하는 경향을 보였으며 색차는 Vit-C>NaCl>Sol-Ca>non-treated 순으로 낮은 값을 나타내었다. 갈변도 또한 색차의 결과와 일치하는 경향을 나타내었다. 총당은 무처리, NaCl, Vit-C 및 Sol-Ca 처리구가 무처리에 비해 높은 함량을 나타내어 향기 및 감미 유지 효과가 있는 것으로 관찰되었고, 유리당은 Vit-C 및 Sol-Ca 처리구에서 fructose, glucose 및 sucrose의 함량이 높은 것으로 나타났다. 절단력은 무처리에 비해 전처리구에서 증가하는 결과를 나타내었으며, Sol-Ca 처리구에서 가장 높은 값을 나타내었다. 관능특성에서는 전처리 구가 무처리에 비하여 외관, 색, 맛, 종합적 기호도가 높아지는 결과를 나타내었으며 특히, Vit-C 처리에서 가장 높은 기호특성을 나타내었다. 전처리방법에 따른 폴리페놀, 플라보노이드 및 프로안토시아니딘 함량에서는 전반적으로 전처리 구에서 높은 함량을 나타내었으며 프로안토시아니딘 함량에서 Vit-C 처리에서 가장 높은 함량을 나타내었다. 항산화능에서는 유용성분 함량이 높을수록 라디칼 소거능이 높아지는 양적 상관관계를 나타내었다.

Psychological Treatment for Pain Among Cancer Patients by Rational-Emotive Behavior Therapy - Efficacy in both India and Iran

  • Mahigir, Foroogh;Khanehkeshi, Ali;Karimi, Ayatollah
    • Asian Pacific Journal of Cancer Prevention
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    • 제13권9호
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    • pp.4561-4565
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    • 2012
  • The aim of the present study is to find out the influence of rational-emotive behavior therapy (REBT) on pain intensity among cancer patients in India and Iran. The study followed a quasi-experimental, pre-post test, carried out with a sample of 88 cancer patients, aged 21-52 years, referred to the Baharat cancer hospital of Mysore in India and Shahidzade hospital of Behbahan in Iran. They were randomly assigned to the experimental (n=India 21; Iran 22) and control (n=India 22; Iran 23) groups. Pain was measured with the McGill Pain Questionnaire-MPQ (1975), the intervention by REBT has given to the experimental group for 45 days (ten sessions) and at the end of intervention, the pain of patients was again evaluated. Concerning to hypothesis of the study, two independent sample T test and three ways mixed ANOVA is used to analyze the data. Results showed that the experimental group in post test had less pain than the control group, but there were no statistically significant differences between Indian and Iranian patients in pain perception. With respect the outcome of study, it has realized that REBT can be used in hospitals and other psychological clinics to reduce the pain of cancer patients.

Quantitative analysis and validation of naproxen tablets by using transmission raman spectroscopy

  • Jaejin Kim;Janghee Han;Young-Chul Lee;Young-Ah Woo
    • 분석과학
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    • 제37권2호
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    • pp.114-122
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    • 2024
  • A transmission Raman spectroscopy-based quantitative model, which can analyze the content of a drug product containing naproxen sodium as its active pharmaceutical ingredient (API), was developed. Compared with the existing analytical method, i.e., high-performance liquid chromatography (HPLC), Raman spectroscopy exhibits high test efficiency owing to its shorter sample pre-treatment and measurement time. Raman spectroscopy is environmentally friendly since samples can be tested rapidly via a nondestructive method without sample preparation using solvent. Through this analysis method, rapid on-site analysis was possible and it could prevent the production of defective tablets with potency problems. The developed method was applied to the assays of the naproxen sodium of coated tablets that were manufactured in commercial scale and the content of naproxen sodium was accurately predicted by Raman spectroscopy and compared with the reference analytical method such as HPLC. The method validation of the new approach was also performed. Further, the specificity, linearity, accuracy, precision, and robustness tests were conducted, and all the results were within the criteria. The standard error of cross-validation and standard error of prediction values were determined as 0.949 % and 0.724 %, respectively.

