• 제목/요약/키워드: Liquid pressing infiltration

검색결과 11건 처리시간 0.022초

액상 성형 가압법을 이용한 탄소나노섬유 강화 Cu 기지 나노 복합재료 개발 (Development of Carbon Nanofiber Reinforced Cu Matrix Composites Using Liquid Pressing Process)

  • 이상관;김두현;엄문광;하동호;김상식
    • 한국복합재료학회:학술대회논문집
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    • 한국복합재료학회 2003년도 추계학술발표대회 논문집
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    • pp.50-53
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    • 2003
  • Carbon nannofiber reinforced Cu matrix composite has potential applications for electrically conducting materials having high strength and electrical conductivity. In this study, we have developed fabrication technology of the nanocomposites using a liquid pressing process. The process is to use the low pressure for infiltration of Cu melt into carbon nanofiber mat as the Cu melt is pressurized directly. The minimum pressure required for infiltration was calculated from force balance equation, permeability measurement and compaction behavior of carbon nanofiber. Also, the melting temperature and the holding time have been optimized.

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액상소결 시의 β-SiC의 입자성장 방지 (Prevention of Grain Growth during the Liquid-Phase Assisted Sintering of β-SiC)

  • 길건영;노비얀토 알피안;한영환;윤당혁
    • 한국세라믹학회지
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    • 제47권6호
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    • pp.485-490
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    • 2010
  • In our previous studies, continuous SiC fiber-reinforced SiC-matrix composites ($SiC_f$/SiC) had been fabricated by two different slurry infiltration methods: vacuum infiltration and electrophoretic deposition (EPD). 12 wt% of $Al_2O_3-Y_2O_3$-MgO with respect to SiC powder was used as additives for liquid-phase assisted sintering. After hot pressing at $1750^{\circ}C$ under 20 MPa for 2 h in Ar atmosphere, a high composite density could be achieved for both cases, whereas the problems such as large grain size and non-uniform distribution of liquid phase were observed, which was resulted in the relatively poor mechanical properties of composites. Therefore, efforts have been made to reduce the grain growth during the sintering, including the optimization for hot pressing condition and utilization of spark plasma sintering using a SiC monolith. Based on the results, spark plasma sintering was found to be effective method in decreasing the amount of sintering additive, time and grain growth, which will be explained in comparison to the results of hot pressing in this paper.

용융가압함침공정으로 제조된 TiC 세라믹 입자 강화 철강복합재의 염수환경에서의 부식 특성 (Corrosion Behaviors of TiC Ceramic Particulate Reinforced Steel Composites Fabricated by Liquid Pressing Infiltration Process in Salt Water Environment)

  • 이영환;고성민;신상민;조승찬;김양도;김정환;이상관;이상복
    • Composites Research
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    • 제33권5호
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    • pp.251-255
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    • 2020
  • 본 연구에서는 용융가압함침공정을 이용하여 제조된 TiC 세라믹 입자강화 철강복합재를 제조하고 상용구상흑연주철과 비교를 위하여 미세조직 분석 및 경도 등 기초물성과 선박 해양 분야등의 적용가능성 검토를 위하여 염수환경에서의 부식 특성에 관한 연구를 진행하였다. 염수환경에서의 부식특성 비교 결과 구상흑연주철 대비 부식전위와 부식전류밀도 모두 낮은 값을 나타내었고, 낮은 연간부식률을 통하여 TiC-Fe 금속복합재의 내식성이 더 뛰어난 것을 확인하였다.

용융가압함침 공정으로 제조한 TiC-SKD11 복합재료의 미세조직 및 내마모 특성 (Microstructure and Wear Characteristics of TiC-SKD11 Composite Fabricated by Liquid Pressing Infiltration Process)

  • 조승찬;조일국;이상관;이상복
    • Composites Research
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    • 제30권3호
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    • pp.209-214
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    • 2017
  • 본 연구에서는 용융가압함침 공정을 통해 고체적율의 TiC 입자가 균일 분산된 SKD11 금속복합재료를 제조하고, 미제조직, 기계적 특성 및 내마모 특성에 대해 분석하였다. 약 60 vol%의 TiC가 균일하게 분산된 TiC-SKD11 복합재료를 제조함으로써 SKD11 대비 약 24% 경량화에 성공하였고 경도 및 압축항복강도는 증가하였다. 내마모 시험 결과 복합소재의 우수한 내마모 특성을 확인하였으며, 이는 높은 경도를 가지는 TiC 입자가 SKD11 기지와 강한 계면 결합력을 가지면서 높은 체적율로 존재함으로 인한 분산강화 효과와 TiC에 의한 SKD11의 산화 억제가 원인으로 판단된다.

