• Title/Summary/Keyword: Powder target

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A Study on the High Quality and Low Cost Fabrication Technology of ZnO Thin Films for Solar Cell Applications (태양전지 응용을 위한 고품위 및 저가격 ZnO 박막 제조에 관한 연구)

  • Lee, Jae-Hyeong
    • Journal of the Korea Institute of Information and Communication Engineering
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    • v.14 no.1
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    • pp.191-196
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    • 2010
  • Aluminum doped zinc oxide (AZO) films have been prepared on Coming 7059 glass substrates by r.f. magnetron sputtering method. A powder target instead of a conventional sintered ceramic target was used in order to improve the utilization efficiency of the target and reduce the cost of the film deposition process. The influence of sputter pressure on the structural, electrical, and optical properties of AZO films were studied. The AZO films had hexagonal wurtzite structure with a preferred c-axis orientation, regardless of sputter pressure and target types. The crystallinity and degree of orientation was increased by increasing the sputter pressure. For higher sputtering pressures, a reduction of the resistivity was observed due to a increase on the mobility and the carrier concentration. The lowest resistivity of $6.5{\times}10^{-3}\;{\Omega}-cm$ and the average transmittance of 80% can be obtained for films deposited at 15 mTorr.

Sintering and Rolling Behavior of Cu-50In-13Ga Ternary Alloy Powder for Sputtering Target (스퍼터링 타겟용 Cu-50In-13Ga 3원계 합금 분말의 소결 및 압연 거동)

  • Kim, Dae-Won;Kim, Yong-Ho;Kim, Jung-Han;Kim, Dae-Guen;Lee, Jong-Hyeon;Choi, Kwang-Bo;Son, Hyeon-Taek
    • Journal of Powder Materials
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    • v.19 no.4
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    • pp.264-270
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    • 2012
  • In this study, we mainly focus on the study of densification of gas-atomized Cu-50 wt.%In-13 wt.%Ga alloy powder without occurrence of crack during the forming process. Cu-50 wt.%In-13 wt.%Ga alloy powder was consolidated by sintering and rolling processes in order to obtain high density. The phase and microstructure of formed materials were examined by X-ray diffraction (XRD), scanning electron microscopy (SEM) and optical microscopy (OM), respectively. Warm rolling using copper can result in the improvement of density. The specimen obtained with 80% of rolling reduction ratio at $140^{\circ}C$ using cooper can have the highest density of $8.039g/cm^3$.

Influence of sputtering parameter on the properties of silver-doped zinc oxide sputtered films

  • S. H. Jeong;Lee, S. B.;J.H. Boo
    • Proceedings of the Korean Institute of Surface Engineering Conference
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    • 2003.10a
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    • pp.58-58
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    • 2003
  • Silver doped ZnO (SZO) films were prepared by rf magnetron sputtering on glass substrates with extraordinary designed ZnO target. With the doping source for target, use AgNO$_3$ powder on a various rate (0, 2, and 4 wt.%). We investigated dependence of coating parameter such as dopant content in target and substrate temperature in the SZO films. The SZO films have a preferred orientation in the (002) direction. As amounts of the Ag dopant in the target were increased, the crystallinity and the transmittance and optical band gap were decreased. And the substrate temperature were increased, the crystallinity and the transmittance were increased. But the crystallinity and the transmittance of SZO films were retrograde at 200$^{\circ}C$. Upside facts were related with composition. In addition, the Oxygen K-edge features of the SZO films were investigated by using near edge X-ray absorption fine structure (NEXAFS) spectroscopy. Changes of optical band gap of the SZO films were explained compared with XRD, XPS and NEXAFS spectra.

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Evaluation of the Accuracy and Precision Three-Dimensional Stereotactic Breast Biopsy (3차원 입체정위 유방생검술의 정확도 및 정밀도 평가)