요통교육프로그램이 간호사의 요통감소에 미치는 효과 (The Effect of Low Back Pain Education Program on the Nurses in a General Hospital)

  • 권영숙
    • 기본간호학회지
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    • 제3권1호
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    • pp.108-127
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    • 1996
  • The purpose of this research was to determine whether or not a education program of low back pain would have benificial effect on nurses. Nonequivalent control group pre-post test research was designed. Subjects for this study were 50 selected from nurses who work at a general hospital in Taegu. Of them, twenty seven were assigned to experimental group, twenty-three to control group. The data were collected during the period from June 27 to August 31, 1994. The instruments used in this study were Visual Analog Scale for low back pain, Sit-and-reach test for trunk flexibility, and 1 min sit up test for abdominal muscle endurance. Data related to general chracteristics and factors of low back pain were collected with questionnaire developed by this reseacher. The data were analyzed by $X^2-test$, t-test and paired t-test, using the SAS package program. The results of this study are summerized as follows : 1. The numbers of the experimental group with low back pain were not a statistically significant difference from pre to posttesting($X^2=0.77$, p=.379), and the numbers of the control group with low back pain were also not a statistically significant difference from pre to posttesting($X^2=0.09$, p=.767). 2. The severity of low back pain of the experimental group was not a statistically significant difference from pre to posttesting(t=-0.55, p=.5857), and the severity of low back pain of the control group was also not a statistically significant difference from pre to posttesting(t=-0.70, p=.3101). 3. The trunk flexibility of the experimental group was not a statistically significant difference from pre to posttesting(t= 1.08, p=.2835), and the control group's trunk flexibility was also not a statistically significant difference from pre to posttesting(t=0.85, p=.4026). 4. The abdominal muscle endurance of the experimental group was a statistically significant difference from pre to posttesting(t=-2.42, p=.0190), but the control group's abdominal muscle endurance was not a statistically significant difference from pre to posttesting(t=-0.06, p=.9556) This study suggest that replication of study with more sample and more rigid treatment should be needed. And furthermore, the longitudinal research is needed to determine the effectiveness of education program.

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초등 예비교사의 협력 과학수업이 과학교수효능감 및 과학지식에 미치는 효과 (The Effects of Team Teaching on Science Learning of Pre-Service Teachers on Science Teaching Efficacy Beliefs and Scientific Knowledge)

  • 이용섭;김순식
    • 대한지구과학교육학회지
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    • 제9권3호
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    • pp.341-351
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    • 2016
  • 본 연구의 목적은 '과학과 교재연구' 강좌를 수강하는 초등예비교사들이 실험처치 후 과학교수효능감 및 과학 지식에 미치는 효과를 알아보는 것이다. 이를 위하여 '과학과 교재연구' 강좌를 수강하는 심화과정 4개 반(118명)을 대상으로 9월 초에서 12월까지 실험처치를 하였다. 실험처치는 한 학기의 교재연구 및 교수법에 대해 교육을 하는 것이며, 초등예비교사들이 모둠별 과학협력 수업을 시연하는 것으로 마무리 하였다. 연구의 결과 및 분석은 집단의 전-후 검사에서 대응 표본 t 검정으로 분석하였다. 연구의 결론은 다음과 같다. 첫째, 본 강좌 수강 후 초등 예비교사들은 과학교수효능감에서 효과가 있는 것으로 나타났다. 둘째, 본 강좌 수강 후 초등 예비교사들은 과학지식 습득에 효과가 있는 것으로 나타났다. 셋째, 수업시연에서 예비교사의 수업에 대한 인식은 긍정적인 영향을 미친 것으로 나타났다. 초등예비교사들은 교수설계의 원리에 의한 과제분석으로 과학과 과정안(세안)을 작성하였으며, 수업에 대한 올바른 마인드 함양과 수업에 대한 자신감을 갖는 것으로 나타났다.

이온삼투요법과 음파영동이 해조류 추출물의 체지방 분해에 미치는 효과 검정(II) (Clinical evaluation of the body fat breakdown effect during topical seaweed extracts treatment and in combination with the iontophoresis and phonophoresis(II))

  • 서태수;박종석;김유영;이동호
    • The Journal of Korean Physical Therapy
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    • 제16권1호
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    • pp.70-84
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    • 2004
  • This study was carried out to evaluate the body fat breakdown during topical seaweed extract treatment and in combination with the iontophoresis, phonophoresis method to enhance skin absorption of lipolytic compounds. Of 24 female obesity subjects, 7 treated a gel types of seaweed extract only(control group) and 10 treated in combination with the iontophoresis(experimental group I) and 7 treated in combination with the phonophoresis(experimental group II). Topical treatment of each sample was designed for 2 weeks, treated with 2 times a day about $10m{\ell}$ on the abdomen, triceps, thigh and superior ilium, respectively. Experimental group treat with the iontophoresis and phonophoresis during 5 minutes immediately after topical treatment. After one and two weeks of topical treatment, measured body weight, body fat, skinfolds thickness respectively. Then venous blood samples were taken and analyzed serum lipids. The results were as follows; 1) There were decrement of body weight, $\%$ of body fat, superior ilium, triceps and thigh thickness between pre and post treatment in all group. Especially, there were more decrement of body weight, $\%$ of body fat in the iontophoresis treated group. 2) There were decrement in total CHOL, LDL, TRIG and increment in HDL in all group. These phenomena were predominant in the iontophoresis treated group. CHOL decrement in the experimental group were significant after two weeks iontophoresis treatment.

