Browse > Article
http://dx.doi.org/10.4150/KPMI.2011.18.3.262

The Characteristic Changes of Sintered WC-10Co Fabricated by PIM Method with Different Carbon Content  

Kang, Sang-Dae (School of Material Science and Engineering, i-Cube Center, Gyeongsang National University)
Park, Dong-Wook (School of Material Science and Engineering, i-Cube Center, Gyeongsang National University)
Kwon, Young-Sam (Cetatech, Inc.)
Cho, Kwon-Koo (School of Material Science and Engineering, i-Cube Center, Gyeongsang National University)
Ahn, In-Shup (School of Material Science and Engineering, i-Cube Center, Gyeongsang National University)
Publication Information
Journal of Powder Materials / v.18, no.3, 2011 , pp. 262-268 More about this Journal
Abstract
In order to investigate the microstructure and mechanical properties of WC-10 wt% Co insert tool alloy fabricated by PIM (Powder Injection Molding) process, the feedstock of WC-10 wt% and wax used as a kind of binder were mixed together by two blade mixer. After injection molding, the debinding process was carried out by two-steps. First, solvent extraction, in which the binder was eliminated by putting the specimen into normal hexane for 24 hrs at $60^{\circ}C$, and subsequently thermal debinding which was conducted at $260^{\circ}C$ and $480^{\circ}C$ for 6 hrs in the mixed gas of $H_2/N_2$, respectively. Meantime, in order to compensate the decarburization due to hydrogen, 1.2~1.8% of carbon was added to ensure the integrity of the phase. Finally, the specimens were sintered in vacuum under different temperatures, and the relative density of 99.8% and hardness of 2100 Hv can be achieved when sintered at $1380^{\circ}C$, even the TRS is lower than the conventional sintering process.
Keywords
Debinding; Tungsten carbide (WC); Sintering; Powder injection moulding (PIM);
Citations & Related Records
연도 인용수 순위
  • Reference
1 R. Kitakawa: Recent trends of coated tool, Mach. Tool, 33 (1989) 27.
2 H. S. Kalish: Status report: cutting tool materials, Met. Prog., 124 (1983) 21.
3 Yoshimitsu Kankawa: USA, US 6051184 (2000).
4 D.-G. Ahn: J. Korean Society for Nondestructive Testing., 20 (2000) 438.
5 R. M. German: Powder Injection Molding, MPIF. Princeton, NJ (1990).
6 R. M. German: Sintering Theory and Practice, John Wiley & Sons, INC., (1996).
7 M. Leiderman, O. Botstein and A. Rosen: Powder Metall., 4 (1997) 219.
8 O. Pacher, W. Schintlmeister and T. Raine: Powder Metall., 4 (1980) 189.
9 S. H. Choi and I. S. Ahn: Research on Chemical Intermediates., 36 (2010) 743.   DOI
10 Baiyun Huang, Shuquan Liang and Xuanhui Qu: J. Mater. Proc. Tech., 137 (2003) 132.   DOI   ScienceOn
11 ASM International: ASM Metals Handbook-Powder Metal Technologies and Applications (9th ed.), 7 (1998) 385.
12 MPIF, Standard Test Methods for Metal Powders and Powder Metallurgy Products-standard 41, (2010 ed.), MPIF, (2010).