용융가압함침 공정으로 제조된 고체적률 TiC-Inconel 718 금속복합재료의 미세조직 및 특성 (Microstructure and Properties of TiC-Inconel 718 Metal Matrix Composites Fabricated by Liquid Pressing Infiltration Process)

  • 조승찬;이영환;고성민;박현재;이동현;신상민;조일국;이상복;이상관
    • Composites Research
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    • 제32권3호
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    • pp.158-162
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    • 2019
  • 본 연구에서는 용융가압함침 공정을 이용하여 고체적률의 TiC 입자가 균일 분산된 Inconel 718 금속복합재료를 제조하고, 미세조직 및 기계적 특성을 분석하였다. 약 55 vol%의 TiC가 균일하게 분산된 TiC-Inconel 718 복합재료를 제조함으로써 Inconel 718 대비 우수한 경도 및 압축강도 특성을 나타내었으며, 이는 기지에 고용된 합금원소인 Mo 및 Nb이 TiC 강화재 내부로 확산 고용되어 우수한 계면 특성을 가지는 core-rim 구조의 TiC 형성에 의한 것으로 판단된다.

용융가압함침공정을 이용한 세라믹 입자 강화 철강복합재료의 제조성 검증 (Fabrication of Ceramic Particulate Reinforced Steel Composites by Liquid Pressing Infiltration Process)

  • 조승찬;이영환;고성민;박현재;이동현;신상민;조일국;이상관;이상복
    • Composites Research
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    • 제31권4호
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    • pp.117-121
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    • 2018
  • 본 연구에서는 용융가압함침 공정을 이용하여 TiC, $TiB_2$, $Al_2O_3$ 세라믹 입자가 분산된 SUS431 금속복합재료를 제조하고 미세조직을 분석하여 세라믹 입자에 따른 제조성에 대해 검토하였다. 젖음성이 나쁜 $Al_2O_3$의 경우 내부에 결함이 다수 존재함을 알 수 있었으며, $TiB_2$ 및 TiC 입자 강화 복합재의 경우 상대적으로 결함이 적고 강화재가 균일 분산되었음을 확인하였다. 특히, TiC-SUS431 복합재료의 경우 TiC와 Fe계 기지합금의 우수한 젖음성 및 용융가압함침공정 적용으로 우수한 계면 특성을 가지며 결함이 적고 균일한 미세조직을 가지는 것을 확인하였다.

액상가압공정으로 제조된 STS304와 Ta 섬유 강화 Zr계 비정질 복합재료의 준정적 및 동적 변형거동 (Quasi-Static and Dynamic Deformation Behavior of STS304- and Ta-fiber-reinforced Zr-based Amorphous Matrix Composites Fabricated by Liquid Pressing Process)

  • 김용진;신상용;김진성;허훈;김기종;이성학
    • 대한금속재료학회지
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    • 제48권6호
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    • pp.477-488
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    • 2010
  • Zr-based amorphous alloy matrix composites reinforced with stainless steel (STS) and tantalum continuous fibers were fabricated without pores or defects by a liquid pressing process, and their quasi-static and dynamic deformation behaviors were investigated by using a universal testing machine and a Split Hopkinson pressure bar, respectively. The quasi-static compressive test results indicated that the fiberreinforced composites showed amaximum strength of about 1050~1300 MPa, and its strength maintained over 700 MPa until reaching astrain of 40%. Under dynamic loading, the maximum stresses of the composites were considerably higher than those under quasi-static loading because of the strain-rate hardening effect, whereas the fracture strains were considerably lower than those under quasi-static loading because of the decreased resistance to fracture. The STS-fiber-reinforced composite showed a greater compressive strength and ductility under dynamic loading than the tantalum-fiber-reinforced composite because of the excellent resistance to fracture of STS fibers.

