• Title/Summary/Keyword: Mass standards

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Evaluation of low vacuum gauge using deadweight piston gauge (분동식압력계를 이용한 저진공게이지의 평가)

  • Woo, Sam-Yong;Choi, In-Mook;Song, Han-Wook;Kim, Boo-Shik
    • Journal of the Korean Vacuum Society
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    • v.16 no.4
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    • pp.244-249
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    • 2007
  • Deadweight piston gauge have been widely used as a fundamental instrument of precise pressure measurement because they are robust, accurate, potable, convenient to use and are able to realize the definition of pressure as farce per unit area. Basically, a deadweight piston gauge consists of a piston mounted vertically in a close-fitting cylinder filled with a gas and weights of known mass values. The pressure to be measured is applied to the base of the piston generating an upward vertical force, and is balanced by the downward gravitational force generated by weights. These instruments can be used to measure pressures above 10 kPa because of tare weights including piston. However, using a variable bell-jar pressure method and a newly developed weight loading device we can extend the application range of deadweight piston gauge to lower pressures. In this paper, we present the practical calibration results for two CDGs(Capacitance diaphragm gauge, MKS) with full-scale ranges of 1.33 kPa and 13.3 kPa, respectively.

Simultaneous Determination of Octylphenol, Nonylphenol and Bis(2-ethylhexyl)phthalate in Fish Samples Using Two Internal Standards (2가지 내부표준물질을 이용하여 어류시료 중 Octylphenol, Nonylphenol, Bis(2-ethylhexyl)phehalate의 동시정량)

  • Kim, Jong-Hun
    • Analytical Science and Technology
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    • v.14 no.3
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    • pp.244-252
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    • 2001
  • A comprehensive analytical method of endocrine distruptors[i.e., nonylphenol(NP), octylphenol(OP), bis(2-ethylhexyl)phthalate(BEHP)] is fish samples was developed using two internal standards. This method employed closed culture tube extraction with dichloromethane and solvent exchange to iso-hexane and SPE(2g) aminopropyl column, followed by determination on gas chromatograph linked to mass spectrometer(GC/MS) operated in the single ion monitoring(SIM) mode. The recoveries of nonylphenol and octyphenol in the range of $0.2{\sim}20{\mu}g/g$ using 1-phenyl decanol as one internal standard were over 75%, and recovery of bis(2-ethylhexyl)phthalate in the range of $0.4{\sim}40{\mu}g/g$ using bis(2-ethylbutyl)phthalate(BEBP) as the other internal standards was showed over 102%. The present method was applied to fish samples from Korea and UK. The range of concentrations for nonylphnol(NP) and bis(2-ethylhexyl)phthalate in Korean fish were $0.02{\sim}0.06{\mu}g/g$ in 2 samples and $0.18{\sim}2.03{\mu}g/g$ in 9 samples respectively, but bis(2-ethylhexyl)phthalate(BEHP) in UK samples was found $2.99{\mu}g/g$ in just 1 sample. But octylphenol(OP) was not dected in any samples by this method. This two internal standard method provides a more precise analytical tool to investigate endocrine disruptors in a biological matrices of limited quantity.

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Free Speech and the Void for Vagueness Doctrine: A Comparative Analysis of Free Speech Cases in the Korea Consitutional Court and the United States Supreme Court (표현의 자유와 "명확성 원칙": 한국 헌법재판소와 미국 연방대법원의 판례 비교연구)

