• 제목/요약/키워드: FE analysis method

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Determination of trace elements in food reference materials by instrumental neutron activation analysis

  • Cho, K.H.;Zeisler, R.;Park, K.W.
    • 분석과학
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    • 제18권6호
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    • pp.520-528
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    • 2005
  • Two biological Certified Reference Materials (CRMs), KRISS 108-04-001 (oyster tissue) and 108-05-001 (water dropwort stem), were prepared by Korea Research Institute of Standards and Science (KRISS)during FY '01. The certified values of these materials had been determined by Isotope Dilution Mass Spectrometry (IDMS) for six elements (Cd, Cr, Cu, Fe, Pb and Zn). Additional analytical works are now progressing to certify the concentrations of a number of the environmental and nutrimental elements in these CRMs. The certified values in a CRM are usually determined by using a single primary method with confirmation by other method(s) or using two independent critically-evaluated methods. Instrumental Neutron Activation Analysis (INAA) plays an important role in the determination of certified values as it can eliminate the possibility of common error sources resulting from sample dissolution. In this study INAA procedure was used in determination of 23 elements in these two biological CRMs to acquire the concentration information and the results were compared with KRISS certified values.

용탕유동과 응고를 고려한 주조공정의 유한요소해석

  • 윤석일;김용환
    • 한국정밀공학회:학술대회논문집
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    • 한국정밀공학회 1995년도 춘계학술대회 논문집
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    • pp.620-625
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    • 1995
  • Finite element analysis tool was developed to analyze the casting process. Generally, casting processes consists of mold filling and solifification. In order to investigate the effects of process variables and to predict the defects, both filling and solidiffication process were simulated simultaneously. At filling process, especiallywe consider thermal coupling to investigate thermal history of material during the filling stage. And thermal condition at the final stage of filling is used as the initial conditions in a solidification process for the exact simulation of the actual casting processes. At mold filling process, Lagrangian-type finite element method with automatic remashing scheme was used to find the material flow. To avoid numerical instability in low viscous fluid, a perturbation method with artificial viscosity is adopted. At solififfication process, enthalpy-based finite element method was used to solve the heat transfer problem with phase change. And elastic stress analysis has been performed to predict the thermal residual stress. Through the FE analysis, solidiffication time, position of solidus line, liquidus line and thermal residual stress are studied. Finite element tools developed in this study will be used process design of casting process and maybe basic structure for total CAE system of castigs which will be constructed afterward.

대형구조물의 효율적 3차원 용접잔류응력해석을 위한 새로운 이동 온도 프로파일 방법 (Moving Temperature Profile Method for Efficient Three-Dimensional Finite Element Welding Residual Stress Analysis for Large Structures)

  • 김철호;김재민;김윤재
    • 한국압력기기공학회 논문집
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    • 제19권2호
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    • pp.75-83
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    • 2023
  • For three-dimensional finite element welding residual stress simulation, several methods are available. Two widely used methods are the moving heat source model using heat flux and the temperature boundary condition model using the temperature profile of the welded beads. However, each model has pros and cons in terms of calculation times and difficulties in determining welding parameters. In this paper, a new method using the moving temperature profile model is proposed to perform efficiently 3-D FE welding residual stress analysis for large structures. Comparison with existing experimental residual stress measurement data of two-pass welding pipe and SNL(Sandia National Laboratories) mock-up canister shows the accuracy and efficiency of the proposed method.

Stress evaluation method of reinforced wall-thinned Class 2/3 nuclear pipes for structural integrity assessment

  • Jae-Yoon Kim;Je-Hoon Jang;Jin-Ha Hwang;Yun-Jae Kim
    • Nuclear Engineering and Technology
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    • 제56권4호
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    • pp.1320-1329
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    • 2024
  • When wall-thinning occurs in nuclear Class 2 and 3 pipes, reinforcement is typically applied rather than replacement. To analyze the structural integrity of reinforced wall-thinned pipe, stress analysis results using full 3-D FE analysis are not compatible to the design code equation, ASME BPVC Sec. III NC/ND-3650. Therefore, the efficient stress evaluation method for the reinforced wall-thinned pipe, compatible to the design code equation, needs to be developed. In this paper, stress evaluation methods for the reinforced wall-thinned pipe are proposed using the equivalent straight pipe concept. Furthermore, for fatigue analysis of the reinforced wall-thinned pipe, the stress intensification factor of reinforced wall-thinned pipe is presented using the structural stress method given in ASME BPVC Sec. VIII Div.2.

