• The Journal of Advanced Prosthodontics
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• 제6권4호
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• pp.317-324
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• 2014

PURPOSE. This study was to evaluate the effect of grinding of the inner metal surface during the porcelain try-in stage on metal-porcelain bonding considering the maximum temperature and the vibration of samples. MATERIALS AND METHODS. Ninety-one square prism-shaped ($1{\times}1{\times}1.5mm$) nickel-chrome cast frameworks 0.3 mm thick were prepared. Porcelain was applied on two opposite outer axial surfaces of the frameworks. The grinding was performed from the opposite axial sides of the inner metal surfaces with a low-speed handpiece with two types of burs (diamond, tungsten-carbide) under three grinding forces (3.5 N, 7 N, 14 N) and at two durations (5 seconds, 10 seconds). The shear bond strength (SBS) test was performed with universal testing machine. Statistical analyzes were performed at 5% significance level. RESULTS. The samples subjected to grinding under 3.5 N showed higher SBS values than those exposed to grinding under 7 N and 14 N (P<.05). SBS values of none of the groups differed from those of the control group (P>.05). The types of bur (P=.965) and the duration (P=.679) did not affect the SBS values. On the other hand, type of bur, force applied, and duration of the grinding affected the maximum temperatures of the samples, whereas the maximum vibration was affected only by the type of bur (P<.05). CONCLUSION. Grinding the inner metal surface did not affect the metal-porcelain bond strength. Although the grinding affected the maximum temperature and the vibration values of the samples, these did not influence the bonding strength.

• 한국분말재료학회지
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• 제18권3호
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• pp.262-268
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• 2011

In order to investigate the microstructure and mechanical properties of WC-10 wt% Co insert tool alloy fabricated by PIM (Powder Injection Molding) process, the feedstock of WC-10 wt% and wax used as a kind of binder were mixed together by two blade mixer. After injection molding, the debinding process was carried out by two-steps. First, solvent extraction, in which the binder was eliminated by putting the specimen into normal hexane for 24 hrs at $60^{\circ}C$, and subsequently thermal debinding which was conducted at $260^{\circ}C$ and $480^{\circ}C$ for 6 hrs in the mixed gas of $H_2/N_2$, respectively. Meantime, in order to compensate the decarburization due to hydrogen, 1.2~1.8% of carbon was added to ensure the integrity of the phase. Finally, the specimens were sintered in vacuum under different temperatures, and the relative density of 99.8% and hardness of 2100 Hv can be achieved when sintered at $1380^{\circ}C$, even the TRS is lower than the conventional sintering process.

• 터널과지하공간
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• 제25권6호
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• pp.496-504
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• 2015

로드헤더는 커팅헤드에 픽커터를 설치하여 지반을 굴착하는 장비이다. 픽커터는 일반적으로 코니컬타입을 사용하며, 코니컬 픽커터는 선단부에 마모에 강한 텅스텐카바이드 팁을 사용하여 커터의 소모를 감소시키는 굴착 도구이다. 본 연구에서는 구리광산의 망토와 역암으로 구성된 복합지반을 대상으로 로드헤더 커팅헤드에 3종류의 코니컬 픽커터를 사용하여 내구성능을 살펴보았다. 현장적용 후, 픽커터의 육안조사와 중량감소율 측정, 그리고 CT 및 SEM을 이용한 내 외부 균열조사를 수행한 결과, 하드페이싱으로 보강한 코니컬 픽커터의 내구성능이 가장 우수하였으며, 각 코니컬 픽커터의 내 외부에서는 현장적용 전과 후 모두에서 매크로 크랙 및 미세균열을 발견할 수 없었다.