  • Chang, Ho-Soon
    • Korean journal of communication and information
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    • v.55
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    • pp.5-32
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    • 2011
  • This paper is a comparative analysis of constitutional decisions in which the Korea Consitutional Court and the United States Supreme Court applied the void for vagueness doctrine into free expression issues. Common aspects are: both courts applied the void for vagueness doctrine on the grounds that vague laws bring chilling effect on freedom of expression. Acknowledging inevitable uncertainties in lawmaking and legal jargons, however, both courts required minimum standards in the void for vagueness doctrine. In the cases where unclear legal meanings resulted in constitutional challenges, both courts adopted the "narrowing construction" by the courts or judges based on average/ordinary person's understanding. The biggest differences between the two constitutional courts are their approach to the degrees of vagueness allowed in free expression cases. The U.S. Supreme Court underscored the necessity of narrowly drawn, reasonable and definite standards. Meanwhile, the Korea Constitutional Court relaxed its standards in some cases such as the National Security Law cases, even though it admitted the possibility of curtailing the right to free expression. The Court reasoned that those laws, though vague, brought with bigger social interests and are necessary tools in dealing with changing world.

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Quantitative Determination of Psoralen and Angelicin from Some Medicinal Herbs by High Performance Liquid Chromatography

  • Dong, Nguyen-Thanh;Bae, Ki-Hwan;Kim, Young-Ho;Hwang, Gwi-Seo;Heo, Ok-Soon;Kim, Se-Eun;Kang, Jong-Seong
    • Archives of Pharmacal Research
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    • v.26 no.7
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    • pp.516-520
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    • 2003
  • A reversed-phase high performance liquid chromatographic method was developed to determine the contents of psoralen and angelicin from some medicinal herbs. The optimum eluent for chromatography was 20 v/v% acetonitrile in water on a Zorbax 300SB $C_{18}$ column. The identification was carried out by comparing the retention time and mass spectra of the relevant peaks with their standards. The variation of the concentration of psoralen and angelicin was wide between different species. The seeds of Psoralea corylifolia showed the highest contents of psoralen (7.8 mg/g) and angelicin (2.3 mg/g) among the tested herbs.

Determining the Priority of Investment for Remedial Works of Slopes (사면관리를 위한 재원의 투자 우선 순위 평가)

  • 김상규;류지협;구호본;정하익;윤수호
    • Proceedings of the Korean Geotechical Society Conference
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    • 1999.03a
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    • pp.269-276
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    • 1999
  • The program ESRAS Ver 0.5 that can assess the risk of slopes by means of fuzzy inference is developed in this paper. The results of assessment involve the degree of stability of slopes, the possible travel distance of the soil mass being failed, and anticipated loss of life and properties. With this program, vulnerable slopes can be managed most effectively and the fuzzy inference is used to express quantitatively the judgement of an expert and the uncertainty of slope stability. The fuzzy rule base is composed of an evaluation list for slope stability together with the experience of an expert. This program has been examined for 88 slopes which have been failed or shown a possibility of failure. With this examination, the standards to assess the stability of slopes can be presented and it is proven that this is particularly useful in determining the priority of investment for remedial works of slopes.

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Environmental Management towards Sustainable Urban Development of Chongju City (지속가능한 도시개발을 위한 환경관리방안의 모색 - 청주시를 중심으로 -)

  • Lee, Jong-Ho
    • Journal of Environmental Impact Assessment
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    • v.4 no.2
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    • pp.131-149
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    • 1995
  • The object of this study is to suggest some alternatives for environmental management towards sustainable urban development of Chongju city in Korea. This study analyses urban environmental indicators (population density, land use, road, park, car, etc.), level of air and water pollution and solids waste generation by comparing Chongju city and other large cities. Some alternatives towards sustainable development in Chongju city would be summerized and suggested as higher concentrated land use(compact city), mixed land use, supply of mass transit, establishment of regional environmental standards, total emission regulation of air and water pollutants, the preparation of Local Agenda21 of Chongju, and the introduction of strategic environmental assessment(SEA) into environmental impact assessment.

