• Title/Summary/Keyword: Calibration Method

Search Result 2,829, Processing Time 0.039 seconds

The Possibility of Environmental Paraquat Exposure (파라콰트의 환경성 노출 가능성)

  • Oh, Se-Hyun;Choi, Hong-Soon;You, Ho-Young;Park, Jun-Ho;Song, Jae-Seok
    • Journal of agricultural medicine and community health
    • /
    • v.36 no.4
    • /
    • pp.218-226
    • /
    • 2011
  • Objectives: Paraquat (PQ) is a widely used ionic pesticide that is fatal when ingested accidentally or for suicidal purposes. It is thought that chronic exposure of PQ is related with the development of Parkinson's disease, but epidemiological studies have not yet confirmed that theory. This study attempted to estimate the possibility of environmental PQ exposure through soil and water. Materials and Methods: We analyzed the amount of decomposed PQ solution in wet soil after exposure to ultraviolet light. An artificial rainfall condition was simulated over soil sprayed with PQ to measure the amount of eluted PQ. In addition, PQ was diluted in water from three differently rated rivers and the changes in PQ concentration were measured after ultraviolet exposure over one month. High performance liquid chromatography/ultra violet detection was used to analyze the concentrations of PQ. Results: In the method we used, the recovery rate of PQ showed a precision rate less than 5%, an accuracy greater than 88%, and the calibration equation was y=5538.8x-440.01($R^2$=0.9985). There were no significant differences in the concentrations of PQ obtained from the three specimens over a 1-week period. From the PQ-sprayed soil, the artificial rainfall conditions showed no PQ elution over a 1-month period, and there was no significant differences in PQ concentrations according to ultraviolet exposure among the three samples. Conclusions: PQ remains well adsorbed naturally in soil. However, it may still exist in an integrated state for a long time in the hydrosphere, so the possibility of PQ exposure through drinking water cannot be disqualified.

Development of Frequency Weighing Sensor and Single Crystal Growth (새로운 무게센서 재발과 단결정성장(1))

  • Jang Y.N.;Sung N.H.;Chae S.C.;Bae I.K.;Kim I.J.
    • Korean Journal of Crystallography
    • /
    • v.8 no.1
    • /
    • pp.38-47
    • /
    • 1997
  • A new weighing sensor for the automatic diameter control system of the crystal growth is developed in this study. This weighing sensor measures the frequency of the vibrating element which is lineally changing with respect to weight. The signal and the power of this system are transmitted without any physical contact, so that this sensor offers high accuracy and resolution. This system consists of a string, a sinusoidal wave generator, an automatic amplification adjusting circuit, signal transformers and a PCB. 4 kinds of programs are developed for checking DAC, weight calibration and controlling growth process. The measurements of the standard deviation and the resolution show $\pm0.10g$(measured at every second) and $5{\times}10^{-5}$, respectively, This weighing sensor is effective under high pres-sure of 200 atm, high temperature and vacuum condition. The weighing system can control the temperature in the accuracy of $\pm0.025^{\circ}C$ with the 'signal divider'. The optical quality single crystals of $(YGd)_3Sc_2Ga_3O_{12},\;Er-Y_3Sc_2Al_3O_{12},\;and\;Bi_{12}GeO_{20}$ have been grown by Czo-chralski method using this auto-diameter control system.

  • PDF

An Estimation of Flood Quantiles at Ungauged Locations by Index Flood Frequency Curves (지표홍수 빈도곡선의 개발에 의한 미 계측지점의 확률 홍수량 추정)

  • Yoon, Yong-Nam;Shin, Chang-Kun;Jang, Su-Hyung
    • Journal of Korea Water Resources Association
    • /
    • v.38 no.1
    • /
    • pp.1-9
    • /
    • 2005
  • The study shows the possible use of the index flood frequency curves for an estimation of flood quantiles at ungauged locations. Flood frequency analysis were made for the annual maximum flood data series at 9 available stations in the Han river basin. From the flood frquency curve at each station the mean annual flood of 2.33-year return period was determined and the ratios of the flood magnitude of various return period to the mean annual flood at each station were averaged throughout the Han river basin, resulting mean flood ratios of different return periods. A correlation analysis was made between the mean annual flood and physiographic parameters of the watersheds i.e, the watershed area and mean river channel slope, resulting an empirical multiple linear regression equation over the whole Han river basin. For unguaged watershed the flood of a specified return period could be estimated by multiplying the mead flood ratio corresponding the return period with the mean annual flood computed by the empirical formula developed in terms of the watershed area and river channel slope. To verify the applicability of the methodology developed in the present study the floods of various return periods determined for the watershed in the river channel improvement plan formulation by the Ministry of Construction and Transportation(MOCT) were compared with those estimated by the present method. The result proved a resonable agreement up to the watershed area of approximately 2,000k $m^2$. It is suggested that the practice of design flood estimation based on the rainfall-runoff analysis might have to be reevaluated because it involves too much uncertainties in the hydrologic data and rainfall-runoff model calibration.

