• Journal of Adhesion and Interface
• /
• v.2 no.2
• /
• pp.11-19
• /
• 2001

The phase-transfer catalyzed radical polymerization of styrene was carried out using tricaprylylmethylammonium chloride as a phase-transfer catalyst in a two-phase system of an aqueous $Na_2S_2O_8$ solution and toluene at $60^{\circ}C$ under nitrogen atmosphere. The initial rate of radical polymerization was expressed as the combined terms of concentrations of quaternary onium cation and peroxydisulfate anion in the aqueous phase rather than the fed concentrations of catalyst and $Na_2S_2O_8$. The observed initial rate of radical polymerization was used to analyze the radical polymerization mechanism with a cycle phase-transfer initiation step in the heterogeneous liquid-liquid system. The viscosity average molecular weight of polystyrene was inversely proportional to concentration of $Na_2S_2O_8$ expressed as $[Q^+]([S_2O{_8}^{2-}]{\alpha}_2)^{1/2}$ derived by the radical polymerization mechanism.

• Journal of the Korean Society for Heat Treatment
• /
• v.21 no.1
• /
• pp.26-32
• /
• 2008

Effects of annealing treatment on microstructure and mechanical property of co-sputtered TiNi thin films were studied. As-deposited films showed amorphous state. However, above annealing temperature of $500^{\circ}C$ martensite phase (B19'), precipitate phase ($Ti_2Ni$) and a small amount of parent phase ($B_2$) were present, and phase transformation behaviors were three multi-step phase transformations $B19^{\prime}{\rightarrow}B_2$ and $B_2{\rightarrow}R-phase$ and $R-phase{\rightarrow}B19^{\prime}$. Increase of martensite transformation temperature, increase of microhardness and Young's modulus of TiNi films annealed above $500^{\circ}C$ were discussed in terms of precipitate phase.

• Journal of the Korean Institute of Telematics and Electronics S
• /
• v.34S no.1
• /
• pp.105-114
• /
• 1997

The phase retrieval problem is concerned with the reconstruction of a signal or its fourier transform phase form the fourier transform magnitude of the signal. This problem does not have a unique solution, in general. If, however, the desired signal is minimum-phase, then it can be decided uniquely. This paper shows that we can make a minimum-phase signal by adding a delta function having a large value at the origin of an arbitrary one-dimensional signal, and a two-dimensional signal can be uniquely specified from its fourier transform magnitude if it is added by a delta function having a large value at the origin, and finally we can solve a two-dimensional phase retrieval problem by decomposing it into several ine-dimensional phase retrieval problems.

• Proceedings of the KIEE Conference
• /
• 1995.07a
• /
• pp.350-352
• /
• 1995

The starting characteristics of single phase induction motor(SPIM) is described by control of phase and voltage. Auxiliary winding voltage is controlled by DC amplifier and phase is integrator. These processes enable comparison of torque with slip in each voltage and phase angle variations. Simulation and experimentation results of the motor's torque-slip characteristics using the controlled auxiliary winding voltage and phase angle arc shown and discussed. As a results, starting time is fast and main winding current is small when auxiliary winding voltage is low than rating voltage and starting characteristics is good in phase angle $90^{\circ}$.

• Journal of Institute of Control, Robotics and Systems
• /
• v.10 no.4
• /
• pp.325-333
• /
• 2004

It is investigated that the relation between the response time of DVR(Dynamic Voltage Restorer) and the possible compensation range of voltage dip by the DVR system which protects the 3-phase phase-controlled rectifier from voltage dip. As a result, the permissible range of voltage dip is presented in the 3-phase phase-controlled rectifier, and it is presented that the range of voltage dip which can be compensated according to the DVR s response time. when the DVR compensates voltage dip, Using the proposed method, the DVR s response time can be determined from the parameters of 3-phase phase-controlled rectifier and the possible compensation range of voltage dip, and it is possible to use the control system which have an appropriate speed. Therefore, the use of excessively fast device can be avoided, and the stability of the overall system is improved. Also the reliance of DVR about the 3-phase phase-controlled rectifier can be verified.

• Journal of the Korea Institute of Military Science and Technology
• /
• v.19 no.3
• /
• pp.379-386
• /
• 2016

In this paper, phase noise analysis result for 2.4 GHz PLL(phase locked loop) using SPD(sample phase detector) is proposed. It can be used for high performance frequency synthesizer's LO(local oscillator) to extend output frequency range or for LO of offset PLL to reduce a division rate or for clock signal of DDS(direct digital synthesizer). Before manufacturing, theoretical estimation of PLL's phase noise performance should be performed. In order to calculate phase noise of PLL using SPD, Leeson model is used for modeling phase noise of VCO(voltage controlled oscillator) and OCXO(ovened crystal oscillator). After theoretically analyzing phase noise of PLL, optimized loop filter bandwidth was determined. And then, phase noise of designed loop filter was calculated to find suitable OP-Amp. Also, the calculated result of phase noise was compared with the measured one. The measured phase noise of PLL was -130 dBc/Hz @ 10 kHz.