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Analysis on Activation Energy Measurement and Application of Nuclear Equipment Non-metallic Materials (원전기기 비금속재료의 활성화에너지 측정 및 적용성 분석)

  • Bhang, Keug-Jin;Hong, Jun-Hee
    • Journal of Power System Engineering
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    • v.20 no.4
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    • pp.38-43
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    • 2016
  • Safety-related equipments of Nuclear Power Plants(NPP) have to perform environmental qualification test in accordance with IEEE-323 standards. However, non-metallic materials replace new one regularly instead of the test because they are considered as consumable parts. In this study, the seven kinds of non-metallic materials are selected and their activation energy was experimentally evaluated with uncertainty analysis by using thermogravimetric analyzer(TGA). In order to obtain activation energy of non-metallic materials, mass difference, temperature raising rate and conversion rate on the specimen are analyzed. It is postulated that the three experiment conditions are important to get a reliable activation energy. This postulate was experimentally confirmed using Arrhenius equation and Flynn-Wall-Ozawa analysis.

Laser Welding Application in Car Body Manufacturing

  • Shin, H.O.;Chang, I.S.;Jung, C.H.
    • International Journal of Korean Welding Society
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    • v.3 no.1
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    • pp.2-7
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    • 2003
  • Laser welding application for car body manufacturing has many advantages in the stiffness and the lightness of vehicle, the productivity of assembly line, and the degree of freedom in design. This presentation will express the innovation of car body manufacturing including parameter optimization, process modeling, and system integration. In this application the investment for systems was cut down dramatically by real time switching over the laser path between two welding stations. Points of technical discussion are as follows; optimization of parameters such as laser power, robot speed and trajectory, compact and useful design of jig & fixture to assure welding quality for 3 sheet-layer zinc-coated steel, system integration between 4㎾ Nd:YAG laser device and the other systems, on-line real time welding quality monitoring system, perfect safety standards for high power laser, minimization of consumption costs such as arc lamp, protective glass for optic, etc. This application was successfully launched mass production line in 2001. The laser-welded line of side panel consists of 122 stitches totally. And the length is about 2.4m.

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A Study on the Development of Child Human Model for Crashworthiness Analysis (충돌해석용 유아 인체모델 개발에 관한 연구)

  • Kim Heon Young;Kim Sang Bum;Kim Joon Sik;Lee In Hyeok;Lee Jin Hee
    • Journal of the Korean Society for Precision Engineering
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    • v.21 no.12
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    • pp.182-191
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    • 2004
  • This study is focused on the development of a child human model, which is composed of skin, skeleton, joints and muscle, etc. The dimension of child outer skin is referred to anthropometric data from KRISS (Korea Research Institute of Standards and Science). The positions of joint and mass properties of body segments are calculated from ATB(Articulated Total Body) program, GEBOD. The properties of bones and muscles are obtained by the way of scaling from adult human model. To verify the developed human model, ROM simulation and sled test is conducted. Developed human model can be effectively applied to the evaluation of human injury in crash situation and development of child restraint system. The explicit finite element program $PAM-CRASH^TM$ was used to simulate six-year old child human model.

Determination of Trace Elements in Atmospheric Dust by X-Ray Fluorescence Spectrometry(II) : X-ray Fluorescence Spectrometric Determination of Light Elements (형광 X선에 의한 대기분진중의 미량성분의 측정(II): 대기부유분진 중 경원소의 X-선 형광분석)

  • 이용근;박현미;이동수;이보경
    • Journal of Korean Society for Atmospheric Environment
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    • v.9 no.3
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    • pp.247-254
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    • 1993
  • A simple and direct method is developed for the determination of light Elements in atmospheric particulates by X-ray fluorescence spectrometry. Calibration standards for the light elements such as Al, Mg, K, Ca, etc are prepared by filtering real atmospheric particulates over variable time and subsequently standardizing them by Inductively Coupled Plasma-Mass Spectrometry(ICP-MS) or Atomic Absorption Spectrophotometry(AAS) analysis. The validity of this calibration method is tested by analyzing more than 100 aerosol samples, collected at urban(Seoul) and rural(Padori) sites over a two year period with this method and then comparing them with those by other accuracy proven methods such as AAS or ICP-MS: for all metals tested the results showed reasonably good agreements (R $\geq$ 0.95).

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