• Title/Summary/Keyword: ultrasonic homogenizer

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Structural, Thermal and Mechanical Properties of Nano Composites according to Homogenizer and Power Ultrasonic (균질기와 초음파 동시 분산을 통한 나노콤포지트의 구조적, 열적, 기계적특성)

  • Yeom, Gyoo-Ho;Park, Kwang-Sik;Choe, Seong-Jo;Jeon, Sang-Hoon;Kwak, Young-Hoon;Park, Jae-Jun
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2010.06a
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    • pp.82-82
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    • 2010
  • 에폭시메트릭스 내에서 초음파 및 균질기를 이용하여 층상실리케이트 마이크로 입자의 균질분산을 위하여 사용하였다. 초음파와 균질기를 동시에 사용하여 최적의 적용시간과 충진나노입자 충진함량과의 관계를 연구하기위하여 구조적 특성으로 X-RD, 열적특성으로 DSC, 열적 기계적 특성으로 DMA를 사용하여 특성을 평가하였다. 충진함량 변화에 대해서 층상실리케이트의 층간사이 간격의 변화는 반비례하는 특성을 나타내었고, 충진함량이 증가됨에따라 자체만으로는 크게 응집된 입자의 분산이 미약한 결과로 볼 수 있다. 그러나 Homogenizer와 동시에 분산할 때는 충진함량이 크게 증가하여도 균질한 분산이 이루어졌다.

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Comparative Growth Performance and Physiological Function of Physically Modified Rice Starch and Gelatinized Rice Starch in Growing Rats (물리적 변성 쌀전분과 호화 쌀전분의 생리적 효과 비교연구: 성장 능력과 장기의 생리적 기능)

  • Chang, Moon-Jeong;Kim, Myung-Hwan
    • Journal of the Korean Society of Food Culture
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    • v.18 no.6
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    • pp.592-600
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    • 2003
  • Male rats were fed a purified diet containing one of 3 experimental diets, gelatinized rice starch that was not modified physically (RC), gelatinized physically modified rice starch using ultrasonic homogenizer(RU), gelatinized physically modified rice starch using hydroshear homogenizer(RH) during 28 days. RC was used as the rice starch control. Feeding a physically modified rice starch (RU) caused an increase in liver weight and RH increased RNA and protein contents in kidney significantly although there were no differences in food intakes compared to feeding a RC diet. The wet weight of liver, kidney and heart were higher in RU. The wet weights of fecal output of the rats fed RH was greater than in rice control group. The gut transit time was longer in the rats fed RH than in the rice control group significantly. Serum GOT, GPT, total bilirubin concentration were tended to be lower and blood urea nitrogen was significantly lower in RH group. The maturation index of kidney was higher in RU than in RC. These results suggest that physically modified rice starch improved growth performance and physiological functions in organs of growing rats.

Electrical and Mechanical Characteristics for Filled Contents Variation of Epoxy-SiO2 Nanocomposites (Epoxy-$SiO_2$ Nanocomposites 충진함량 변화의 전기적 그리고 기계적 특성)

  • Park, Jae-Jun;Lee, Dong-Yoon
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2008.11a
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    • pp.361-362
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    • 2008
  • 에폭시 메트릭스에 $10{\pm}5nm$ SiO2 입자를 함량별 (1,3,5,7,9wt%)로 혼합하여 초음파 및 균질기를 이용한 분산을 실시하여 나노콤포지트를 제조하였다. 엉킴이 있는 나노입자를 물리적분산법을 이용하여 분산시킬 수 있었고, 그 결과 여러특성을 연구하였다. 기계적 굴곡강도 특성은 나노입자 충진함량 증가에따라 증가되는 경향을 나타내었고, 무충진 에폭시수지에 비하여 상대적으로 높은 굴곡강도를 나타내었다. 나노입자의 충진함량 증가에따라 절연파괴강도는 1wt%에서 가장 높는 절연파괴강도를 기록하였고 함량증가에 따라 약간 감소되는 경향을 보이고 있다. 이는 여러 연구자의 경향과 대체로 유사함을 알 수 있었다.

