DOI QR코드

DOI QR Code

The Characteristic Changes of Sintered WC-10Co Fabricated by PIM Method with Different Carbon Content

금속분말사출성형법으로 제조된 WC-10Co계 초경합금 소결체의 탄소첨가량에 따른 특성변화

  • Kang, Sang-Dae (School of Material Science and Engineering, i-Cube Center, Gyeongsang National University) ;
  • Park, Dong-Wook (School of Material Science and Engineering, i-Cube Center, Gyeongsang National University) ;
  • Kwon, Young-Sam (Cetatech, Inc.) ;
  • Cho, Kwon-Koo (School of Material Science and Engineering, i-Cube Center, Gyeongsang National University) ;
  • Ahn, In-Shup (School of Material Science and Engineering, i-Cube Center, Gyeongsang National University)
  • 강상대 (국립 경상대학교 나노 신소재공학부.금속재료공학과) ;
  • 박동욱 (국립 경상대학교 나노 신소재공학부.금속재료공학과) ;
  • 권영삼 ((주)쎄타텍) ;
  • 조권구 (국립 경상대학교 나노 신소재공학부.금속재료공학과) ;
  • 안인섭 (국립 경상대학교 나노 신소재공학부.금속재료공학과)
  • Received : 2011.03.23
  • Accepted : 2011.05.13
  • Published : 2011.06.28

Abstract

In order to investigate the microstructure and mechanical properties of WC-10 wt% Co insert tool alloy fabricated by PIM (Powder Injection Molding) process, the feedstock of WC-10 wt% and wax used as a kind of binder were mixed together by two blade mixer. After injection molding, the debinding process was carried out by two-steps. First, solvent extraction, in which the binder was eliminated by putting the specimen into normal hexane for 24 hrs at $60^{\circ}C$, and subsequently thermal debinding which was conducted at $260^{\circ}C$ and $480^{\circ}C$ for 6 hrs in the mixed gas of $H_2/N_2$, respectively. Meantime, in order to compensate the decarburization due to hydrogen, 1.2~1.8% of carbon was added to ensure the integrity of the phase. Finally, the specimens were sintered in vacuum under different temperatures, and the relative density of 99.8% and hardness of 2100 Hv can be achieved when sintered at $1380^{\circ}C$, even the TRS is lower than the conventional sintering process.

Keywords

References

  1. Baiyun Huang, Shuquan Liang and Xuanhui Qu: J. Mater. Proc. Tech., 137 (2003) 132. https://doi.org/10.1016/S0924-0136(02)01100-7
  2. ASM International: ASM Metals Handbook-Powder Metal Technologies and Applications (9th ed.), 7 (1998) 385.
  3. MPIF, Standard Test Methods for Metal Powders and Powder Metallurgy Products-standard 41, (2010 ed.), MPIF, (2010).
  4. R. Kitakawa: Recent trends of coated tool, Mach. Tool, 33 (1989) 27.
  5. H. S. Kalish: Status report: cutting tool materials, Met. Prog., 124 (1983) 21.
  6. Yoshimitsu Kankawa: USA, US 6051184 (2000).
  7. D.-G. Ahn: J. Korean Society for Nondestructive Testing., 20 (2000) 438.
  8. R. M. German: Powder Injection Molding, MPIF. Princeton, NJ (1990).
  9. R. M. German: Sintering Theory and Practice, John Wiley & Sons, INC., (1996).
  10. M. Leiderman, O. Botstein and A. Rosen: Powder Metall., 4 (1997) 219.
  11. O. Pacher, W. Schintlmeister and T. Raine: Powder Metall., 4 (1980) 189.
  12. S. H. Choi and I. S. Ahn: Research on Chemical Intermediates., 36 (2010) 743. https://doi.org/10.1007/s11164-010-0176-8