• Title/Summary/Keyword: Liquid pressing infiltration

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Development of Carbon Nanofiber Reinforced Cu Matrix Composites Using Liquid Pressing Process (액상 성형 가압법을 이용한 탄소나노섬유 강화 Cu 기지 나노 복합재료 개발)

  • 이상관;김두현;엄문광;하동호;김상식
    • Proceedings of the Korean Society For Composite Materials Conference
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    • 2003.10a
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    • pp.50-53
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    • 2003
  • Carbon nannofiber reinforced Cu matrix composite has potential applications for electrically conducting materials having high strength and electrical conductivity. In this study, we have developed fabrication technology of the nanocomposites using a liquid pressing process. The process is to use the low pressure for infiltration of Cu melt into carbon nanofiber mat as the Cu melt is pressurized directly. The minimum pressure required for infiltration was calculated from force balance equation, permeability measurement and compaction behavior of carbon nanofiber. Also, the melting temperature and the holding time have been optimized.

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Prevention of Grain Growth during the Liquid-Phase Assisted Sintering of β-SiC (액상소결 시의 β-SiC의 입자성장 방지)

  • Gil, Gun-Young;Noviyanto, Alfian;Han, Young-Hwan;Yoon, Dang-Hyok
    • Journal of the Korean Ceramic Society
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    • v.47 no.6
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    • pp.485-490
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    • 2010
  • In our previous studies, continuous SiC fiber-reinforced SiC-matrix composites ($SiC_f$/SiC) had been fabricated by two different slurry infiltration methods: vacuum infiltration and electrophoretic deposition (EPD). 12 wt% of $Al_2O_3-Y_2O_3$-MgO with respect to SiC powder was used as additives for liquid-phase assisted sintering. After hot pressing at $1750^{\circ}C$ under 20 MPa for 2 h in Ar atmosphere, a high composite density could be achieved for both cases, whereas the problems such as large grain size and non-uniform distribution of liquid phase were observed, which was resulted in the relatively poor mechanical properties of composites. Therefore, efforts have been made to reduce the grain growth during the sintering, including the optimization for hot pressing condition and utilization of spark plasma sintering using a SiC monolith. Based on the results, spark plasma sintering was found to be effective method in decreasing the amount of sintering additive, time and grain growth, which will be explained in comparison to the results of hot pressing in this paper.

Corrosion Behaviors of TiC Ceramic Particulate Reinforced Steel Composites Fabricated by Liquid Pressing Infiltration Process in Salt Water Environment (용융가압함침공정으로 제조된 TiC 세라믹 입자 강화 철강복합재의 염수환경에서의 부식 특성)

  • Lee, Yeong-Hwan;Ko, Seongmin;Shin, Sangmin;Cho, Seungchan;Kim, Yangdo;Kim, Junghwan;Lee, Sang-Kwan;Lee, Sang-Bok
    • Composites Research
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    • v.33 no.5
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    • pp.251-255
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    • 2020
  • In this study, TiC ceramic particulate reinforced steel composites was fabricated using a liquid pressing infiltration process. Studies were conducted on microstructure analysis and basic physical properties such as hardness and corrosion characteristics in salt water environment for comparison with commercial nodular cast iron. As a result of comparison of corrosion characteristics in a salt water environment, both corrosion potential and corrosion current density were lower than that of ductile graphite cast iron. The lower calculated corrosion rate confirms that the TiC-Fe metal composite has superior corrosion resistance than the cast iron.

Microstructure and Wear Characteristics of TiC-SKD11 Composite Fabricated by Liquid Pressing Infiltration Process (용융가압함침 공정으로 제조한 TiC-SKD11 복합재료의 미세조직 및 내마모 특성)

  • Cho, Seungchan;Jo, Ilguk;Lee, Sang-Kwan;Lee, Sang-Bok
    • Composites Research
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    • v.30 no.3
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    • pp.209-214
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    • 2017
  • Titanium carbide (TiC) reinforced SKD11 matrix composites were successfully fabricated by a novel liquid pressing infiltration process. Microstructure, mechanical properties, and wear characteristics of the fabricated 60 vol% TiC-SKD11 composite are analyzed. The composite exhibits superior mechanical properties, such as hardness and compressive strength with 24% lower density as compared with SKD11. Improved wear resistance of the TiC-SKD11 composite originates from uniformly reinforced TiC having strong interfacial bonding strength between TiC/SKD11 interface.

