• 한국수소및신에너지학회논문집
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• 제13권3호
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• pp.224-232
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• 2002

CdS-$TiO_2$ nano-composite sol was prepared by the sol-gel method in organic solvents at room temperature and further hydrothermal treatment at various temperatures to control the physical properties of the primary particles. Again, CdS-$TiO_2$ composite particulate films were made by casting CdS-$TiO_2$ sols onto $F:SnO_2$ conducting glass and then heat-treatment at $400^{\circ}C$. Physical properties of these 61ms were further controlled by the surface treatment with $TiCl_4$, aqueous solution. The photo currents and hydrogen production rates measured under the experimental conditions varied according to the $CdS/[CdS+TiO_2]$ mole ratio and the mixed-sol preparation method. For $CdS-TiO_2$ composite sols prepared in IPA, CdS particles were homogeneously surrounded by $TiO_2$ particles. Also, the surface treatment with $TiCl_4$ aqueous solution caused a considerable improvement in the photocatalytic activity, probably as a result of close contacts between the primary particles by the etching effect of $TiCl_4$. It was found that the photoelectrochemical performance of these particulate films could be effectively enhanced by this approach.

• 대한안전경영과학회지
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• 제9권6호
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• pp.197-204
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• 2007

Ceramic pigments were developed by using 4 kinds of Brass scraps. Each Brass scraps were mixed with same weight-ratio of Husk ash, and fine-ground by Rotate ring mill(RRG-120, Armstech industrial. co. Ltd, Korea) after firing at $900^{\circ}C$, $1000^{\circ}C$ and $1100^{\circ}C$. As a result, analysis of particle size of synthetic pigments by particle size analyser, they are $3{\mu}m$ as average. The resulting pigments were characterized by using XRD, FT-IR, SEM Structure of the crystals are Zn2SiO4,, and ZnO, Cu2O, CuO, and cristobalite are existed and particles' shape are plate or needle. As a result of analysis of chemical composition by XRF, synthetic pigments have high SiO2 and CuO content and have SnO2, ZnO and NiO, too. 1wt%, 3wt% and 5wt% pigments were added in each lime glaze, lime-barium glaze and lime-magnesia glaze, and fired at oxidation and reducing atmosphere to figure hue in glazes out. As a result of analysis of color, chroma and brightness by UV, colors of glazes fired at oxidation atmosphere turned into green from sky blue, and colors of glazes fired at reducing atmosphere turned into pink and red.

• Journal of Pharmaceutical Investigation
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• 제40권6호
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• pp.353-356
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• 2010

Although liposomes have been applied as drug delivery systems in various fields, the usage was limited due to the low encapsulation efficiency compared to other carrier systems. Here, cationic liposomes were prepared by mixing 1,2-dioleoyl-3-trimethylammoniopropane (DOTAP) as a cationic lipid, 1,2-dioleoyl-sn-glycerol-phosphoethanolamine (DOPE) and cholesterol (CH), and the liposomes were hydrated by varying the aqueous phases such as phosphate-buffered saline (PBS), 5% dextrose, and 10% sucrose in order to improve the encapsulation efficiency of bovine serum albumin (BSA). The particle size and zeta potential were determined by dynamic light scattering method and in vitro release patterns were investigated by spectrophotometry. Particle size and zeta potential of liposomes were varied depending on the ratio of DOTAP/DOPE/CH in range of 270-350 nm and 0.8-9.7 mV, respectively. Moreover, the addition of polyethylene glycol (PEG) improved the encapsulation efficiency from 37% to 43% as well as reduced particle sizes of liposomes while the liposomes were hydrated in PBS. When the liposomes were hydrated with 10% sucrose, the encapsulation efficiency of BSA was higher than any other groups. Whereas PBS was used as hydration solution, lower encapsulation efficiency was obtained compared with other groups. More than 60% of BSA was released from the liposomes hydrated with 10% sucrose; thereafter another 20% of BSA was released. Therefore, release pattern of BSA from cationic liposomes was extended release in this study. From the results, cationic liposomes dispersed in 10% sucrose would be potential carrier with high encapsulation efficiency.

