• 한국분말재료학회지
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• 제18권6호
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• pp.482-487
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• 2011

Alloy 617, Ni-22Cr-12Co-9Mo base oxide dispersion strengthened alloy was fabricated by using mechanical alloying, hot isostatic pressing and hot rolling. Uniaxial tensile tests were performed at room temperature and at $700^{\circ}C$. Compared with the conventional Alloy 617, ODS alloy showed much higher yield strength and tensile strength, but lower elongation. Fracture surfaces of the tensile tested specimens were investigated in order to find out the mechanism of fracture mode at each test temperature. Grain adjustment during tensile deformation was analyzed by electron backscattered diffraction mapping, inverse pole figures and TEM observation.

• Nuclear Engineering and Technology
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• 제46권6호
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• pp.857-862
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• 2014

Mechanical alloying under various gas atmospheres such as Ar, an Ar-$H_2$ mixture, and He gases were carried out, and its effects on the powder properties, microstructure and mechanical properties of ODS ferritic steels were investigated. Hot isostatic pressing and hot rolling processes were employed to consolidate the ODS steel plates. While the mechanical alloyed powder in He had a high oxygen concentration, a milling in Ar showed fine particle diameters with comparably low oxygen concentration. The microstructural observation revealed that low oxygen concentration contributed to the formation of fine grains and homogeneous oxide particle distribution by the Y-Ti-O complex oxides. A milling in Ar was sufficient to lower the oxygen concentration, and this led a high tensile strength and fracture elongation at a high temperature. It is concluded that the mechanical alloying atmosphere affects oxygen concentration as well as powder particle properties. This leads to a homogeneous grain and oxide particle distribution with excellent creep strength at high temperature.

• Journal of Advanced Marine Engineering and Technology
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• 제36권2호
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• pp.276-285
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• 2012

본 연구목적은 열간압연용 런-아웃 테이블 롤러 표면의 기계적 성질을 개선하기 위해 다공질 자용성 합금으로 피복하는 방법을 개발하는 것이다. 열간압연에서 런-아웃 테이블의 롤러 내구성을 높이기 위해서는 고온에서 롤러표면의 경도를 높게 유지해야 하고, 내마모성, 내식성, 내열성, 내소부성 및 내응착성의 향상을 유지하여야 한다. 또한, 고온의 열연 강판을 안정적으로 이송할 수 있도록 하기 위해서는 롤러표면에 적절한 마찰계수를 유지하도록 하여야 하고, 롤러와 강판 사이에 미끄럼 발생이 없어야 한다. 본 연구에서는 자용성 합금에 텅스텐카바이드를 첨가시켜 서메트화하여 롤러의 내마모성을 증대시켰고, 미세 철분말을 롤러표면에 피복하여 다공질을 만들어 마찰계수를 높이고 붙잡음성을 향상시켰다. 그 결과, Ni-Cr 피복 롤러에 비하여 다공질 자용성 합금 피복 롤러는 피복층에 철분이 5 ~ 10 wt%로 많이 함유되어 재용융 공정에서 전기로로 가열하여 일부분만 합금화되고 나머지는 산화 및 용해에 의해 탈락되어 다공질로 나타나 강판과의 붙잡음성을 향상시켰다.

• 한국분말재료학회지
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• 제21권4호
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• pp.271-276
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• 2014

15Cr-1Mo base oxide dispersion strengthened (ODS) steel which is considered to be as a promising candidate for high- temperature components in nuclear fusion and fission systems because of its excellent high temperature strength, corrosion and radiation resistance was fabricated by using mechanical alloying, hot isostatic pressing and hot rolling. Torsion tests were performed at room temperature, leading to two different shear strain routes in the forward and reverse directions. In this study, microstructure evolution of the ODS steel during simple shearing was investigated. Fine grained microstructure and a cell structure of dislocation with low angle boundaries were characterized with shear strain in the shear deformed region by electron backscattered diffraction (EBSD). Grain refinement with shear strain resulted in an increase in hardness. After the forward-reverse torsion, the hardness value was measured to be higher than that of the forward torsion only with an identical shear strain amount, suggesting that new dislocation cell structures inside the grain were generated, thus resulting in a larger strengthening of the steel.

• 한국분말재료학회지
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• 제18권5호
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• pp.456-462
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• 2011

Yttrium oxide is one of the most thermo-dynamically stable materials, so that it is generally used as a dispersoid in many kinds of dispersion strengthed alloys. In this study, a nickel-base superalloy is strengthened by dispersion of yttrium oxide particles. Elemental powders with the composition of Ni-22Cr-18Fe-9Mo were mechanically alloyed(M.A.) with 0.6 wt% $Y_2O_3$. The MA powders were then HIP(hot isotactic press)ed and hot rolled. Most oxide particles in Ni-22Cr-18Fe-9Mo base ODS alloy were found to be Y-Ti-O type. The oxide particles were uniformly dispersed in the matrix and also on the grain boundaries. Tensile test results show that the yield strength and ultimate tensile strength of ODS alloy specimens were 1.2~1.7 times higher than those of the conventional $Hastelloy^{TM}$ X(R), which has the same chemical compositions with ODS alloy specimens except the oxide particles.