• The Journal of Advanced Prosthodontics
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• 제6권6호
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• pp.491-497
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• 2014

PURPOSE. This study evaluated the influence of abutment materials on the stability of the implant-abutment joint in internal conical connection type implant systems. MATERIALS AND METHODS. Internal conical connection type implants, cement-retained abutments, and tungsten carbide-coated abutment screws were used. The abutments were fabricated with commercially pure grade 3 titanium (group T3), commercially pure grade 4 titanium (group T4), or Ti-6Al-4V (group TA) (n=5, each). In order to assess the amount of settlement after abutment fixation, a 30-Ncm tightening torque was applied, then the change in length before and after tightening the abutment screw was measured, and the preload exerted was recorded. The compressive bending strength was measured under the ISO14801 conditions. In order to determine whether there were significant changes in settlement, preload, and compressive bending strength before and after abutment fixation depending on abutment materials, one-way ANOVA and Tukey's HSD post-hoc test was performed. RESULTS. Group TA exhibited the smallest mean change in the combined length of the implant and abutment before and after fixation, and no difference was observed between groups T3 and T4 (P>.05). Group TA exhibited the highest preload and compressive bending strength values, followed by T4, then T3 (P<.001). CONCLUSION. The abutment material can influence the stability of the interface in internal conical connection type implant systems. The strength of the abutment material was inversely correlated with settlement, and positively correlated with compressive bending strength. Preload was inversely proportional to the frictional coefficient of the abutment material.

• 한국표면공학회:학술대회논문집
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• 한국표면공학회 2016년도 추계학술대회 논문집
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• pp.99-99
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• 2016

최근 공구산업은 산업 발전으로 공구의 사용 환경이 가혹화 되고, 첨단산업용 특수합금들이 발달하면서 이를 가공할 수 있는 새로운 절삭공구소재들이 개발되어지고 있다. 또한 고성능 절삭공구는 공구소재보다 코팅개발이 상대적으로 더욱 효과적이기 때문에 코팅 기술 개발이 활발히 진행되고 있다. 최근 일본에서는 새로운 코팅층 물질 개발보다는 기존의 코팅물질을 조합하거나 개량하여 성능을 향상시키는 추세이며, 이는 현재 공구산업의 효율적인 개발방향을 제시하고 있다. 기존의 빗각 증착은 기판의 각도를 변경하여 증기가 기판에 비스듬하게 입사하도록 조절하여 코팅하는 기술로 박막의 조직을 다양하게 제어하는 것이 가능하며, 구조 제어를 통한 완전화 박막을 이용한 one-batch 다기능 구현을 위하여 많은 연구가 진행되고 있다. 가공이 까다로운 소재를 가공하기 위한 공구에 적용하기 위해서 Al의 함량이 높은 AlTiN 소재가 개발되어 적용되고 있으며, 이 소재는 공구의 수명향상을 위한 표면처리 소재로 각광을 받고 있다. 본 연구에서는 음극아크 증착 시 거대입자가 박막에 증착되어 결함을 만들기 때문에 그 밀도를 낮추기 위해서 음극 아크 증착을 이용하여 공정 변화에 따른 AlTiN 박막의 표면형상을 관찰하고 특성을 평가하였다. 또한 빗각 증착을 적용하여 제작한 AlTiN 박막의 특성을 평가하였다. 고 함량의 AlTi합금 타겟을 음극 아크 소스에 장착하여 AlTiN 박막을 코팅하였다. 시편은 스테인리스강판(SUS304)과 초경(tungsten carbide; WC)을 사용하였다. 음극 아크 소스에 인가되는 전류가 낮을수록 AlTiN 박막 표면에 거대입자의 밀도가 낮아졌으며, 기판 전압과 공정압력이 높을수록 AlTiN 박막의 표면에 존재하는 거대입자의 밀도가 낮아지는 경향을 보였다. 이를 통하여 거대입자밀도를 낮추는 기초공정을 도출하였다. AlTiN 박막 제작 시 빗각을 적용한 결과 $60^{\circ}$의 빗각을 적용한 다층 박막에서 상대적으로 가장 높은 경도 값을 보였다. 본 연구를 통해 음극 아크 증착을 이용하여 거대입자의 밀도가 낮은 박막을 제작할 수 있는 공정을 도출하였고, 빗각증착을 적용하면 경도가 향상되는 결과를 확인하였다.