• Korean Journal of Animal Reproduction
• /
• v.20 no.2
• /
• pp.143-153
• /
• 1996

To improve the efficiency of nuclear transplantation in the rabbit, this study were evaluated the influence of celly cycle of donor nuclei on the in vitro developmental potential in the nuclear transplant embryos. The embryos of 16-cell stage were collected from the mated does at 48h post-hCG injection and they were synchronized to G1 phase of 32-cell stage. Synchronization of the cell cylce of blastomeres were induced, first, using an microtubules polymerization inhibitor, 0.5$\mu\textrm{g}$/ml colcemid for 10h to arrest blastomeres in metaphase, and secondly, using a DNA synthesis inhibitor, 0.1$\mu\textrm{g}$/ml aphidicolin for 1.5 to 2h to cleave to 32-cell stage and arrest them in G1 phase. The separated G1 phase blastomeres of 32-cell stage were injectied into enucleated recipient cytoplasms by micromanipulation. After culture until 20h post-hCG injection, the nuclear transplant oocytes were electrofused and activated by electrical stimulation. The nuclear transplant embryos were co-cultured for 120h. In vitro cultured embryos were monitored every 24h to assess for development rate. After in vitro cultue for 120h, the nuclear transplant embryos developed to blastocyst stage were stained with Hoechst 33342 dye for counting the number of blastomeres under a fluorescence microscopy. The cleavage rate of blastomeres from 16-cell stage stage rabbit embryos treated with colcemid for 10h or aphidicolin for 6h following colcemid for 10h were not significantly different. The electrofusion rate was similar by high in S and G1 phase donor nuclei as 80.6 and 79.1%, respectively. However, the nuclear transplant embryos using G1 phase donor nuclei were developed to blastocyst at high rate(60.3%) than those using S phase donor nuclei(26.0%). Moreover, the mean blastocyst stage were increased significantly(P<0.05) with the G1 phase donor nuclei(176.6 cells and 1.50 cycles), as compared with the S phase donor nuclei(136.6 cells and 1.42 cycles). These results show that the blastomeres of G1 phase were more successful as donor nuclei in the nuclear transplant procedure, compared with S phase.

• Asian-Australasian Journal of Animal Sciences
• /
• v.23 no.2
• /
• pp.169-174
• /
• 2010

A meta-analysis was conducted to summarize the results of studies which have described the profiles of hormones during the oestrous cycle in buffalo using a fixed effect model and a random effect model. Plasma progesterone concentrations were lowest (0.30${\pm}$0.06 ng/ml) during the peri-oestrous phase and increased (p = 0.067) through the early luteal phase to a maximum concentration (1.94${\pm}$0.03 ng/ml) during the mid-luteal phase. Circulating plasma inhibin and estradiol concentrations were lowest (0.31${\pm}$0.01 and 11.04${\pm}$0.13 ng/ml) during the mid-luteal phase, increased through the late luteal phase to maximum concentrations (0.44${\pm}$0.02 and 22.48${\pm}$0.32 ng/ml) during the peri-oestrous phase. Plasma FSH concentrations were lowest during the early luteal phase and increased through the mid-luteal phase to a maximum concentration during the peri-oestrous phase. Peripheral prolactin concentrations were lowest during the late luteal phase and increased to a maximum concentration during the peri-oestrous phase which then declined (p = 0.716) during the early luteal phase. Peripheral plasma cortisol concentrations decreased from 2.68${\pm}$0.14 ng/ml during the early luteal phase to 1.43${\pm}$0.27 ng/ml during the mid-luteal phase (p<0.001) which then increased to 2.06${\pm}$0.17 ng/ml during the late luteal phase. Plasma $T_{5}$ concentrations decreased from the late luteal phase to the peri-oestrous phase (p<0.001) which then increased during the early luteal phase. $T_{4}$ concentrations increased from the late luteal phase to the peri-oestrous phase which then decreased during the early luteal phase.

• The Transactions of The Korean Institute of Electrical Engineers
• /
• v.62 no.4
• /
• pp.510-516
• /
• 2013

This paper suggests a 3-phase series-resonant type high voltage capacitor charger for an EML pulsed power system. The operating principle on the charger is explained by an equivalent circuit. Additionally, we analyze the charging characteristic in one discontinuous conduction mode and three continuous conduction modes. The analysis shows that the resonant current per phase is two thirds of the 3-phase charger's average charging current and one third of the single-phase charger's average charging current with the same capacity. We suggest a design method of the 3-phase capacitor charger in each operational mode and present an example of 3.5 kW capacitor charger at ${\omega}_s=0.33{\omega}_r$. The 3.5 kW 3-phase capacitor charger prototype is assembled with a TI28335 controller and a 40 kJ, 7 kV capacitor. The design rules based on the analysis are verified by experiment.

• Parasites, Hosts and Diseases
• /
• v.29 no.2
• /
• pp.121-128
• /
• 1991

The degree of attraction of Toxoplasma gondii to vertebrate cells varies with cell type and cell phase. Human promyelocytic leukemia cells, HL-60, were synchronized by double thymidine block method and co-cultured with Toxoplasma for 1 hr at each cell stage to investigate the cell cycle specific susceptibility of parasites to host cells. For 30 hr the average number of Texoplasma that invaded was a little changed except at 3 hr from G1/S phase boundary which concurred with the peak point of DNA synthesis. At 3 hr which is a relatively short interval compared to whole S phase, modification of cells by parasitic invasion was most remarkable. The number of Toxoplasma that penetrated was increased to more than sin times. The shape of the cells became sludgy and almost indiscernible by strong accessibility of parasites only for an hour of mfd-S phase. The same auctuation was also observed at the second peak of S phase but weakly. This suggests that there be surface molecules concerning with the attachment of Texoplasma to the host cells, which is expressed at special point of S phase. further studies on the specific protein or similar molecules related could be carried out using synchronized HL-60 cells.