텅스텐 다공성폼 강화 Zr계 비정질 기지 복합재료의 미세조직과 기계적 성질 (Microstructure and Mechanical Properties of Amorphous Matrix Composite Reinforced with Tungsten Porous Foam)

  • 손창영;이상복;이상관;김충년;이성학
    • 대한금속재료학회지
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    • 제48권2호
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    • pp.109-115
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    • 2010
  • In the present study, a Zr-based amorphous alloy matrix composite reinforced with tungsten porous foam was fabricated without pores or defects by liquid pressing process, and its microstructures and mechanical properties were investigated. About 69 vol.% of tungsten foam was homogeneously distributed inside the amorphous matrix, although the matrix of the composite contained a small amount of crystalline phases. The compressive test results indicate that the composite was not fractured at one time after reaching the maximum compressive strength, but showed considerable plastic strain as the compressive load was sustained by tungsten foam. The tungsten foam greatly improved the strength (2764 MPa) and ductility (39.4%) of the composite by homogeneously dispersing the stress applied to the matrix. This was because the tungsten foam and matrix were simultaneously deformed without showing anisotropic deformation due to the excellent bonding of tungsten/matrix interfaces. These findings suggest that the liquid pressing process is useful for the development of amorphous matrix composites with improved strength and ductility.

Plain woven carbon/6061Al 금속복합재료의 제조와 특성분석 (Thin Plate Fabrication and Characterization of Plain Woven Carbon / 6061 Al Composites)

  • 장재준;하동호;엄문광;이상관
    • 한국복합재료학회:학술대회논문집
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    • 한국복합재료학회 2004년도 춘계학술발표대회 논문집
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    • pp.250-253
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    • 2004
  • Emphasis has been placed on thin plate fabrication of plain woven carbon fabric reinforced Al matrix composites using liquid pressing process. The composite has potential applications for PDP rear plate. The process is to use the low pressure for infiltration of Al melt into plain woven carbon fabric as the Al melt is pressurized directly. The minimum pressure required for the infiltration was calculated from force balance equation, permeability measurements and compaction behavior of carbon fiber. Also, the melting temperature and the holding time have been optimized. In order to measure coefficient of thermal expansion (CTE) of the composites, the thermal strain measurement using strain gage was performed and the thermal conductivity of the composites was measured using laser flash method. The constituent materials of the composite are PAN type carbon fibers as reinforcements and 6061 Al alloys as matrices.

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일방향 및 평직 CF/Mg 복합재 적층판의 부식에 따른 미세조직 및 기계적 특성 변화 (Microstructure and Mechanical Property Changes of Unidirectional and Plain Woven CF/Mg Composite Laminates after Corrosion)

  • 임시온;이정무;이상관;박용호;박익민
    • 대한금속재료학회지
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    • 제50권9호
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    • pp.697-702
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    • 2012
  • In this study, unidirectional and plain woven carbon fiber reinforced magnesium matrix composite laminates were fabricated by the liquid pressing infiltration process, and evolutions of the microstructure and compressive strength of the composite laminates under corrosion were investigated by static immersion tests. In the case of the unidirectional composite laminate, the main microstructural damage during immersion appeared as a form of corrosion induced cracks, which were formed at both CF/Mg interfaces and the interfaces between layers. On the otherhand, wrap/fill interface cracks were mainly formed in the plain woven composite laminate, without any cracks at the CF/Mg interface. The formation of these cracks was considered to be associated with internal thermal residual stress, which was generated during cooling after the fabrication process of these materials. As a consequence of the corrosion induced cracks, the thickness of both laminates increased in directions vertical to the fibers with increasing immersion time. With increasing immersion time, the compressive strengths of both composite laminates also decreased continuously. It was found that the plain woven composite laminates have superior corrosion resistance and stability under a corrosive condition than unidirectional laminates.