• 한국분말재료학회지
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• 제28권2호
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• pp.110-119
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• 2021

In this study, the high-temperature oxidation properties of austenitic 316L stainless steel manufactured by laser powder bed fusion (LPBF) is investigated and compared with conventional 316L manufactured by hot rolling (HR). The initial microstructure of LPBF-SS316L exhibits a molten pool ~100 ㎛ in size and grains grown along the building direction. Isotropic grains (~35 ㎛) are detected in the HR-SS316L. In high-temperature oxidation tests performed at 700℃ and 900℃, LPBF-SS316L demonstrates slightly superior high-temperature oxidation resistance compared to HR-SS316L. After the initial oxidation at 700℃, shown as an increase in weight, almost no further oxidation is observed for both materials. At 900℃, the oxidation weight displays a parabolic trend and both materials exhibit similar behavior. However, at 1100℃, LPBF-SS316L oxidizes in a parabolic manner, but HR-SS316L shows a breakaway oxidation behavior. The oxide layers of LPBF-SS316L and HR-SS316L are mainly composed of Cr₂O₃, Fe-based oxides, and spinel phases. In LPBF-SS316L, a uniform Cr depletion region is observed, whereas a Cr depletion region appears at the grain boundary in HR-SS316L. It is evident from the results that the microstructure and the high-temperature oxidation characteristics and behavior are related.

• 한국분말재료학회지
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• 제10권1호
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• pp.15-20
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• 2003

Hybrid $A1_2O_3-TiC$ ceramic particle reinforced 6061 and 5083 Al composite powders were prepared by the combination of twin rolling and stone mill crushing process, followed by consolidating processes of cold compaction, degassing and hot extrusion. The composite bar consists of lamellar structure of ceramic particle rich area and matrix area, in which the hybrid was decomposed into each TiC of about $3-4\mutextrm{m}$ and $AI_2O_3$ particles of about $1-2\mutextrm{m}$ in diameter. It also found that fine $Mg_2Si$ precipitates of about 30 nm were embedded in the matrix, which have grains of about 3 $\mutextrm{m}$. Higher UTS was measured at the 5083 composite bar compared to the conventionally fabricated composite, due to again refinement effect by the rapid solidification. No particle was shown to form in the interface between the matrix and reinforcement, whereas carbon was diffused into the matrix.

• Composites Research
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• 제26권2호
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• pp.111-115
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• 2013

$C_{60}$ 풀러렌이 분산된 알루미늄기지 복합재를 볼 밀링법과 열간압연 공정을 이용하여 제조하였다. 볼 밀링이 진행되는 동안, 알루미늄기지는 그 결정립이 100 nm 이하 수준으로 미세화되어 강화되었다. 동시에 $C_{60}$ 풀러렌이 알루미늄기지 내에 균일하게 분산되어, $C_{60}$ 풀러렌의 첨가량이 증가할수록 복합재의 강도가 증가하였으며, 10 vol%의 $C_{60}$ 풀러렌을 포함하는 순 알루미늄기지 복합재는 1 GPa 수준의 압축 강도를 나타내었다.

• 한국분말재료학회지
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• 제27권4호
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• pp.311-317
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• 2020

In this study, the effects of Co content on the microstructure and Charpy impact properties of Fe-Cr-W ferritic/martensitic oxide dispersion strengthened (F/M ODS) steels are investigated. F/M ODS steels with 0-5 wt% Co are fabricated by mechanical alloying, followed by hot isostatic pressing, hot-rolling, and normalizing/tempering heat treatment. All the steels commonly exhibit two-phase microstructures consisting of ferrite and tempered martensite. The volume fraction of ferrite increases with the increase in the Co content, since the Co element considerably lowers the hardenability of the F/M ODS steel. Despite the lowest volume fraction of tempered martensite, the F/M ODS steel with 5 wt% Co shows the highest micro-Vickers hardness, owing to the solid solution-hardening effect of the alloyed Co. The high hardness of the steel improves the resistance to fracture initiation, thereby resulting in the enhanced fracture initiation energy in a Charpy impact test at - 40℃. Furthermore, the addition of Co suppresses the formation of coarse oxide inclusions in the F/M ODS steel, while simultaneously providing a high resistance to fracture propagation. Owing to these combined effects of Co, the Charpy impact energy of the F/M ODS steel increases gradually with the increase in the Co content.