• 대한치과교정학회지
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• 제30권4호
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• pp.387-398
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• 2000

이 연구는 악외견인장치의 하나인 Anterior J hook headgear의 상악골 성장 억제효과를 관찰하기 위하여 혼합 치열기의 골격성 II급 부정교합 아동 20명을 대상으로 얻어진 측모두부 방사선규격사진이 분석되었다. 구강내 교정장치로서는 horseshoe appliance가 사용되었으며, J hook의 견인은 상악견치 중앙부에서 후상방으로 이루워졌다. Anterior J hook headgear의 적용기간은 평균 14개월이었으며 계수형 분석법에 의해 적용전후 측모두부 방사선규격사진이 분석된 바, 다음과 같은 결과를 얻었다. 1. 상악골의 전하방성장이 억제되었다. 2. 상악골의 회전효과는 일어나지 않았다. 3. 상악치열은 전체적으로 후방이동하였다. 4. 상악의 치아치조부 성장억제변화는 구치부보다는 전치부에서 더 뚜렷하였다. 5. 하악평면각(SN-MP)은 치료후 변화가 없었으며 하악골은 정상적인 성장을 나타냈다. 6. 전안면고경과 후안면고경 사이의 비율은 유의한 변화가 없었다.

• 한국가스학회지
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• 제8권4호
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• pp.30-35
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• 2004

본 논문은 다구찌 실험 설계법을 이용하여 압력용기의 메탈시일 구조물에 대한 해석을 수행하였다. 다구찌 설계방법은 압력용기의 밀봉을 위한 캔티레버 타입 밀봉장치 구조물에 대한 설계 파라메터를 최적화 하는데 대단히 유용하다. 다구찌 기법으로 수행된 해석결과에 따르면, 최적화 설계 치수는 단지 16번의 반복 실험법에 의해 파라메터 치수를 최적의 조건으로 얻을 수 있다는 측면에서 간편한 설계도구이다. 이것은 다구찌 설계 실험법이 곡선면을 갖는 구조물의 최적화 설계에서 대단히 유용하다는 것을 의미한다. 다구찌 설계기법에 기초한 해석결과를 보면, 메탈시일 구조물의 에지부에 대한 최적화 치수와 경사각도는 $d_1=50mm,\;d_2=60mm,\;a_1=20^{\circ},\;a_2=8^{\circ},\;a_3=5^{\circ}$으로 각각 요약될 수 있다.

• Progress in Superconductivity
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• 제14권1호
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• pp.1-10
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• 2012

We fabricated a closed coils by using resistive-joint method and the joint resistance of the coils were estimated by field decay technique in liquid nitrogen. We used the Runge-kutta method for the numerical analysis to calculate the decay properties. The closed coil was wound by $(Bi,Pb)_2Sr_2Ca_2Cu_3O_x$/Ag tape. Both ends the tape were overlapped and soldered to each other. The current was induced in a closed coils by external magnetic flux density. Its decay characteristic was observed by means of measuring the magnetic flux density generated by induced current at the center of the closed coil with hall sensor. The joint resistance was calculated as the ratio of the inductance of the loop to the time constants. The joint resistances were evaluated as a function of critical current of loop, contact length, sweep time, and external magnetic flux density in a contact length of 7 cm. It was observed that joint resistance was dependent on contact length of a closed coil, but independent of critical current, sweep time, and external magnetic flux density. The joint resistance was measured to be higher for a standard four-probe method, compared with that for the field decay technique. This implies that noise of measurement in a standard four-probe method is larger than that of field decay technique. It was estimated that joint resistance was $8.0{\times}10^{-9}{\Omega}$ to $11.4{\times}10^{-9}{\Omega}$ for coils of contact length for 7 cm. It was found that 40Pb/60Sn solder are unsuitable for persistent mode.

• 한국도로학회논문집
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• 제1권2호
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• pp.155-168
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• 1999

본 연구에서는 아스팔트 포장에서 소성변형과 균열에 대한 저항성, 그리고 경제성효과를 만족시킬 수 있는 최적 단면을 구하고자 하였다. 국내 아스팔트 포장재료의 물성치와 현행 국내설계적용 상대강도계수로 부터 구한 탄성계수의 2종류 물성요인을 입력변수로 하여 다층탄성이론에 의한 구조해석과 유한요소해석을 실시하여 아스팔트층의 하단인장변형률과 노상압축변형률에 대한 저항성 효과를 분석하였고. 점탄성해석에 의한 소성변형 예측과 경제성 분석을 통해 아스팔트 포장단면설계의 개선방안을 제시하였다. 점탄성 구조해석결과, 표층의 두께는 다층탄성해석과 마찬가지로 표층의 두께는 최소두께인 5cm일 때 소성변형에 대한 저항성이 큰 단면으로 나타났으며, 기층의 두께는 SN치가 감소함에 따라 다층탄성 구조해석시보다 기층두께감소가 커지는 것으로 나타났다. 본 연구에서는 아스팔트포장의 내구성, 소성변형, 경제성을 만족하는 단면을 찾기위해 상대지수개념을 도입하였으며 상대지수분석을 통하여 보조기층의 두께에 대한 아스팔트층의 적정단면비가 1.0$\sim$2.5임을 제시하였다.

