• Title/Summary/Keyword: three-dimensional characterization

검색결과 141건 처리시간 0.031초

4개의 폴리카프로락톤 가지 코어를 가지는 스타형 폴리카프로락톤의 합성 및 분석 (Synthesis and characterization of Star Shape Polycaprolactone containing 4-Arm Polycaprolactone Core)

  • An, Sung-Guk;Cho, Chang-Gi
    • 한국섬유공학회:학술대회논문집
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    • 한국섬유공학회 2002년도 봄 학술발표회 논문집
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    • pp.199-202
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    • 2002
  • The synthesis of materials with controlled composition and architectures continues to be a focus of considerable current research. Dendritic multiarm polymers such as dendrimer, hyperbranched polymer, and star polymers are three dimensional macromolecules, in which a large number of linear arms of similar molecular weight and narrow molecular weight distribution emanate from a central core. (omitted)

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STRUCTURES OF GEOMETRIC QUOTIENT ORBIFOLDS OF THREE-DIMENSIONAL G-MANIFOLDS OF GENUS TWO

  • Kim, Jung-Soo
    • 대한수학회지
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    • 제46권4호
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    • pp.859-893
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    • 2009
  • In this article, we will characterize structures of geometric quotient orbifolds of G-manifold of genus two where G is a finite group of orientation preserving diffeomorphisms using the idea of handlebody orbifolds. By using the characterization, we will deduce the candidates of possible non-hyperbolic geometric quotient orbifolds case by case using W. Dunbar's work. In addition, if the G-manifold is compact, closed and the quotient orbifold's geometry is hyperbolic then we can show that the fundamental group of the quotient orbifold cannot be in the class D.

Pentiptycene Diacetylene의 합성 (Synthesis of Pentiptycenediacetylene)

  • 한정민;권형준
    • 통합자연과학논문집
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    • 제2권2호
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    • pp.69-72
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    • 2009
  • Pentiptycenediacetylene is very useful precursor materials for the synthesis of conducting polymer materials. The incorporation of rigid three-dimensional pentiptycene moieties into conjugated polymer backbones would offer several design advantages. They prevent ${\pi}$-stacking of the polymer backbones and thereby maintain high fluorescence quantum yields and spectroscopic stability in thin films. The pentiptycenediactylene was synthesized and characterized by 1H- and 13C-NMR spectroscopy.

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Structural characterization of ladder-type cadmium(II) citrate complex, (C3H12N2)[{Cd(H2O)(C6H5O7)}2]·6H2O

  • Kim, Chong-Hyeak;Lee, Sueg-Geun
    • 분석과학
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    • 제20권4호
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    • pp.355-360
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    • 2007
  • The title complex, $(C_3H_{12}N_2)[\{Cd(H_2O)(C_6H_5O_7)\}_2]{\cdot}6H_2O$, I, has been prepared and its structure characterized by FT-IR, EDS, elemental analysis, ICP-AES, and X-ray single crystallography. It is triclinic system, $P{\bar{1}}$ space group with a = 10.236(2), b = 11.318(2), c = $13.198(2){\AA}$, ${\alpha}=77.95(1)^{\circ}$, ${\beta}=68.10(1)^{\circ}$, ${\gamma}=78.12(1)^{\circ}$, V = $1373.5(3){\AA}^3$, Z = 2. Complex I has constituted by protonated 1,3-diaminopropane cations, citrate coordinated cadmium(II) anions, and free water molecules. The central cadmium atoms have a capped trigonal prism geometry by seven coordination with six oxygen atoms of three different citrate ligands and one water molecule. Citrate ligands are bridged to three different cadmium atoms. Each cadmium atom is linked by carboxylate and hydroxyl groups of citrate ligand to construct an one-dimensional ladder-type assembly structure. The polymeric crystal structure is stabilized by three-dimensional networks of the intermolecular O-H${\cdots}$O and N-H${\cdots}$O hydrogen-bonding interaction.

3 차원 하이드로젤 지지체 제작을 위한 고분자 몰드의 가공 특성에 대한 실험적 연구 (Experimental Study of Machining Process of Polymer Mold for Fabrication of Three-Dimensional Hydrogel Scaffold)

  • 이필호;이상원;김대훈;김시현;성종환;정하승
    • 대한기계학회논문집B
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    • 제37권7호
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    • pp.669-674
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    • 2013
  • 최근 생체모사 융모는 검체검사 및 신약개발 등의 분야에서 비용 및 윤리적 문제를 해결하기 위한 대안으로 부각되고 있다. 본 연구는 생체모사 융모구조 3 차원 하이드로젤 지지체의 효과적인 제작을 위한 고분자 몰드의 가공에 관한 내용을 다루고 있다. 고분자 몰드 제작을 위하여 레이저 가공 및 마이크로 드릴링 가공 프로세스를 적용한 실험이 수행되었다. 가공 프로세스 최적화를 위하여 다양한 조건에서 레이저 가공 및 마이크로 드릴링 실험을 진행하였으며, 이 때 폴리카보네이트(poly-carbonate) 고분자 몰드가 사용되었다. 전자주사현미경 및 광학현미경 관측을 통하여 고분자 몰드 및 생체모사 융모 형상을 관측하였다. 실험결과 생체모사 융모는 레이저 가공 및 마이크로 드릴링을 적용한 경우 모두 적절한 형상을 보이는 것으로 확인되었다.