Application of the weather radar-based quantitative precipitation estimations for flood runoff simulation in a dam watershed (기상레이더 강수량 추정 값의 댐 유역 홍수 유출모의 적용)

  • Cho, Yonghyun;Woo, Sumin;Noh, Joonwoo;Lee, Eulrae
    • Journal of Korea Water Resources Association
    • /
    • v.53 no.3
    • /
    • pp.155-166
    • /
    • 2020
  • In this study, we applied the Radar-AWS Rainrates (RAR), weather radar-based quantitative precipitation estimations (QPEs), to the Yongdam study watershed in order to perform the flood runoff simulation and calculate the inflow of the dam during flood events using hydrologic model. Since the Yongdam study watershed is a representative area of the mountainous terrain in South Korea and has a relatively large number of monitoring stations (water level/flow) and data compared to other dam watershed, an accurate analysis of the time and space variability of radar rainfall in the mountainous dam watershed can be examined in the flood modeling. HEC-HMS, which is a relatively simple model for adopting spatially distributed rainfall, was applied to the hydrological simulations using HEC-GeoHMS and ModClark method with a total of eight independent flood events that occurred during the last five years (2014 to 2018). In addition, two NCL and Python script programs are developed to process the radar-based precipitation data for the use of hydrological modeling. The results demonstrate that the RAR QPEs shows rather underestimate trends in larger values for validation against gauged observations (R2 0.86), but is an adequate input to apply flood runoff simulation efficiently for a dam watershed, showing relatively good model performance (ENS 0.86, R2 0.87, and PBIAS 7.49%) with less requirements for the calibration of transform and routing parameters than the spatially averaged model simulations in HEC-HMS.

A Study on Estimation of Systolic Blood Pressure using PTT (PTT를 이용한 수축기 혈압의 측정에 관한 연구)

  • Park E. K.;Lee S. M.;Han Y. H.;Lee J. Y.;Kwon S. Y.;Kim I. Y.;Kim Sun I.
    • Journal of Biomedical Engineering Research
    • /
    • v.25 no.6
    • /
    • pp.605-609
    • /
    • 2004
  • Blood pressure (BP) is one of the important physiological parameters for diagnosing cardiovascula diseases by means of noninvasive method. Existing noninvasive methods for measuring arterial BP have to use cuff and difficult in measuring arterial BP continuously. Systolic blood pressure (SBP) and pulse transit time (PTT) have a kind of inverse relationship. We acquired PTT data when subjects were in relaxation and also after exercise. We performed the linear regression analysis for making the regression equations for each subject and the regression equation for all subjects. We compared the estimated SBP with the measured SBP to check the accuracy of our regression equations. From the result, the regression equations for each subject was appropriate according to the American National Standards Institute of the Association of the Advancement of Medical Instrument (ANSI/AAMI) which says that BP devices should have ±5mmHg mean of error and 8mmHg standard deviation of error. However, the regression equation for all subjects was not proper to ANSI/AAMI recommendation. The result means that, without cuff, we can continuously estimate each subject's SBP through PTT and indivisual calibration.

HPLC-based Analysis of Biogenic Amines in Aging-Cheese (HPLC를 이용한 숙성치즈로부터 바이오제닉 아민 분석법 개발)

  • Park, Jong-Hyuk;Lee, Sang-Cheon;Moon, Hye-Jung;Oh, Jeon-Hui;Song, Gi-Bong
    • Journal of Dairy Science and Biotechnology
    • /
    • v.34 no.3
    • /
    • pp.187-191
    • /
    • 2016
  • Biogenic amines have been used as chemical indicators of fermented foods. So far, several chromatography methods have been developed to detect biogenic amines in foods. However, few methods have identified these compound in domestic cheese. We analyzed the biogenic amines (histamine dihydrochloride, tyramine hydrochloride, ${\beta}$-phenylethylamine hydrochloride, putrescine dihydrochloride, cadaverine, spermidine, tryptamine hydrochloride, ethanolamine hydrochloride and butylamine) in cheese by using HPLC. The calibration curves of the biogenic amines were found to be linear over the concentration range of 10-50 ppm with a correlation coefficient of above 0.99. The limit of detection (LOD) and limit of quantitation (LOQ) of the biogenic amines in the given order were 3.7 and 11.3 ppm, 3.4 and 10.4ppm, 3.4 and 10.3 ppm, 4.0 and 12.2 ppm, 3.4 and 10.4 ppm, 3.4 and 10.5 ppm, 3.5 and 10.7 ppm, 4.1 and 12.5 ppm, and 3.4 and 10.4 ppm, respectively. Recovery rates of the biogenic amines in the given order were 112, 104, 93, 108, 91, 102, 101, and 92%, respectively. The findings of this study suggest that HPLC is a suitable method for the determination of biogenic amines, thereby indicating its potential application in the quality control of aging cheese.