  • Lee, Mi-Hwa
    • Journal of radiological science and technology
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    • v.38 no.3
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    • pp.213-220
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    • 2015
  • This research was study the accuracy of three-dimensional stereotactic breast biopsy, using a core Needle Biopsy and to assess the accuracy of Stereotactic biopsy and Sono guided biopsy. Using Stereotactic QC phantom to measure the accuracy of the 3D sterotactic machine. CT Scan and equipment obtained in the measured X, Y, Z and compares the accuracy of the length. Using Agar power phantom compare the accuracy of the 3D sterotactic machine and 2D ultrasound machine. Z axis measured by the equipment to compare the accuracy and reliability. Check the accuracy by using visual inspection and Specimen Medical application phantom. The accuracy of the 3D sterotactic machine measured by Stereotactic QC phantom was 100%. Accuracy as compared to CT, all of X, Y, Z axis is p > 0.05. The accuracy of the two devices was 100% as measured by Agar powder phantom. There was no difference between t he t wo d evices as C T and p > 0.05. 3D sterotactic machine of the ICC was 0.954, 2D ultrasound machine was 0.785. 2D ultrasound machine was different according to the inspector. Medical application phantom experiments in 3D sterotactic machine could not find the Sliced boneless ham. 2D ultrasound machine has not been able to find a small chalk powder group. The reproducibility of the three-dimensional stereotactic breast biopsy was better than effect of Sono guided biopsy.

Preparation of Nano-Sized ITO Powder from Waste ITO Target by Spray Pyrolysis Process (폐(廢) ITO 타겟으로부터 분무열분해(噴霧熱分解) 공정(工程)에 의한 ITO 나노 분말(粉末) 제조(製造))

  • Yu, Jae-Keun;Kang, Seong-Gu;Sohn, Jin-Gun
    • Resources Recycling
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    • v.16 no.1 s.75
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    • pp.28-36
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    • 2007
  • Nano-sized ITO powders with the average particle size below 50 nm were synthesized from complex acid solution dissolved the ITO target into hydrochloric acid by a spray pyrolysis process, and the influences of reaction factors as reaction temperature and concentration of raw material solution were investigated. As the reaction temperature increases from 800 to $1000^{\circ}C$, the average particle size of the ITO powder increases from 40 nm to 100 nm, the microstructure gradually becomes solid, individual particles independently appear with the shape of polygon, the particle size distribution becomes increasingly irregular, the XRD peak intensity gradually increases and the specific surface area decreases. As the concentration of the raw material solution increases from 50g/l to 400g/l, the average particle size of ITO powder gradually increases, yet the particle size distribution appears more irregular. When the concentration is at 50 g/l, the average particle size of ITO powder is below 30 nm and the particle size distribution appears comparatively uniform. Nevertheless, when the concentration reaches 400 g/l, which is close to e saturated concentration, the particle size distribution appears extremely irregular, and the particles with the size ranging from 20 nm to 100 nm coexist. Along with the concentration rise, the XRD peak intensity gradually increases, yet the specific surface area decreases.

Preparation of Nano Sized Indium Tin Oxide (ITO) Powder with Average Particle Size Below 30 nm from Waste ITO Target by Spray Pyrolysis Process (폐 ITO 타겟으로부터 분무열분해 공정에 의한 평균입도 30 nm 이하의 인듐-주석 산화물 분체 제조)

  • Kim, Donghee;Yu, Jaekeun
    • Resources Recycling
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    • v.27 no.2
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    • pp.24-31
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    • 2018
  • In this study, waste ITO target is dissolved into hydrochloric acid to generate a complex indium-tin chloride solution. Nano sized ITO powder with an average particle size below 30 nm are generated from these raw material solutions by spray pyrolysis process. Also, in this study, thermodynamic equations for the formation of indium-tin oxide (ITO) are established. As the reaction temperature increased from $800^{\circ}C$ to $900^{\circ}C$, the proportion and size of the spherical droplet shape in which nano sized particles aggregated gradually decreased, and the surface structure gradually became densified. When the reaction temperature was $800^{\circ}C$, the average particle size of the generated powder was about 20 nm, and no significant sintering was observed. At a reaction temperature of $900^{\circ}C$, the split of the droplet was more severe than at $800^{\circ}C$, and the rate of maintenance of the initial atomized droplet shape decreased sharply. The average particle size of the powder formed was about 25 nm. The ITO particles were composed of single solid crystals, regardless of reaction temperature. XRD analysis showed that only the ITO phase was formed. Remarkably, the specific surface area decreased by about 30% as the reaction temperature increased from $800^{\circ}C$ to $900^{\circ}C$.