유선추적법을 이용한 자유표면 예측기법 개발 (Prediction of Free Surface by Streamline-Tracing Method)

  • 김태효;황상무
    • 한국소성가공학회:학술대회논문집
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    • 한국소성가공학회 1998년도 춘계학술대회논문집
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    • pp.175-178
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    • 1998
  • Tracings streamlines in global coordinate, especially with finite element mesh, requires much computation due to C0 continuity of velocity field. In this study, a new approach is presented for the determination of streamlines from velocity field obtained by FE analysis. It is shown that amount of calculation can be drastically reduced and boundary of element can be easily treated. The approach is applied to the problem of free surface of deforming workpieces in shape rolling.

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유한요소해석을 활용한 비구조 조적벽의 면외방향 설계 (Design for Out-of-Plane Direction of Nonstructural Masonry Walls Using Finite Element Analysis)

  • 최명규;유은종;김민재
    • 한국지진공학회논문집
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    • 제26권1호
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    • pp.23-30
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    • 2022
  • This study proposed a simplified finite element analysis procedure for designing the nonstructural masonry wall in the out-of-plane direction. The proposed method is a two-step elastic analysis procedure by bilinearizing the behavior of the masonry wall. The first step analysis was conducted with initial stiffness representing the behavior up to the effective-yield point, and the second step analysis was conducted with post-yield stiffness. In addition, the orthotropic material property of the masonry was considered in the FE analysis. The maximum load was estimated as the sum of the maximum loads in the first and second step analyses. The maximum load was converted into the moment coefficients and compared with those from the yield line method applied in Eurocode 6. The moment coefficients calculated through the proposed procedure showed a good match with those from the yield line method with less than 6% differences.

비대칭 Tetradentate Schiff 염기 리간드의 전이금속 착물에 대한 합성 및 특성 (Synthesis and Characterization of Some Transition Metal Complexes of Unsymmetrical Tetradentate Schiff Base Ligand)

  • Munde, A. S.;Jagdale, A. N.;Jadhav, S. M.;Chondhekar, T. K.
    • 대한화학회지
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    • 제53권4호
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    • pp.407-414
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    • 2009
  • o-phenylenediamine, 3-acetyl-6-methyl-(2H) pyran, 2,4 (3H)-dione (dehydroacetic acid or DHA) 및 살리실 알데히드로부터 유도한 4-hydroxy-3-(1-{2-(2-hydroxy-benzylidene)-amino phenylimino}-ethyl)-6- methy-pyran-2-one (H2L) 의 Cu(II), Ni(II), Co(II), Mn(II) 및 Fe(III) 고체 착물을 합성한 후, 원소분석, 전도 도법, 수자율, 자외선-가시선, 적외선, $^1H$-NMR 스펙트라, X-선 회절, 열분석을 통해 특성을 규명하고 항균 활성을 조사하였다. IR 스펙트럼 데이터로부터 이 리간드가 중심 금속이온에 대해 ONNO 주개원자 배열을 갖는 이염기성 네자리 리간드로 행동함을 제안하였다. 원소분석 데이터로부터 이들 착물의 화학량론이 1:1 (금속:리간드)임을 알았다. 물리-화학적 데이타로부터 Cu(II) 및 Ni(II) 착물이 사각평면 기 하구조, 그리고 Co(II), Mn(II) 및 Fe(III) 착물이 팔면체 기하구조임을 제안하였다. X-선 회절 데이터로 부터 Cu(II) 착물이 사방정계(orthorhombic) 결정계, Ni(II), Co(II) 및 Fe(III) 착물이 단사계(monoclinic) 결정계 그리고 Mn(II) 착물이 정방정계(tetragonal) 결정계임을 제안하였다. 착물의 열적 행동(TG/DTA) 을 연구하였으며 Coats-Redfern 방법으로 반응속도 파라메터를 결정하였다. 리간드와 이들 금속 착물을 이용하여 Staphylococcus aureus 및 Escherichia coli에 대한 향균 활성과 Aspergillus Niger 및 Trichoderma 에 대한 살균 활성을 조사하였다.