A Brief Overview of Atom Probe Tomography Research

  • Gault, Baptiste
    • Applied Microscopy
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    • 제46권3호
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    • pp.117-126
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    • 2016
  • Atom probe tomography (APT) has been fast rising in prominence over the past decade as a key tool for nanoscale analytical characterization of a range of materials systems. APT provides three-dimensional mapping of the atom distribution in a small volume of solid material. The technique has evolved, with the incorporation of laser pulsing capabilities, and, combined with progress in specimen preparation, APT is now able to analyse a very range of materials, beyond metals and alloys that used to be its core applications. The present article aims to provide an overview of the technique, providing a brief historical perspective, discussing recent progress leading to the state-of-the-art, some perspectives on its evolution, with targeted examples of applications.

광원주위의 3차원 광선속 측정 및 평가 (Measurement and Characterization of Three Dimensional Luminous Flux)

  • 최종운;유문종
    • 대한전기학회논문지:전기물성ㆍ응용부문C
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    • 제52권7호
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    • pp.314-318
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    • 2003
  • This paper describes the construction, measurement, and characterization of an instrument for the distribution of luminous flux. This is done by measuring the flux around a light source while a detector and a source is rotating, and integrating it over an entire imaginary surface surrounding the source. We make a gonio radiometer to realize the scales of total luminous flux and geometrically integrate to get total spectral flux from standards of irradiance and illuminance. The uncertainties of a total flux in the gonioradiometry are 1.3%, and 0.4% below the standard lamps of NIST and NIM for each other.

An improved 1D-model for computing the thermal behaviour of concrete dams during operation. Comparison with other approaches

  • Santillan, D.;Saleteb, E.;Toledob, M.A.;Granados, A.
    • Computers and Concrete
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    • 제15권1호
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    • pp.103-126
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    • 2015
  • Thermal effects are significant loads for assessing concrete dam behaviour during operation. A new methodology to estimate thermal loads on concrete dams taking into account processes which were previously unconsidered, such as: the evaporative cooling, the night radiating cooling or the shades, has been recently reported. The application of this novel approach in combination with a three-dimensional finite element method to solve the heat diffusion equation led to a precise characterization of the thermal field inside the dam. However, that approach may be computationally expensive. This paper proposes the use of a new one-dimensional model based on an explicit finite difference scheme which is improved by means of the reported methodology for computing the heat fluxes through the dam faces. The improved model has been applied to a case study where observations from 21 concrete thermometers and data of climatic variables were available. The results are compared with those from: (a) the original one-dimensional finite difference model, (b) the Stucky-Derron classical one-dimensional analytical solution, and (c) a three-dimensional finite element method. The results of the improved model match well with the observed temperatures, in addition they are similar to those obtained with (c) except in the vicinity of the abutments, although this later is a considerably more complex methodology. The improved model have a better performance than the models (a) and (b), whose results present larger error and bias when compared with the recorded data.

Drosophila sp.(robusta species group)의 난황 단백질의 분리 및 부분적 화학적 특성 (Isolation and Partial Chemical Characterization of the Yolk Proteins from Drosophila sp. (robusta species group))

  • Kim, Se-Jae;Gi
    • 한국동물학회지
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    • 제35권1호
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    • pp.17-22
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    • 1992
  • The three yolk polypeptides have been isolated and partially characterized. Their molecular weights of YPI, YP2, and YP3 were 48, 000, 47, 000, and 46, 000, respectivelv, as judged by SDS-polyacrvlamide gel electrophoresis. They have different digestion products upon in situ peptide mapping by limited proteolysis. Two-dimensional gel electrophoresis showed that their isoelectric points were heterogeneous from 5.92 to 6.54. And thew showed three different antigen-antibody reactions when each polvpeptides is reacted with antisera made to a mixture of all of three. These data reported here indicate that the yolk proteins are consisted of distinctive polypeptides in Drosophlla sp. (robusta species group).

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위상측정방식을 이용한 3차원 초음파 풍향풍속계의 특성분석 (Characterization of three-dimensional ultrasonic anemometer using phase measurement)

  • 박도현;예윤해
    • 센서학회지
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    • 제15권6호
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    • pp.442-448
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    • 2006
  • Ultrasonic anemometers using pulse envelope detection-based method are standard instruments in most meteorological studies. In this paper, a new phase measurement method is tried to achieve the enhanced resolution without changing dimensions. The measurement sensitivity, dynamic range, and measurement speed of the new instrument are 0.2 mm/s, 13.3 m/s, and 13 measurements/sec, respectively. A graphic user interface is added to show the velocity and direction of the wind with the speed of sound and temperature of the wind in the 3 dimensional space. The new anemometer could be useful for the measurement of the air speed, the flow of fluids, and even air flow inside the downtown buildings.