Installation for Preparing of Nanopowders by Target Evaporation with Pulsed Electron Beam

  • Sokovnin S. Yu.;Kotov Yu. A.;Rhee C. K.
    • Journal of Powder Materials
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    • v.12 no.3
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    • pp.167-173
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    • 2005
  • Production of weakly agglomerated nanopowders with the characteristic size of about 10 nm and a narrow particle size distribution is still a topical problem especially if the matter is an acceptable output (>50 g/hour), a high purity of the final product, and a low (energy consumption. The available experience and literature data show that the most promising approach to production of such powders is the evaporation-condensation method, which has a set of means for heating of the target. From this viewpoint the use of pulsed electron accelerators for production of nanopowders is preferable since they allow a relatively simple adjustment of the energy, the pulse length, and the pulse repetition rate. The use of a pulsed electron accelerator provides the following opportunities: a high-purity product; only the target and the working gas will interact and their purity can be controlled; evaporation products will be removed from the irradiation zone between pulses; as a result, the electron energy will be used more efficiently; adjustment of the particle size distribution and the characteristic size of particles by changing the pulse energy and the irradiated area. Considering the obtained results, we developed a design and made an installation for production of nanopowders, which is based on a hollow-cathode pulsed gas-filled diode. The use of a hollow-cathode gas-filled diode allows producing and utilizing an electron beam in a single chamber. The emission modulation in the hollow cathode will allow forming an electron beam 5 to 100 ms long. This will ensure an exact selection of the beam energy. By now we have completed the design work, manufactured units, equipped the installation, and began putting the installation into operation. A small amount of nanopowders has been produced.

Evaluation of the Basic Property Evaluation of Eco-powder, a Hydrothermal Synthesis Product for Improving Waste Vinyl Recycling Efficiency (농촌 폐비닐 활용률 제고를 위한 수열합성 생성물인 에코 파우더(Eco-powder)의 기초물성 평가)

  • Sun-Mi Choi;Min-Chul Lee;Jin-Man Kim;Young-Gon Son;Nam-Ho Kim
    • Resources Recycling
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    • v.33 no.1
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    • pp.48-57
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    • 2024
  • This study aimed to improve utilization of the Class C vinyl waste generated in rural areas based on a preliminary investigation on the use of eco-powder, generated through pyrolysis, as a raw material for plastic. The efficiency of pre-processing treatments in controlling ash content of the generated eco-powder and its effect on the basic properties of manufactured plastic were evaluated. The basic properties included ash content of the compressed eco-powder at different levels of ash content, impact strength, flexural strength, and tensile strength. The experimental results confirmed that pre-processing improved the separation efficiency of soil particles and vinyl waste through physical impact. The eco-powder with ash content of less than or equal to 26% was found to satisfy the target performance during impact strength, flexural strength, and tensile strength evaluation. Thus, it was confirmed that the Class C vinyl waste, having low utilization and recovery rates, could be effectively utilized as a plastic raw material after optimum thermal treatment and physical processing using the eco-powder.

The strength characteristic of extruding solid according to substitution ratio and curing methods of waste concrete powder (폐콘크리트 미분말 대체율 및 양생방법에 따른 압출경화체의 강도특성)

  • Yu, Jae-Seong;Kim, Jin-Man;Lee, Myeong-Jin
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2015.11a
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    • pp.49-50
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    • 2015
  • Recently, by-products from concrete industry are generated in large quantities because of urban redevelopment. Accordingly, waste concrete powder(WCP) inevitably generated in the course of crushing, screening, and separating the waste concrete also show high emission and be increasing gradually, but which is mostly buried with waste concrete aggregate. This is a basic research to increase the value added utilization rate of WCP. We have examined strength characteristic of extruding panel with WCP, depending on the curing methods. The result of study shows similar strength to the base specimen in autoclave curing condition. And in autoclave curing condition, the specimen with WCP of 20% and 30% satisfy the target strength of 14MPa.

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Fundamental Properties of Cement Mortar with Waste Concrete Sludge (폐콘크리트 슬러지를 혼합 사용한 시멘트 모르터의 기초 특성)

  • Lee, Myeong-Jin;Lee, Ha-Na;Yu, Jae-Seong;Kim, Jin-Man
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2015.11a
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    • pp.160-161
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    • 2015
  • This research reviewed the characteristics of waste concrete sludge occurred from recycled aggregate producing process and the physical and mechanical properties of the mortar incorporated the pulverized the waste concrete sludge. From the results of the experiment, as the replacement ratio of waste concrete sludge powder was increased, the dosage of superplasticizer to satisfy the target flow of 200 ± 10 was increased, and the compressive and flexural strengths were decreased. On the other hand, when the sludge powder replacement ratio was 25 %, outstanding performance of general characteristics of mortar was obtained while it was lower than Plain mixture, thus, further detail study on various replacement ratios of waste concrete sludge powder is needed.

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