• 한국재료학회지
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• 제18권10호
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• pp.558-563
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• 2008

TiAlN films were deposited on WC-5Co substrates with different buffer layers by D.C. magnetron sputtering. The films were evaluated by microstructural observations and measuring of preferred orientation, hardness value, and adhesion force. As a process variable, various buffer layers were used such as TiAlN single layer, TiAlN/TiAl, TiAlN/TiN and TiAlN/CrN. TiAlN coating layer showed columnar structures which grew up at a right angle to the substrates. The thickness of the TiAlN coating layer was about $1.8{\mu}m$, which was formed for 200 minutes at $300^{\circ}$. XRD analysis showed that the preferred orientation of TiAlN layer with TiN buffer layer was (111) and (200), and the specimens of TiAlN/TiAl, TiAlN/CrN, TiAlN single layer have preferred orientation of (111), respectively. TiAlN single layer and TiAlN/TiAl showed good adhesion properties, showing an over 80N adhesion force, while TiAlN/TiN film showed approximately 13N and the TiAlN/CrN was the worst case, in which the layer was destroyed because of high internal residual stress. The value of micro vickers hardness of the TiAlN single layer, TiAlN/TiAl and TiAlN/TiN layers were 2711, 2548 and 2461 Hv, respectively.

• Tribology and Lubricants
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• 제34권6호
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• pp.241-246
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• 2018

This research addresses the improvement of tribo-systems, specifically regarding the reduction of friction and wear through tribo-coupling between tetrahedral amorphous carbon (ta-C) with different types of counterpart materials, namely bearing steel (SUJ2), tungsten carbide (WC), stainless steel (SUS304), and alumina ($Al_2O_3$). A second variable in this project is the utilization of different values of duct bias voltage in the deposition of the ta-C coating - 0, 5, 10, 15, and 20 V. The results of this research are expected to determine the optimum duct bias and best counter materials associated with ta-C to produce the lowest friction and wear. Results obtained reveal that the tribo-couple between the ta-C coating and SUJ2 balls produces the lowest friction coefficient and wear rate. In terms of duct bias changes, deposition using 5 V produces the most optimum tribological behavior with lowest friction and wear on the tribo-system. In contrast, the tribo-couple between ta-C with a WC ball causes penetration through the coating surface layer and hence high surface delamination. This study demonstrates that the most effective ta-C coating duct bias is 5 V associated with SUJ2 counter material to produce the lowest friction and wear.

• 대한치과보철학회지
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• 제50권2호
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• pp.106-111
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• 2012

연구 목적: 본 연구는 탄성의치 제작 시 주로 사용되는 polyamide를 수종의 연마방법을 사용하여 처리 후 $Candida$ $albicans$의 부착정도와 표면거칠기를 비교하고자 하였다. 연구 재료 및 방법: $25{\times}15{\times}2mm$ 크기의 polyamide 시편을 4군으로 나누어 연마재를 사용하여 기공용 lathe 연마하는 방법(기공실내 연마방법)과 각기 다른 2종의 실리콘 포인트로 진료실내 연마하는 방법, 그리고 실리콘포인트 연마 후 pumice로 연마하는 방법으로 처리하였다. $C.$ $albicans$의 부착성을 평가하기 위해 $5{\times}10^6CFU/ml$의 $C.$ $albicans$ 현탁액에 시편을 2시간 동안 침적하였고 5회 수세처리 후 한천배지에서 배양하였다. 그리고 주사전자 현미경(JSM-5900, JEOL LTd., Tokyo, Japan) 촬영을 시행하였다. Profilometer (Surf-pak; Kawasaki, Japan)를 이용하여 표면거칠기를 측정하였고 통계처리를 위하여 SPSS 18.0 프로그램을 사용하였다. 일원변량분석으로 비교 분석하였고 사후 검증은 $C.$ $albicans$의 부착성 검증을 위해 Scheffe test를 시행하였으며 표면조도검증을 위해 Tamhane's T2 test를 시행하였다(${\alpha}$=.01). 결과: 최대 거칠기 값을 보인 군은 2단계의 연마용 버를 사용한 것으로 $0.32{\mu}m{\pm}0.10$ 값을 나타냈으며, 가장 낮은 거칠기 값을 보인 것은 tungsten carbide를 사용하지 않고 기공용 lathe로만 연마를 한 군으로 $0.02{\mu}m{\pm}0.00$의 거칠기 값을 나타냈다. $C.$ $albicans$ 부착 실험에서는 기공용 lathe만을 이용한 연마방법이 가장 적은 부착수를 보였으며 다른 세 군과 유의한 차이가 발견되었다($P$<.01). 결론: 표면거칠기 및 미생물 부착능 실험 결과 기공실 연마만을 시행한 경우 유의하게 낮은 거칠기 값과 부착율을 보였다. Pumice로 추가 연마한 군은 진료실연마를 시행한 군에 비해 낮은 거칠기 값을 보였으나 $C.$ $albicans$ 부착에 있어서는 유의한 차이를 보이지 않았다($P$>.01).

