• 비파괴검사학회지
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• 제31권2호
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• pp.174-180
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• 2011

본 연구에서는 초음파원자현미경을 이용하여 비파괴적인 표면탄성이미지 분석과 나노표면에서의 기계적 물성 평가를 연구하였다. 이를 위해 접촉역학 특성에 따른 캔틸레버의 공진주파수 변화를 이론적으로 해석하고 실험적으로 측정하였다. 스프링-질량 모델과 Herzian 이론을 이용하여 계산한 이론적인 접촉공천주파수는 초음파원자현미경 캔틸레버의 실험적인 접촉 공진주파수의 변화와 매우 유사하였다. 결과적으로, 초음파원자현미경의 표면 높이 이미지와 진폭이미지를 성공적으로 얻을 수 있었고 진폭신호를 통하여 시료표면에서의 탄성특성을 정성적으로 평가하였다.

• Journal of Electrical Engineering and Technology
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• 제13권6호
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• pp.2434-2440
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• 2018

A new type of piezoelectric micromachined ultrasonic transducer (pMUT) with high resonant frequency was developed by using a thin lead zirconate titanate (PZT) as an insulation layer on a floating $10{\mu}m$ silicon membrane. The PZT insulation layer facilitated acoustic impedance matching at active pMUT, leading to a high performance in the acoustic conversion property compared with the transducer using $SiO_2$ insulation layer. The fabricated ultrasonic devices were wirelessly measured by connecting two identical acoustic transducers to two separate ports in a single network analyzer simultaneously. The acoustic wave emitted from a transducer induced a $3.16{\mu}W$ on the other side of the transducer at a distance of 2 cm. The transducer performances in terms of device diameters, PZT thickness, annealings, and different DC polings, etc. were investigated. COMSOL simulation was also performed to predict the device performances prior to fabrication. Based on the COMSOL simulation, the device was fabricated and the results were compared.

• 한국분말재료학회지
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• 제23권4호
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• pp.307-310
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• 2016

$TiOF_2$, which has remarkable electrochemical and optical properties, is used in various applications such as Li-ion batteries, electrochemical displays, and photocatalysts. In addition, it is possible to utilize the template which is allowed to synthesize fluorine doped $TiO_2$ powders with hollow or faceted structures. However, common synthesis methods of $TiOF_2$ powders have some disadvantages such as the use of expensive and harmful precursors and batchtype processes with a limited production scale. In this study, we report a synthetic route for preparing $TiOF_2$ powders by using an inexpensive and harmless precursor and a continuous ultrasonic spray pyrolysis process under a controlled atmosphere to address the aforementioned problems. The synthesized powder has an average size of $1{\mu}m$, a spherical shape, a pure $TiOF_2$ phase, and exhibits a band-gap energy of 3.2 eV.

• 한국분말재료학회지
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• 제24권4호
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• pp.326-331
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• 2017

The structural formation of inorganic nanoparticles dispersed in polymer matrices is a key technology for producing advanced nanocomposites with a unique combination of optical, electrical, and mechanical properties. Barium titanate ($BaTiO_3$) nanoparticles are attractive for increasing the refractive index and dielectric constant of polymer nanocomposites. Current synthesis processes for $BaTiO_3$ nanoparticles require expensive precursors or organic solvents, complicated steps, and long reaction times. In this study, we demonstrate a simple and continuous approach for synthesizing $BaTiO_3$ nanoparticles based on a salt-assisted ultrasonic spray pyrolysis method. This process allows the synthesis of $BaTiO_3$ nanoparticles with diameters of 20-50 nm and a highly crystalline tetragonal structure. The optical properties and photocatalytic activities of the nanoparticles show that they are suitable for use as fillers in various nanocomposites.

• 한국전기전자재료학회:학술대회논문집
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• 한국전기전자재료학회 2005년도 하계학술대회 논문집 Vol.6
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• pp.352-353
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• 2005

In this paper, an ultrasonic level limit sensor with a new structure utilizing the acoustic impedance matching is proposed to be able to check it out a change of water-level. 2 PZT resonators with the same property are bonded directly on the polyethylene plate. One is for transmitter as an ultrasonic transducer, the other one is for receiver. In this case, a polyethylene plate will operate as an acoustic guider to transmit a transverse wave between 2 PZT resonators in air. While in the water, a polyethylene plate having a similar acoustic impedance with the water will be emitted an acoustic energy into the water as a longitudinal wave. According to this mechanism, there was a wide difference of acoustic signal output between underwater and in air. As a summary, it is believed that this proposed level limit sensor could be used as a new one with strong toughness from the external electrical and mechanical noise.

