• Title/Summary/Keyword: 미세결합

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Effects of direct and indirect bonding techniques on bond strength and microleakage after thermocycling (직접 부착법과 간접 부착법이 열순환 후 부착강도와 미세누출에 미치는 영향에 대한 연구)

  • Ozturk, Firat;Babacan, Hasan;Nalcaci, Ruhi;Kustarci, Alper
    • The korean journal of orthodontics
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    • v.39 no.6
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    • pp.393-401
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    • 2009
  • Objective: The purpose of this study was to compare the shear bond strength (SBS) of brackets and microleakage of a tooth-adhesive-bracket complex bonded with a direct and an indirect bonding technique after thermocycling. Methods: Fifty non-carious human premolars were divided into two equal groups. In the direct bonding group a light-cured adhesive and a primer (Transbond XT) was used. In the indirect-bonding group, a light-cured adhesive (Transbond XT) and chemical-cured primer (Sondhi Rapid Set) were used. After polymerization, the teeth were kept in distilled water for 24 hours and thereafter subjected to thermal cycling (500 cycles). For the microleakage evaluation, 10 teeth from each group were further sealed with nail varnish, stained with 0.5% basic fuchsin for 24 hours, and examined under a stereomicroscope. Fifteen teeth from each group were used for SBS testing with the universal testing machine and adhesive remnant index (ARI) evaluation. Data were analyzed using the Mann-Whitney U test, Chi-square test, and Fisher's exact test. Results: There were no statistical differences on SBS and microleakage between the two bonding techniques. The indirect bonding group had a significantly lower ARI score. Bracket failures were obtained between enamel-resin interfaces. Conclusions: The type of bonding technique did not significantly affect the amount of microleakage and SBS.

Remediation of Soils Contaminated with Arsenic and heavy Metals by Soil Washing (토양세척에 의한 비소 및 중금속 오염토양의 복원)

  • Ko Ilwon;Lee Cheol-Hyo;Lee Kwang-Pyo;Kim Kyoung-Woong
    • Journal of Soil and Groundwater Environment
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    • v.9 no.4
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    • pp.52-61
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    • 2004
  • In order to remediate soils contaminated with oxyanionic As and cationic Zn and Ni through the pilot-scale acid washing, the effectiveness of acid washing and the properties of contaminated soils, fine soil particle and dissolved contaminants were evaluated. $H_{2}SO_4\;and\;H_{3}PO_4$ washing at pH $2{\sim}3$ enhanced the removal of As by the presence of competitive oxyanions and HCl washing effectively removed simultaneously As, Zn and Ni. The effectiveness of soil washing was little enhanced above the critical reaction time, and the carbonate, Fe/Mn oxide and organic/sulfides associated fraction were dominantly removed. The washing of coarse soil particles was highly efficient, but that of fine soil particles($<74{\mu}m$) was recalcitrant due to the enrichment with contaminants. Moreover, the physical separation of fine particles($<149{\mu}m$) enhanced the overall efficiency of soil washing. Therefore, both chemical extraction and separation of fine soil particles showed the high effectiveness of soil washing in the intersection point to minimize the amount of fine soil particles and to maximize the chemical extraction of contaminants.

Stabilization of Soil Moisture and Improvement of Indoor Air Quality by a Plant-Biofilter Integration System (식물-바이오필터에 의한 토양수분 안정화 및 실내 공기질 향상)

  • Lee, Chang Hee;Choi, Bom;Chun, Man Young
    • Horticultural Science & Technology
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    • v.33 no.5
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    • pp.751-762
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    • 2015
  • This study was performed to investigate the stability of soil moisture in controlling air ventilation rate within a horizontal biofilter, and to compare removal efficiency (RE) of indoor air pollutants including fine dust, volatile organic compounds (VOCs), and formaldehyde (HCHO), depending on whether dieffenbachias (Diffenbachia amoena) were planted in the biofilter. The relative humidity, air temperature, and soil moisture contents showed stable values, regardless of the presence of D. amoena, and the plants grew normally in the biofilter. REs for number of fine dust particles (PM10 and PM2.5) within the biofilter filled with only soil were at least 30% and 2%, respectively. REs for number of fine dust particles (PM10 and PM2.5) within the biofilter including the plants were above 40% and 4%, respectively. RE for fine dust (PM10) weight was above 4% and 20%, respectively, in the biofilter containing only soil or soil together with plants. In the case of the biofilter filled with only soil, REs for xylene, ethylbenzene, toluene or total VOC (T-VOC) were each more than 63%; however, REs for benzene and formaldehyde (HCHO) were above 22% and 38%, respectively. In the biofilter with the plants, REs for xylene, ethylbenzene, toluene, and T-VOC were each above 72%, and REs for benzene and HCHO were above 39%. Thus, RE of the biofilter integrated with plants was found to be higher for volatile organic compounds than for fine dust. Hence, the biofilter was very effective for indoor air quality improvement and the effect was higher when integrated with plants.