• Journal of Advanced Marine Engineering and Technology
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• 제36권2호
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• pp.276-285
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• 2012

본 연구목적은 열간압연용 런-아웃 테이블 롤러 표면의 기계적 성질을 개선하기 위해 다공질 자용성 합금으로 피복하는 방법을 개발하는 것이다. 열간압연에서 런-아웃 테이블의 롤러 내구성을 높이기 위해서는 고온에서 롤러표면의 경도를 높게 유지해야 하고, 내마모성, 내식성, 내열성, 내소부성 및 내응착성의 향상을 유지하여야 한다. 또한, 고온의 열연 강판을 안정적으로 이송할 수 있도록 하기 위해서는 롤러표면에 적절한 마찰계수를 유지하도록 하여야 하고, 롤러와 강판 사이에 미끄럼 발생이 없어야 한다. 본 연구에서는 자용성 합금에 텅스텐카바이드를 첨가시켜 서메트화하여 롤러의 내마모성을 증대시켰고, 미세 철분말을 롤러표면에 피복하여 다공질을 만들어 마찰계수를 높이고 붙잡음성을 향상시켰다. 그 결과, Ni-Cr 피복 롤러에 비하여 다공질 자용성 합금 피복 롤러는 피복층에 철분이 5 ~ 10 wt%로 많이 함유되어 재용융 공정에서 전기로로 가열하여 일부분만 합금화되고 나머지는 산화 및 용해에 의해 탈락되어 다공질로 나타나 강판과의 붙잡음성을 향상시켰다.

• 대한치과의사협회지
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• 제53권9호
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• pp.644-655
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• 2015

Purpose: This study was conducted to evaluate the effect of the fixture abutment connection type and diameter on the screw joint stability in external butt joint for 2nd surgery and internal cone connected type implant system for 1st and 2nd surgery using ultimate fracture strength. Materials and Methods: USII system, SSII system and GSII system of Osstem Implant were used. Each system used the fixture with two different diameters and cement-retained abutments, and tungsten carbide / carbon coated abutment screws were used. Disc shaped stainless steel metal tube was attached using resin-based temporary cement. The experimental group was divided into seven subgroups, including the platform switching shaped specimen that uses a regular abutment in the fixture with a wide diameter in USII system. A static load was increased to the metal tube at 5mm deviated point from the implant central axis until it reached the compression bending strength at a rate of 1mm/min. Then the deformations and patterns of fracture in threaded connection were compared. Results and Conclusion: 1. In the comparison between the Regular diameter, compression bending strength of SSII system was higher than USII system and GSII system. There was no significant difference between USII system and GSII system. 2. In the comparison between wide diameter, compression bending strength was increased in the order of GSII system, USII system, and SSII system. 3. In comparison between the implant diameter, compression bending strength of the wide diameter was greater than the regular diameter in any system(P<0.05). 4. There was no significant difference between the platform switching (III group) and the regular diameter (I group) in USII system. 5. In USII system, fracture of abutment screw and deformation of both fixture and abutment were observed in I, II and III subgroups. 6. Failure pattern of SSII system, which was the fracture of abutment screw and deformation of the abutment and fixture, was observed in both IV and V subgroups. Fracture of some fixtures was observed in subgroup V. 7. Failure pattern of GSII system, which was the fracture of the abutment screw and deformation of the fixture and the abutment, was observed in both VI and VII subgroups. Apart from other subgroups, subgroup VII demonstrated no bending neither the fracture at the top of the fixture. The compressive deformation of internal slope in the fixture was the only thing observed in subgroup VII.