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발효 소목 추출물의 키토산초산 용액과 일라이트 분말에 의한 염색 특성 (Dyeing Characteristics of Fermented Caesalpinia Sappan L. Wood Extract with Chitosan-Acetic Acid Solution and Illite Powder)

  • 박영미
    • 한국염색가공학회지
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    • 제31권4호
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    • pp.268-275
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    • 2019
  • In this study, silk fabrics was dyed with sappan wood extracts fermented for 5 and 15 days, respectively, and then the dyeability, durability and the functionality of the dyed silk were investigated. Before dyeing, the silk was pretreated with chitosan-acetic acid solution or chitosan acetic acid and illite blend solution. Thereafter, UV-Visible transmittance, color, fastness, antimicrobial activity, and the FIR emissivity were analyzed. As a result, the K/S value was higher in the samples that were not pre-treated or fermented. Regardless of fermentation, the lightfastness was not significantly different. The color fastness to washing was slightly better when the samples were pretreated with chitosan-acetic acid and illite, and then dyed with extracts fermented 5 days. In addition, all samples showed high antimicrobial activity of 99.9%, regardless of the fermentation. Far-infrared emissivity was confirmed to be slightly increased by the illite and chitosan-acetic acid solution treatment compared to the untreated sample.

근적외선 분광법을 이용한 고순도 SiCI4 중의 미량 불순물 SiHCI3의 분석 (Analysis of Trace Trichlorosilane in High Purity Silicon Tetrachloride by Near-IR Spectroscopy)

  • 박찬조;이석근
    • 분석과학
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    • 제15권1호
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    • pp.87-90
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    • 2002
  • The content of $SiHCl_3$ as a trace impurity in $SiCl_4$ was analyzed by Near IR spectrophotometer with optical fiber. The strong absorption bands of $5345{\sim}5116cm^{-1}$ and $4848{\sim}4349cm^{-1}$ were used for analysis of $SiHCl_3$, and the detection limit of impurity $SiCl_3$ was appeared to be 0.005 % in the spectrum. The quantitative analysis by Near IR spectrophotometry showed the analytical possibility of trace impurity in $SiCl_4$ without sample pre-treatment not only in the laboratory but also in the field.

식품 산업에서의 근적외선 분광법을 이용한 비파괴 분석법 동향 (Trends in non- destructive analysis using near infrared spectroscopy in food industry)

  • 박종락
    • 식품과학과 산업
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    • 제55권1호
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    • pp.2-22
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    • 2022
  • Near-infrared spectroscopy (NIRS) is one of the representative non-destructive and eco-friendly analysis methods used for rapid analysis of various ingredients in the food industry. To develop analysis model with NIRS, Chemometrics are applied after pre-treatment of spectrum. Many studies have been reviewed on the analysis of general and functional components for agricultural and livestock products. In the case of livestock products, some studies have been conducted for on-line analysis. This study investigated results on various samples and component applying near-infrared spectroscopy. Furthermore, the results according to sample condition were compared. It was confirmed that NIRS is applied to various fields in the food industry.

이온성 액체를 이용한 바이오매스 추출에 의해 얻어진 추출물의 건조 방법 (Method for Drying of Crude Extract Obtained by Biomass Extraction Using an Ionic Liquid)

  • 김슬기;김진현
    • Korean Chemical Engineering Research
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    • 제54권3호
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    • pp.374-379
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    • 2016
  • 이온성 액체를 보조용매로 이용할 경우 바이오매스로부터 파클리탁셀의 추출 효율은 획기적으로 개선되지만 잔류 이온성 액체로 후속 농축 및 건조에 많은 어려움이 따른다. 따라서 본 연구에서는 공정 효율 향상을 위하여 이온성 액체를 이용한 바이오매스 추출물을 효과적으로 건조할 수 있는 새로운 방법을 개발하였다. 추출물을 물로 전처리하고 추가적으로 세척함으로써 잔류 이온성 액체 제거를 통해 효과적으로 건조할 수 있었다. 물 전처리을 위한 최적의 시료/물 비, 혼합시간 및 추가세척을 위한 최적의 시료/물 비는 각각 1:70 (w/v), 4분, 1:100 (w/v)이었다. 또한 진공 건조보다 마이크로웨이브를 이용한 건조의 경우 건조시간을 9배 정도 단축 가능하여 공정 효율이 획기적으로 개선될 것으로 판단된다.