Improvement of the Stability of the Multibead Assay for Pneumococci by the Use of 6B-protein Complex (피막 다당류 6B-단백질 복합체를 이용한 폐렴구균에 대한 Multibead Assay의 안정성 향상)

  • 김지혜;임낙룡;박문국
    • Korean Journal of Microbiology
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    • v.39 no.1
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    • pp.62-65
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    • 2003
  • A procedure to increase the stability of 6B capsular polysaccharide on microbead surface in the mutibead assay, a serotyping method for Streptococcus pneumoniae, was studied. Pneumococcal capsular polysaccharide 6B was conjugated to bvine serum albumin (BSA), and the coating efficiency and the stability of the 6B-BSA complex was measured. The 6B-BSA complex showed about 200-fold higher coating efficiency to polystyrene surface than 6B polysaccharide. And the stability of the 6B- BSA to be used in the multibead assay for 30 days after coating.

The Ultrastructure of the Spermatheca of the Pulmonate Snail Nesiohelix samarangae (동양 달팽이의 정자낭 (Spermatheca)의 미세구조)

  • Jeong, Kye-Heon
    • The Korean Journal of Malacology
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    • v.9 no.2
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    • pp.94-102
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    • 1993
  • 동양달팽이(Nesiohelix samarangae)의 자성생식기 중 정자낭(spermatheca)의 미세구조를 투과전자현미경을 이용하여 관찰하였다. 성체의 정자낭의 내강에서는 정자와 이와 관련된 물질들 또는 상피로부터의 분비물질들이 관찰되었다. 정자낭의 내강을 둘러싸고 있는 벽의 상피는 단층원주상피로서 내강과 연한 세포의 원형질막은 미세융모를 가지고 있었으며 섬모는 가지고 있지 않았다. 이 미세융모들의 기부에서는 고배율 하에서 pinocytotic vesicle들이 관찰되었고 때로 세포의 분비물을 세포 밖으로 방출하는 모습도 관찰되었다. 세포들의 상부세포질에는 많은 수의 mitochondria가 있었고, 때로 분비과립과 lysosomd들이 존재하기도 하였다. 이들보다 아래에는 잘 발달한 골지체와 과립소포체(RER)들이 있었다. 이 부위에서 분비과립들이 많이 형성되어 있는 모습이 세포에 따라 관찰되었고, 그 아래에 즉, 각 세포의 하반부 세포질에 상하로 긴 핵이 관찰되었다. 세포의 기부 원형질막은 상부 세포질 내로 깊게 그리고 수없이 많이 주름을 이루고 있어 인접한 세포와의 경계를 구분할 수 없을 정도였다. 기저막의 아래에는 근육다발과 색소세포들이 결합조직 내에서 관찰되었고, 정자낭의 외막은 큰 액포로 인하여 세포질들이 원형질막 주변으로 밀려나 있는 특이한 세포들로 이루어져 있었다. 정자낭의 기능은 정자를 일시 저장하며 정자낭 상피에서 분비되는 소화액들로 정자를 일차적으로 세포외 소화하고 소화되지 않은 물질들을 흡수하여 이차적으로 세포내소화하는 것으로 생각된다.

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A Study on Visualization of Fine Dust Captured by FOG Droplet (미세액적에 의한 미세먼지 포집 가시화 연구)

  • Oh, Jinho;Kim, Hyun Dong;Lee, Jung-Eon;Yang, Jun Hwan;Kim, Kyung Chun
    • Journal of the Korean Society of Visualization
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    • v.19 no.3
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    • pp.39-45
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    • 2021
  • An experiment to visualize fine dust captured by FOG droplet is conducted. Coal dust with 23.56 MMD (Mean Median Diameter) and water with 17.02 MMD is used as fine dust and FOG droplet. Long distance microscope and high-speed camera are used to capture the images of micro-scale particles sprinkled by acrylic duct. After measuring and comparing the size of the coal dust and FOG droplet to MMD, process to seize the coal dust with FOG droplet is recorded in 2 conditions: Fixed and Floated coal dust in the floated FOG droplet flow. In both conditions, a coal dust particle is collided and captured by a FOG droplet particle. A FOG droplet particle attached at the surface of the coal dust particle does not break and remains spherical shape due to surface tension. Combined particles are rotated by momentum of the particle and fallen.