Microstructure and Properties of TiC-Inconel 718 Metal Matrix Composites Fabricated by Liquid Pressing Infiltration Process (용융가압함침 공정으로 제조된 고체적률 TiC-Inconel 718 금속복합재료의 미세조직 및 특성)

  • Cho, Seungchan;Lee, Yeong-Hwan;Ko, Seongmin;Park, Hyeonjae;Lee, Donghyun;Shin, Sangmin;Jo, Ilguk;Lee, Sang-Bok;Lee, Sang-Kwan
    • Composites Research
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    • v.32 no.3
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    • pp.158-162
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    • 2019
  • Titanium carbide (TiC) reinforced Inconel 718 matrix composites were successfully fabricated by a novel liquid pressing infiltration process. Microstructure and mechanical properties of the fabricated 55 vol% TiC-Inconel 718 composite are analyzed. The composite exhibits superior mechanical properties, such as hardness and compressive strength as compared with Inconel 718. It is believed that Mo and Nb, which are alloying elements in the matrix, diffuse and solidify into the TiC reinforcement, resulting in generation of core-rim structure with excellent interfacial properties.

Fabrication of Ceramic Particulate Reinforced Steel Composites by Liquid Pressing Infiltration Process (용융가압함침공정을 이용한 세라믹 입자 강화 철강복합재료의 제조성 검증)

  • Cho, Seungchan;Lee, Yeong-Hwan;Ko, Seongmin;Park, Hyeon Jae;Lee, Donghyun;Shin, Sangmin;Jo, Ilguk;Lee, Sang-Kwan;Lee, Sang-Bok
    • Composites Research
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    • v.31 no.4
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    • pp.117-121
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    • 2018
  • Various ceramic particulate such as TiC, $TiB_2$, $Al_2O_3$ reinforced SUS431 matrix composites were successfully fabricated by a novel liquid pressing infiltration process. Microstructures of the SUS431 composite were analyzed to determine manufacturability of composites. $Al_2O_3$-SUS431 composite had lots of defects due to poor wettability between the $Al_2O_3$ and steel matrix. On the other hand, TiC was uniformly dispersed in the SUS431 matrix than $TiB_2$ and $Al_2O_3$ due to good wettability and interfacial properties.

Quasi-Static and Dynamic Deformation Behavior of STS304- and Ta-fiber-reinforced Zr-based Amorphous Matrix Composites Fabricated by Liquid Pressing Process (액상가압공정으로 제조된 STS304와 Ta 섬유 강화 Zr계 비정질 복합재료의 준정적 및 동적 변형거동)

  • Kim, Yongjin;Shin, Sang Yong;Kim, Jin Sung;Huh, Hoon;Kim, Ki Jong;Lee, Sunghak
    • Korean Journal of Metals and Materials
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    • v.48 no.6
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    • pp.477-488
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    • 2010
  • Zr-based amorphous alloy matrix composites reinforced with stainless steel (STS) and tantalum continuous fibers were fabricated without pores or defects by a liquid pressing process, and their quasi-static and dynamic deformation behaviors were investigated by using a universal testing machine and a Split Hopkinson pressure bar, respectively. The quasi-static compressive test results indicated that the fiberreinforced composites showed amaximum strength of about 1050~1300 MPa, and its strength maintained over 700 MPa until reaching astrain of 40%. Under dynamic loading, the maximum stresses of the composites were considerably higher than those under quasi-static loading because of the strain-rate hardening effect, whereas the fracture strains were considerably lower than those under quasi-static loading because of the decreased resistance to fracture. The STS-fiber-reinforced composite showed a greater compressive strength and ductility under dynamic loading than the tantalum-fiber-reinforced composite because of the excellent resistance to fracture of STS fibers.