• 비파괴검사학회지
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• 제30권2호
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• pp.132-138
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• 2010

본 연구에서는 접촉역학 특성에 의한 캔틸레버 탑의 접촉-진동을 연구하고 나노스케일의 표면에서 탄성특성을 이미지화 하였다. 스프링-질량 모텔과 Herzian 이론을 이용하여 접촉공진주파수를 이론적으로 계산하고 초음파원자현미경을 이용하여 캔틸레버의 자유공진주파수와 접촉공진주파수의 변화를 분석하였다. 또한, 프로토타입의 초음파원자현미경을 이용하여 구상화 열처리된 시험편의 탄성 이미지를 위상과 진폭 신호를 이용하여 성공적으로 얻을 수 었었다.

• Smart Structures and Systems
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• 제18권3호
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• pp.471-484
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• 2016

Optical fiber sensors have been proven that they have the potential to detect high-frequency ultrasonic signals, in structural health monitoring field which generally refers to acoustic emission signals from active structural damages and guided waves excited by ultrasonic actuators and propagating in waveguide. In this work, the sensing properties of optical fiber sensors based on Mach-Zehnder interferometer were investigated in the metal plate. Analytical formulas were conducted first to explore the parameters affecting its sensing performances. Due to the simple and definable frequency component, the Lamb wave excited by the piezoelectric wafer was employed to study the sensitivity of the proposed optical fiber sensors with respect to the frequency, rather than the acoustic emission signals. In the experiments, according to above investigations, spiral shape optical fiber sensors with different size were selected to increase their sensitivity. Lamb waves were excited by a circular piezoelectric wafer, while another piezoelectric wafer was used to compare their voltage responses. Furthermore, by changing the excitation frequency, the tuning frequency characteristic of the proposed optical fiber sensor was also investigated experimentally.

• 한국분말재료학회지
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• 제25권6호
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• pp.482-486
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• 2018

Despite numerous advances in the preparation and use of GaN, and many leading-edge applications in lighting technologies, the preparation of high-quality GaN powder remains a challenge. Ammonolytic preparations of polycrystalline GaN have been studied using various precursors, but all were time-consuming and required high temperatures. In this study, an efficient and low-temperature method to synthesize high-purity hexagonal GaN powder is developed using sub-micron $Ga_2O_3$ powder as a starting material. The sub-micron $Ga_2O_3$ powder was prepared by an ultrasonic spray pyrolysis process. The GaN powder is synthesized from the sub-micron $Ga_2O_3$ powder through a nitridation treatment in an $NH_3$ flow at $800^{\circ}C$. The characteristics of the synthesized powder are systematically examined by X-ray diffraction, scanning and transmission electron microscopy, and UV-vis spectrophotometer.

• 한국세라믹학회지
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• 제27권1호
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• pp.74-78
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• 1990

In this study, to develope the ultrasonic transducer element, the extrusion method which is the processing technique of the piezoelectric composite materials is introduced, the connectivity of the piezoelectric composite materials is the 1-3 type, and we study the properties of the materials. The electromechanical coupling factor(kt) of the materials is above 0.6, the resonance property(fr) is the thickness mode in the frequency range of 0.5 to 2 [MHz] and the acoustic impedance(Zac) is about 5 to 7 [Maryl]. From these results, it is known that the piezoelectric composite materials manufactured byt he extrusion method will be able to develope the ultrasonic transducer elements.

• 한국정보기술응용학회:학술대회논문집
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• 한국정보기술응용학회 2005년도 6th 2005 International Conference on Computers, Communications and System
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• pp.215-218
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• 2005

We have investigated on the development of 2-2 piezocomposites that have better piezoelectric activity and lower acoustic impedance than those of conventional piezoceramics. In this study, we have investigated the piezoelectric and acoustic properties of 2-2 piezocomposites sensor which were fabricated using dice-and-fill technique for the different volume fraction of PZT. The resonance characteristics measured by an impedance analyzer were similar to the analysis of finite element method. The resonance characteristics and the electromechanical coupling factor were the best when the volume fraction PZT was 0.6. It also showed the highest result from the standpoint of sensitivity, bandwidth and ring-down property and so on at the same condition. The specific characteristics shows that the 2-2 piezocomposites turned out to be superior to the ultrasonic sensor composed by single phase PZT.