The Supplementation of Yam Powder Products Can Give the Nutritional Benefits of the Antioxidant Mineral (Cu, Zn, Mn, Fe and Se) Intakes

  • Shin, Mee-Young;Cho, Young-Eun;Park, Chana;Sohn, Ho-Yong;Lim, Jae-Hwan;Kwun, In-Sook
    • Preventive Nutrition and Food Science
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    • 제17권4호
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    • pp.299-305
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    • 2012
  • Yam has been recognized having the beneficial effects for the prevention of various diseases, such as cancer, immunity, infection and obesity etc. There is increasing consideration to supplement the antioxidant nutrients to make up the lack of the antioxidant nutrient intakes. No study has been reported for the analysis of antioxidant mineral contents and comparison to dietary recommended intake for the sense of health promotion. In our study, we analyzed the contents of antioxidant trace elements (Zn, Mn, Fe, Cu and Se) and Cr contents in cultivated Korean yam powders for evaluation of nutrient intake aspects. We collected the commercial yam powders from six different cultivated areas in the South Korea and measured antioxidant minerals (Zn, Mn, Fe, Cu and Se) and Cr contents using trace element-free plasma spectrometer (ICP) or atomic absorption spectrometer (AAS) after dry-ashing and then wet-acid digestion. The accuracy of mineral analysis method was confirmed by the mineral analysis of standard reference material. Each analyzed element contents in yam were compared to dietary reference intakes of Koreans (KDRIs). The average levels of trace elements (Zn, Mn, Fe, Cu, Se and Cr) in yam powders were 18.3, 11.9, 36.0, 3.7, 1.9 and 1.27 ${\mu}g/g$ yam powder, respectively. The intakes of Zn, Fe, Cu and Se of which KDRIs is determined, are accounted as being up to 23.8%, 55.6%, 32.5% and 236% recommended intake (RI) of KDRIs, if daily yam supplementation (50 g) of commercial instruction would be considered. The intake of Mn is about 25% adequate intake (AI) of KDRIs with the daily supplementation of yam powder. Most of mineral intakes from daily yam supplementation were with the range of non-detectable to <10% upper limit (UL) level, which is very much safe. The study results show that daily supplementation of Korean yam power is beneficial to provide the supplemental nutrient intake and also is safe, if the suggested dosage would be considered.

FCC계 고엔트로피 합금의 냉간 인발 유한요소해석 및 실험적 검증 (Finite Element Analysis and Experimental Verification for the Cold-drawing of a FCC-based High Entropy Alloy)

  • 조한솔;배성준;나영상;김정한;이동근;이광석
    • 소성∙가공
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    • 제29권3호
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    • pp.163-171
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    • 2020
  • We present a multi-step cold drawing for a non-equiatomic Co10Cr15Fe25Mn10Ni30V10 high entropy alloy (HEA) with a simple face-centered cubic (FCC) crystal structure. The distribution of strain in the cold-drawn Co10Cr15Fe25Mn10Ni30V10 HEA wires was analyzed by the finite element method (FEM). The effective strain was expected to be higher as it was closer to the surface of the wire. However, the reverse shear strain acted to cause a transition in the shear strain behavior. The critical effective strain at which the shear strain transition behavior is completely shifted was predicted to be 4.75. Severely cold-drawn Co10Cr15Fe25Mn10Ni30V10 HEA wires up to 96% of the maximum cross-sectional reduction ratio were successfully manufactured without breakage. With the assistance of electron back-scattering diffraction and transmission electron microscope analyses, the abundant deformation twins were found in the region of high effective strain, which is a major strengthening mechanism for the cold-drawn Co10Cr15Fe25Mn10Ni30V10 HEA wire.

유한요소해석기법을 이용한 토크 시편의 축 오열 영향 분석 (Effects of Axial Misalignments on the Torque Specimens Using Finite Element Analysis)

  • 김주희;김윤재;허용학
    • 대한기계학회논문집A
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    • 제35권11호
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    • pp.1461-1469
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    • 2011
  • 본 논문은 3 차원 유한요소해석 기법을 이용하여 토오크 시험을 위한 표준시험시편의 각도 및 동심 오열이 시편의 응력과 변형률 변화에 미치는 영향을 분석하였다. 해석 결과의 정량적 비교를 위해 각, 동심 및 복합 축 오열에 대한 평균 굽힘 변형률을 적용하였으며, 시편 형상에 따른 축 오열 영향을 확인하기 위해 환봉형 시편과 튜브형 시편에 대해 각각 유한요소해석을 실시하였다. 해석결과로부터 얻어진 변형률과 응력의 변화로 축 오열의 종류와 방향을 예측하는 일반적인 기준을 제시하였으며, 초기 항복조건을 적용하여 축 오열이 토오크 시편의 초기 항복 모멘트에 미치는 영향을 분석하였다.