Determination of bromide in bottled mineral water and ground water in Korea (먹는 샘물 및 지하수 원수 중 bromide 분석연구)

  • Ahn, Hye-Sil;Seo, Kyoung-Ae;Park, Ju-Hyun;Lee, Jun-Bae;Kim, Tae-Seung;Han, Jin-Seok;Kwon, Oh-Sang
    • Analytical Science and Technology
    • /
    • v.24 no.1
    • /
    • pp.10-14
    • /
    • 2011
  • This study was performed to compare international analytical methods of bromide and applied to determine bromide in bottled mineral water and raw ground water in Korea. Bromide in water was eluted by 10~50 mM potassium hydroxide (KOH) and determined by ion chromatography-suppressed conductivity detector (IC-CD). Sample was purified with Ba- and H-on-guard cartridge and $0.2\;{\mu}m$ membrane filter. The method detection limit (MDL) and the limit of quantitation (LOQ) of bromide were 0.2 and $0.5\;{\mu}g/L$, respectively. The calibration curve showed good lineality above 0.9993 in the ranges of the $0.5\sim80\;{\mu}g/L$. A correlation coefficient of bromide in ground water and sum of bromide and bromate in bottled mineral water is 0.808.

Theory of X-ray microcomputed tomography in dental research: application for the caries research (치과 분야 연구에서 미세전산화 단층촬영술의 이론: 치아우식증에 대한 적용)

  • Park, Young-Seok;Bae, Kwang-Hak;Chang, Ju-Hea;Shon, Won-Jun
    • Restorative Dentistry and Endodontics
    • /
    • v.36 no.2
    • /
    • pp.98-107
    • /
    • 2011
  • Caries remains prevalent throughout modern society and is the main disease in the field of dentistry. Although studies of this disease have used diverse methodology, recently, X-ray microtomography has gained popularity as a non-destructive, 3-dimensional (3D) analytical technique, and has several advantages over the conventional methods. According to X-ray source, it is classified as monochromatic or polychromatic with the latter being more widely used due to the high cost of the monochromatic source despite some advantages. The determination of mineral density profiles based on changes in X-ray attenuation is the principle of this method and calibration and image processing procedures are needed for the better image and reproducible measurements. Using this tool, 3D reconstruction is also possible and it enables to visualize the internal structures of dental caries. With the advances in the computer technology, more diverse applications are being studied, such automated caries assessment algorithms.

Quantitative Analysis of Acid Value, Iodine Value and Fatty Acids Content in Sesame Oils by NIRS (근적외선분광광도법을 이용한 참기름의 산가, 요오드가, 지방산정량법에 관한 연구)

  • Kim, Jae-Kwan;Lee, Myung-Jin;Kim, Myung-Gill;Kim, Kyung-A;Park, Eun-Mi;Kim, Young-Sug;Ko, Hoan-Uck;Son, Jin-Seok
    • Journal of Food Hygiene and Safety
    • /
    • v.21 no.4
    • /
    • pp.204-212
    • /
    • 2006
  • This study was conducted to investigate the possibility of rapid and non-des tructive evalution of AV (Acid Value), IV (Iodine Value) and fatty acids in sesame oils. The samples were scanned over the range $400\sim2500nm$ using transmittance spectrum of NIRS(Near-infrared spectroscopy). A calibration equation calculated by MPLS regression technique was developed and correlation coefficient of determination for AV, IV, palmitic acid, stearic acid, linoleic acid and linolenic acid content were 0.9907, 0.9677, 0.9527, 0.9210, 0.9829, 0.9736 and 0.9709 respectively. The validation model for measuring the AV content had R of 0.989, SEP of 0.058 and IV content had R of 0.944, SEP of 0.562 and palmitic acid content had R of 0.924, SEP of 0.194 and stearic acid content had R of 0.717, SEP of 0.168 and oleic acid content had R of 0.989, SEP of 0.221 and linoleic acid content had R of 0.967, SEP of 0.297 and linolenic acid content had R of 0.853, SEP of 0.480 by MPLS. The obtained results indicate that the NIRS procedure can potentially be used as a non-destructive analysis method for the purpose of rapid and simple measurement of AV, IV and fatty acids in sesame oils.

Comparison Study of Beam Pattern for FDD downlink CDMA Signals (FDD에서 하향링크 CDMA신호의 빔패턴 비교 연구)

  • Kim, Sang-Choon;Son, Kyung-Soo;Ha, Joo-Young;Lee, Sung-Mok;Jang, Won-Woo
    • Journal of the Korea Institute of Information and Communication Engineering
    • /
    • v.11 no.2
    • /
    • pp.358-365
    • /
    • 2007
  • In this paper, the effects of transmit beamforming on downlink performance in DS-CDMA communication systems are investigated. The uplink and downlink in FDD systems use different carrier frequencies. If the downlink uses the same weighting vectors as the uplink, the antenna beam for downlink is formed with certain DOA shift and it thus affects the beamforming gain. So, the impacts of different frequencies on the downlink beam patterns are studied. One possible algorithm to convert uplink beamforming weights to downlink, which is called frequency-calibrated processing, is also evaluated to reduce the degradation of downlink performance due to different frequencies. Under frequency selective channels, the downlink chooses a PUPW beamforming scheme when the uplink employs a PPPW vectors. To form a beam pattern for a PUPW after combining the downlink PPPWs converted from the uplink PPPWs, three approaches are studied. One method is to consider only one dominant path and thus obtain a single main-beam. In the others, multiple-beams weighted with the magnitudes of all paths and equally weighted with all paths are constructed.