Microstructure and Mechanical Properties of Amorphous Matrix Composite Reinforced with Tungsten Porous Foam (텅스텐 다공성폼 강화 Zr계 비정질 기지 복합재료의 미세조직과 기계적 성질)

  • Son, Chang-Young;Lee, Sang-Bok;Lee, Sang-Kwan;Kim, Choongnyun Paul;Lee, Sunghak
    • Korean Journal of Metals and Materials
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    • v.48 no.2
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    • pp.109-115
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    • 2010
  • In the present study, a Zr-based amorphous alloy matrix composite reinforced with tungsten porous foam was fabricated without pores or defects by liquid pressing process, and its microstructures and mechanical properties were investigated. About 69 vol.% of tungsten foam was homogeneously distributed inside the amorphous matrix, although the matrix of the composite contained a small amount of crystalline phases. The compressive test results indicate that the composite was not fractured at one time after reaching the maximum compressive strength, but showed considerable plastic strain as the compressive load was sustained by tungsten foam. The tungsten foam greatly improved the strength (2764 MPa) and ductility (39.4%) of the composite by homogeneously dispersing the stress applied to the matrix. This was because the tungsten foam and matrix were simultaneously deformed without showing anisotropic deformation due to the excellent bonding of tungsten/matrix interfaces. These findings suggest that the liquid pressing process is useful for the development of amorphous matrix composites with improved strength and ductility.

Thin Plate Fabrication and Characterization of Plain Woven Carbon / 6061 Al Composites (Plain woven carbon/6061Al 금속복합재료의 제조와 특성분석)

  • Chang Jae-Jun;Ha Dong-Ho;Eom Mun-Gwang;Lee Sang-kwan
    • Proceedings of the Korean Society For Composite Materials Conference
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    • 2004.04a
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    • pp.250-253
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    • 2004
  • Emphasis has been placed on thin plate fabrication of plain woven carbon fabric reinforced Al matrix composites using liquid pressing process. The composite has potential applications for PDP rear plate. The process is to use the low pressure for infiltration of Al melt into plain woven carbon fabric as the Al melt is pressurized directly. The minimum pressure required for the infiltration was calculated from force balance equation, permeability measurements and compaction behavior of carbon fiber. Also, the melting temperature and the holding time have been optimized. In order to measure coefficient of thermal expansion (CTE) of the composites, the thermal strain measurement using strain gage was performed and the thermal conductivity of the composites was measured using laser flash method. The constituent materials of the composite are PAN type carbon fibers as reinforcements and 6061 Al alloys as matrices.

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Microstructure and Mechanical Property Changes of Unidirectional and Plain Woven CF/Mg Composite Laminates after Corrosion (일방향 및 평직 CF/Mg 복합재 적층판의 부식에 따른 미세조직 및 기계적 특성 변화)

  • Yim, Shi On;Lee, Jung Moo;Lee, Sang Kwan;Park, Yong Ho;Park, Ik Min
    • Korean Journal of Metals and Materials
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    • v.50 no.9
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    • pp.697-702
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    • 2012
  • In this study, unidirectional and plain woven carbon fiber reinforced magnesium matrix composite laminates were fabricated by the liquid pressing infiltration process, and evolutions of the microstructure and compressive strength of the composite laminates under corrosion were investigated by static immersion tests. In the case of the unidirectional composite laminate, the main microstructural damage during immersion appeared as a form of corrosion induced cracks, which were formed at both CF/Mg interfaces and the interfaces between layers. On the otherhand, wrap/fill interface cracks were mainly formed in the plain woven composite laminate, without any cracks at the CF/Mg interface. The formation of these cracks was considered to be associated with internal thermal residual stress, which was generated during cooling after the fabrication process of these materials. As a consequence of the corrosion induced cracks, the thickness of both laminates increased in directions vertical to the fibers with increasing immersion time. With increasing immersion time, the compressive strengths of both composite laminates also decreased continuously. It was found that the plain woven composite laminates have superior corrosion resistance and stability under a corrosive condition than unidirectional laminates.