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It's effects for engine emission of water/oil emulsified fuel (Water/Oil 에멀젼 연료가 배출가스에 미치는 영향)

  • Kim, Moon-Chan;Lee, Chang-Suk
    • Analytical Science and Technology
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    • v.21 no.3
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    • pp.159-166
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    • 2008
  • In this study, the characteristics of emulsified fuel and engine emissions were studied. Emulsified fuel which composed of water and diesel was manufactured by using homogenizer and ultrasonic generator. Engine emissions were studied whit engine dinamometer. In emulsified fuel, density and viscosity were increased with increasing water contents, but viscosity was decreased over 60% of water in emulsion fuel. The emulsion type of W/O changed to that of O/W over 60% of water in emulsion fuel. In the results of engine dinamometer test, NOx concentration and smoke density were reduced with increasing water contents in emulsified fuel but reciprocal in the case of THC, CO. Temperature and power were reduced with increasing water contents in emulsion fuel. In conclusion, it seemed that using emulsified fuel for diesel engine was effective for reducing NOx concentration and smoke density.

Optimal Extraction Conditions of Active Components from the Adventitious Roots of Noni (Morinda citrifolia) (노니 부정근으로부터 유효성분의 최적 추출조건)

  • Kim, Myong-Ki
    • Korean Journal of Food Science and Technology
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    • v.48 no.2
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    • pp.111-116
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    • 2016
  • To determine the optimum condition for the extraction of active components, noni adventitious roots were extracted under various conditions employing various solvents including methanolic water at different ratio (20, 40, 60, 80, and 100% water), extraction times and extraction methods. Anthraquinones, phenolic compounds, and flavonoids extraction using different solvents showed that 1 h of ultrasonic extraction was effective in 60-80% methanol, and 2 h of reflux extraction was effective in 80% methanol. To compare the extraction efficiency of active components according to different extraction methods and extraction times for noni adventitious roots, the active components were extracted by ultrasonic extraction, shaking extraction, reflux extraction, homogenizer extraction, high-pressure extraction, and soaking extraction. The highest phenolic contents were found in the extracted from ultrasonic extraction and anthraquinones and flavonoids contents were highest in the reflux extraction.

Tribological Behavior of Lubricating Oil-Based Nanofluids Containing Ag and Carbon Nanoparticles (Ag 및 탄소 나노윤활유의 제조 및 윤활특성 평가)

  • Choi, Cheol;Jung, Mi-Hee;Choi, Young-Min;Oh, Jae-Myung
    • Korean Journal of Materials Research
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    • v.18 no.11
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    • pp.610-616
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    • 2008
  • Oil-based nanofluids were prepared by dispersing Ag, graphite and carbon black nanoparticles in lubricating oil. Agglomerated nanoparticles were dispersed evenly with a high-speed bead mill and/or ultrasonic homogenizer, and the surfaces of the nanoparticles were modified simultaneously with several dispersants. Their tribological behaviors were evaluated with a pin-on-disk, disk-on-disk and four-ball EP and wear tester. It is obvious that the optimal combination of nanoparticles, surfactants and surface modification process is very important for the dispersity of nanofluids, and it eventually affects the tribological properties as a controlling factor. Results indicate that a relatively larger size and higher concentration of nanoparticles lead to better load-carrying capacity. In contrast, the use of a smaller size and lower concentration of particles is recommended for reducing the friction coefficient of lubricating oil. Moreover, nanofluids with mixed nanoparticles of Ag and graphite are more suitable for the improvement of load-carrying capacity and antiwear properties.

Preparation and Characterization of Lubricating Oil-based Nanofluids Containing Carbon Nanoparticles (탄소 나노소재를 이용한 윤활유 기반 나노유체의 제조 및 평가)

  • Choi, Cheol;Jung, Mi-Hee;Oh, Jae-Myung
    • Korean Journal of Materials Research
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    • v.19 no.3
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    • pp.156-162
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    • 2009
  • Lubricant-based nanofluids were prepared by dispersing carbon nanoparticles in gear oil. In this study, the effects of the particle size, shape and dispersity of the particles on the tribological properties of nanofluids were investigated. Dispersion experiments were conducted with a high-speed bead mill and an ultrasonic homogenizer, and the surfaces of the nanoparticles were simultaneously modified with several dispersants. The effective thermal conductivity of the nanofluids was measured by the transient hot-wire method, and the tribological behaviors of the nanofluids were also investigated with a disk-on-disk tribo-tester. The results of this study clearly showed that the combination of the nanoparticles, the deagglomeration process, the dispersant and the dispersion solvent is very important for the dispersity and tribological properties of nanofluids. Lubricant-based nanofluids showed relatively low thermal conductivity enhancement, but they were highly effective in decreasing the frictional heat that was generated. For nanofluids containing 0.1vol.% graphite particles in an oil lubricant, The friction coefficient in the boundary and fluid lubrication range was reduced to approximately 70% of the original value of pure lubricant.