• 한국표면공학회지
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• 제47권5호
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• pp.239-243
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• 2014

The electrical and optical properties of amorphous In-Tin-Zinc-Oxide(ITZO) deposited at room temperature using rf-magnetron sputtering were investigated. The amorphous ITZO thin films were obtained at the composition of In:Sn:Zn = 6:2:2, 4:3:3, and 2:4:4, but the ITZO (8:1:1) showed a crystalline phase of bixbyite structure of In2O3. The resistivity of ITZO could be controlled by oxygen pressure in the sputtering ambient. The resistivity of post-annealed ITZO thin films exhibited the dependence on the amount of Indium. Optical energy band gap and transmittance increased as the amount of indium in ITZO increased. For the device application with ITZO, the bottom-gated thin-film transistor using ITZO as a active channel layer was fabricated. It showed a threshold voltage of 1.42V and an on/off ratio of $5.63{\times}10^7$ operated with saturation field-effect mobility of $14.2cm^2/V{\cdot}s$.

• 한국분말재료학회지
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• 제28권6호
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• pp.462-469
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• 2021

Tin/graphite composites are prepared as anode materials for Li-ion batteries using a dry ball-milling process. The main experimental variables in this work are the ball milling time (0-8 h) and composition ratio (tin:graphite=5:95, 15:85, and 30:70 w/w) of graphite and tin powder. For comparison, a tin/graphite composite is prepared using wet ball milling. The morphology and structure of the different tin/graphite composites are investigated using X-ray diffraction, Raman spectroscopy, energy-dispersive X-ray spectroscopy, and scanning and transmission electron microscopy. The electrochemical properties of the samples are also examined. The optimal dry ball milling time for the uniform mixing of graphite and tin is 6 h in a graphite-30wt.%Sn sample. The electrode prepared from the composite that is dry-ball-milled for 6 h exhibits the best cycle performance (discharge capacity after 50^th cycle: 308 mAh/g and capacity retention: 46%). The discharge capacity after the 50^th cycle is approximately 112 mAh/g, higher than that when the electrode is composed of only graphite (196 mAh/g after 50^th cycle). This result indicates that it is possible to manufacture a tin/graphite composite anode material that can effectively buffer the volume change that occurs during cycling, even using a simple dry ball-milling process.

• 대한치과교정학회지
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• 제34권3호
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• pp.241-251
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• 2004

교정치료에 대한 인지도 변화 및 보호자의 관심증가로 조기에 내원하는 환자가 많으며 그 중 일부가 전치부 치근첨이 완성되기 전인 10세 이전에 고정식 교정장치가 필요하게 된다 따라서 본 연구에서는 미완성 치근의 치료 전후 치근의 길이 변화를 측정하고 형태변화를 관찰하여 완성된 치근의 교정력에 의한 변화양상과 비교하고, 환자의 성별, 기간, 이동양상 등과의 연관성을 조사하였다. 상악의 전치부 치근첨이 완성되지 않은 상태에서 고정식 교정치료를 시작한 8~10세 환자 28명을 실험군으로 하고, 치근첨이 완성된 상태에서 고정식 교정치료를 시작한 11~15세 환자 31명을 대조군으로 삼았다. 상악 4전치의 치료 전후 치근단 방사선사진상에서 치관, 치근길이를 측정해서, 치근길이의 변화량, 치관/치근 비의 변화량을 계산했고 분류체 계에 따라 치근형태에 점수를 부여했다. 결과는 다음과 같다. 1. 대부분의 미완성 치근은 교정치료 후에도 치근 길이가 증가하였으며 정상적인 치근첨 형태를 보였다. 2. 치료기간이 길어지거나 개방교합의 경우, 미완성 치근이라도 치근길이가 증가하지 않거나 더 짧아진 경우도 있었으며 정상적인 길이가 되더라도 치근첨의 완성 형태가 뭉툭한 흡수 형태를 보였다. 3. 완성치근에서는 교정치료에 의하여 대부분의 치근이 경미한 치근흡수를 보였으며, 흡수된 치근첨의 형태는 미완성 치근의 완성형태보다 더 뭉툭하였다(p<0.05). 4, 미완성 치근에서는 치료기간과, 완성치근에서는 치아의 이동거리(U1 to facial plane의 변화량)와 유의한 상관관계를 보였다(P<0.05). 5. 미완성 치근, 완성치근 모두 성별, 부정교합 분류, 수직피개의 변화량, 두개저에 대한 치아의 위치 변화(U1 to SN의 변화량)등과는 유의한 상관관계를 보이지 않았다.