Microfluidic Fabrication of Conjugated Polymer Sensor Fibers (미세유동을 이용한 공액 고분자 센서 섬유 제작)

  • Yoo, Imsung;Song, Simon
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.38 no.10
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    • pp.853-858
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    • 2014
  • We propose a fabrication method for polydiacetylene (PDA)-embedded hydrogel microfibers on a microfluidic chip. These fibers can be applied to the detection of cyclodextrines (CDs), which are a family of sugar and aluminum ions. PDA, a family of conjugated polymers, has unique characteristics when used for a sensor, because it undergoes a blue-to-red color transition and nonfluorescence-to-fluorescence transition in response to environmental stimulation. PDAs have different sensing characteristics depending on the head group of PCDA. By taking advantage of ionic crosslinking-induced hydrogel formation and the 3D hydrodynamic focusing effect on a microfluidic chip, PCDA-EDEA-derived diacetylene (DA) monomer-embedded microfibers were successfully fabricated. UV irradiation of the fibers afforded blue-colored PDA, and the resulting blue PDA fibers underwent a phase transition to red and emitted red fluorescence upon exposure to CDs and aluminum ions. Their fluorescence intensity varied depending on the CDs and aluminum ion concentrations. This phase transition was also observed when the fibers were dried.

Fine Structure of Pericanalicular Cytoplasm of Taurocholic Acid-treated Rat Liver as Revealed by Deep Etching with Rapid Freezing (Taurocholic acid 투여 흰쥐 담세관주위세포질의 미세구조에 관한 급속동결 deep etching법에 의한 연구)

  • Shin, Young-Chul
    • Applied Microscopy
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    • v.28 no.1
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    • pp.73-82
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    • 1998
  • To elucidate how microfilaments and vesicles participate in bile formation, the pericanalicular cytoplasms were observed in the liver of rats treated with taurocholic acid by deep etching with rapid freezing, and copmpared them with the findings on convensional thin sections. The microfilaments were identified around the bile canaliculi in the forms of core filaments of microvilli, filaments of pericanalicular web running in parallel to the border of bile canaliculi, and filaments on the junctional complex. In taurocholic acid-treated rats, microfilaments could be visualized around the bile canaliculi and along their borders. The microfilaments appeared to be installed to link to both the canalicular membrane and vesicles. Such specialized microfilaments are considered to participate in the translocation of vesicles in the pericanalicular cytoplasm. From the evidence, it is assumed that the microfilament induces the vesicles to transport and fuse to bile canalicull into which bile acids is secreted by exocytosis.

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MICROSTRUCTURE OF COMBINATION CLASP JOINTS IN REMOVABLE PARTIAL DENTURE (가철성(可撤性) 국부의치(局部義齒)에서 연합(聯合) Clasp 연결부위(連結部位)의 미세구조(微細構造))

  • Son, Han-Kee;Kim, Tae-Wan
    • The Journal of Korean Academy of Prosthodontics
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    • v.22 no.1
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    • pp.123-132
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    • 1984
  • To evaluate the microstructure of various combination clasp joint in removable partial denture, the auther selected framework alloys (Type IV gold alloy, Dentaurium, Ticonium 100) and wrought wires (gold alloy, Ticonium) for this study. Twelve series of combination joints were made by investment soldering technic and wrought wire embedded casting technic. All specimens were cut cross-sectionally and longitudinally, then examined with metallurgical microscope. The results were as follows; Some diffusion was observed in the properly constructed combination clasp joints. In soldered joints, empolying precious alloys were more favorable than non-precious alloys. In castion joints, assemblage of same alloy between framework and wrought wire was superior to other groups. Some impurities were observed in both joints by technical problems.

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Microencapsulation Characteristics Depending on Mixing Ratio of Wall Materials and Squid Liver Oil (피복물질과 오징어 간유의 혼합 비율에 따른 미세캡슐화 특성)

  • Hwang, Sung-Hee;Youn, Kwang-Sup
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.36 no.1
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    • pp.100-104
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    • 2007
  • This study was carried out to investigate the microencapsulation characteristics of squid liver oil according to various ratios of wall materials and squid liver oil. The emulsion stability and the water binding capacity increased with an increase in wall materials contents. The microencapsulation efficiency was found to be in the order of 7:3>4:6>3:7>5:5>6:4 by mixing ratio of wall materials and squid liver oil; also, ratio of 7:3 was found to be inappropriate because the oil content in the powder was not sufficient. Regarding the fatty acid composition, the content of polyunsaturated fatty acid was found to be over 50% in all treatment groups. The ratio of polyunsaturated to saturated fatty acid of the powder was the highest (2.13) at the mixing ratio of 4:6.