Effects of Preparation Conditions on Thermal and Electrical Properties of Oil-based Nanofluids for Transformer Application (변압기 냉각용 오일 기지 나노유체의 제조조건이 열 및 전기적 특성에 미치는 영향)

  • Choi, Cheol;Yoo, Hyun-Sung;Oh, Jae-Myung
    • Korean Journal of Materials Research
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    • v.17 no.9
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    • pp.493-499
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    • 2007
  • Oil-based nanofluids were prepared by dispersing nonconducting fibrous $Al_2O_3$ and spherical AlN nanoparticles in transformer oil. In this study, the effects of wet grinding and surface modification of particles on thermal and electrical properties of nanofluids were investigated. Grinding experiments were conducted with high-speed bead mill and ultrasonic homogenizer and nanoparticles were surface modified by oleic acid and polyoxyethylene alkyl acid ester(PAAE) in n-hexane or transformer oil, at the same time. It is obvious that the combination of nanoparticle, dispersant and dispersion solvent is very important for the dispersity of nanofluids. For nanofluids containing 1.0vol.% AlN particles in transformer oil, the enhancement of thermal conductivity was 11.6% compared with pure transformer oil. However, the electric-insulating property of AlN nanofluids was very low due to used dispersant itself. Therefore, the effect of the dispersant on thermal/electrical/physical properties of the transformer oil should be considered before selecting a proper dispersant.

Insecticidal efficiency of orange peel (Citrus sinensis) essential oil nanoemulsions against Rhyzopertha dominica (Fabricius, 1792) and Tribolium castaneum (Herbst, 1797)

  • Semra Cicek;Yesim Bulak Korkmaz;Sevda Isik
    • Advances in nano research
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    • v.17 no.1
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    • pp.75-86
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    • 2024
  • The insecticidal efficiency of orange (Citrus sinensis) peel essential oil (OP-EO) is limited because of its low stability under environmental conditions. Nanoemulsion formulations show promise in overcoming this limitation. Therefore, this study aimed to formulate and characterize the OP-EO nanoemulsion form (OP-EON) and investigate its insecticidal properties against two significant storage pests, Rhyzopertha dominica (Fabricius, 1792), and Tribolium castaneum (Herbst, 1797). The OP-EON (4:3:3:90 w/w, EO: Tween 80: Ethanol: water) was successfully created using an ultrasonic homogenizer. The major chemical components of the OP-EO were determined to be D-limonene (87.93%), myrcene (3.62%), and α-pinene (1.34%) through GC-MS analysis. The OP-EON was characterized using TEM (50-100 nm), Zeta sizer (the mean droplet particle size of 58.60 nm, the ζ-potential value of -12.6 mV, and the polydispersity index of 0.486), and FT-IR analysis. After 7 days, exposure to 500 ppm of the OP-EON resulted in 50% and 30% mortality rates in R. dominica and T. castaneum, respectively. Exposure to 1000 ppm of OP-EON resulted in 90% and 55% mortality in R. dominica and T. castaneum, respectively, after 7 days. Overall, these results clearly showed the potential to exceed the limits of the insecticidal activity of the OP-EO with its nanoemulsion form.

A Study on the Application of Marine Emulsion Fuel for Tier 3 Regulation (Tier 3 규제 대응을 위한 선박용 에멀젼 연료 적용성 연구)

  • Lee, Ki-Bong;Kim, Moon-Chan;Park, Hea Kyung
    • Journal of Korean Society of Environmental Engineers
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    • v.34 no.10
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    • pp.671-677
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    • 2012
  • In this study, the characteristics of emulsified fuel and engine emissions were studied with an engine dynamometer. In the results of physical property analysis, the margin of error of net calorific value and gross calorific value was ${\pm}0.5%$, were almost same theoretical calculation and results of physical property analysis test. In emulsified fuel, density and viscosity increased with increasing water contents. Emulsified fuel which is composed of water and Bunker-A was manufactured by using homogenizer and ultrasonic generator in $80^{\circ}C$. Phase separation did not take place in $20^{\circ}C$ and $50^{\circ}C$. In the results of engine dynamometer test, NOx concentration and smoke density were reduced with increasing water contents in using emulsified fuel. Total NOx could be reduced by about 41%, 10%, 32% and 28% at 1,000 rpm, 1,200 rpm, 1,500 rpm and 2,500 rpm respectively. Total smoke density was reduced to 42%, 65%, 70%, 62%, and 82% at 1,000 rpm, 1,200 rpm, 1,500 rpm, 2,000 rpm, and 2,500 rpm respectively.