• Title/Summary/Keyword: temperature limit

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Quantitation and Validation of Atorvastatin using HPLC-UV

  • Heine, Daniel;Yong, Chul-Soon;Kim, Jung-Sun
    • Journal of Pharmaceutical Investigation
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    • v.37 no.3
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    • pp.187-192
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    • 2007
  • A reversed phase HPLC analysis of atorvastatin (AS) standard solution was performed using diclofenac (DF) as internal standard. Column oven temperature, flow rate and the composition of the mobile phase were varied in order to determine a practical system setup using a C18 column and UV detector. Two C18 columns of different length were compared regarding their influence on the AS peak shape. Based on these preliminary experiments a validation study was performed utilizing a C18 column at $62^{\circ}C$ with a mobile phase consisting of sodium phosphate buffer (0.05 M, pH 4.0), methanol and acetonitrile (40:50:10, v/v/v). The detection limit for AS was $0.1{\mu}g/ml$ and inter- and intra-day calibration curves were linear over a concentration range of $0.2-50{\mu}g/ml$. Accuracy and precision were satisfactory in the AS concentration range of $0.5-50{\mu}g/ml$.

Bridgeless High Efficiency ZVZCS Power Factor Correction Circuit for PDP Power Module (PDP용 브리지가 없는 고효율 ZVZCS 역률개선회로)

  • Cho Kyu-Min;Yu Byung-Gyu;Moon Gun-Woo
    • Proceedings of the KIPE Conference
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    • 2004.07b
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    • pp.704-708
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    • 2004
  • Recently, many nation have released standard such as IEC 61000-3-2 and IEEE 59, which impose a limit on the harmonic current drawn by equipment connected to AC line in order to prevent the distortion of an AC Line. Therefore, Plasma Display Panel (PDP) which is highlightened in digital display device also has the Power Factor Correction (PFC) circuit to meet the harmonic requirements. In PDP power module, the conventional boost converter is usually used for the PFC circuit. However, it comes serious thermal problem on it's bridge diode due to heat of PDP, and therefore the system stability is not guaranteed. In this paper, the bridgeless boost converter, which is used for PFC circuit of the PDP power module, is designed and verified the possibility of the application in a practical product in a view of efficiency, component count, temperature and etc.

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The effects of congestion cost reduction by the application of Superconducting cable (초전도케이블에 의한 전력계통의 혼잡비용 저감 효과)

  • Kim, Hyun-Houng;Lee, Geun-Jun
    • Proceedings of the KIEE Conference
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    • 2005.07a
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    • pp.66-68
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    • 2005
  • In Korea power system, the transfer capability of transmission line is limited by the voltage stability and it is difficult to construct new iron tower due to incremental interest for environmental problem and construction costs. Recently, HTS cable could be one of the countermeasures to solve the transfer limit because of it is transported to large power with compact size However, the characteristic of HTS cable have a various problem. This paper presents the effects of congestion cost reduction by the application of HTS (High-Temperature Superconducting) cable. In this paper, the transmission ability before and after application of HTS cable are examined in a viewpoint for voltage stability. therefore, the effects of congestion cost reduction by HTS cable.

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Effect of NaCl on Germination of Artiplex gmelini and Pharagmites communis (갈대 및 가는갯능쟁이의 발아에 미치는 NaCl의 효과)

  • 김관수
    • Journal of Plant Biology
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    • v.28 no.3
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    • pp.253-259
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    • 1985
  • The results of the conducted experiment obtained basic data on seed germination for Phragmites communis and Atriplex gmelini were; Seed germination was not influenced till 0.5% NaCl, but at over 1.0% NaCl it dropped remarkably. The germination limit fro degree of NaCl was 2.0% in Phragmites communis. Atriplex gemelini was 2.5% and in accordance with the increase of the degree of NaCl. Germination speed showed a negative correlation being highly significant and the germination period lengthened. Compared with growing top plants, growth of roots was largely influenced by a high degree of NaCl. In accordance with the rise of temperature, the germination rate, and speed of both plants remarkably increased and the germination period was shortened. Ubride of Atriplex gmelini was germinated at the early days of picking but was not as the passing of the period. The seeds also did not germinated likewise Ubride. By a seedcoat breaking germination became 81%. During 20 min soaking treatment in conc H2SO4 seed germination possibility of 63% was known to be hard. Adequate soaking time in conc H2SO4 was 17.5 min.

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An Enhanced Architecture of CMOS Phase Frequency Detector to Increase the Detection Range

  • Thomas, Aby;Vanathi, P.T.
    • JSTS:Journal of Semiconductor Technology and Science
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    • v.14 no.2
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    • pp.198-201
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    • 2014
  • The phase frequency detector (PFD) is one of the most important building blocks of a phase locked Loop (PLL). Due to blind-zone problem, the detection range of the PFD is low. The blind zone of a PFD directly depends upon the reset time of the PFD and the pre-charge time of the internal nodes of the PFD. Taking these two parameters into consideration, a PFD is designed to achieve a small blind zone closer to the limit imposed by process-voltage-temperature variations. In this paper an enhanced architecture is proposed for dynamic logic PFD to minimize the blind-zone problem. The techniques used are inverter sizing, transistor reordering and use of pre-charge transistors. The PFD is implemented in 180 nm technology with supply voltage of 1.8 V.

A Study on the fracture behavior of surface treated Al 5083-H131 alloy under the high velocity impact (표면처리된 Al 5083-H131 합금의 고속 충격 거동에 관한 연구)

  • 손세원;김희재;홍성희;황도연
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 1997.10a
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    • pp.820-824
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    • 1997
  • In order to investigate the effect of surface treatment(Anodizing) and rolling in Al 5083-H131 alloy, ballistic testing was conducted. Ballistic resistance of these materials. was measured by protection ballistic limit(V$_{50}$), a statical velocity with 50% probability for incomplete penetration. Fracture behaviors and ballistic tolerance, described by penetration modes, are observed respectfully, resulting from V$_{50}$ test and Projectile Through Plates(PTP) test at velocities greater than V$_{50}$. PTP tests were conducted with 0$^{\circ}$obliquity at room temperature were also conducted with projectiles that were able to achieve near or complete penetration during PTP tests. Resistance to penetration, and penetration modes of Al 5052-H34 alloy, compared to those of Al 5083-H131 alloy.alloy.

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A Study on the Deep drawing drawability and Analyzing process of AZ31B Magnesium Sheet at Warm and Hot temperature (AZ31B 마그네슘 판재의 온,열간 딮드로잉 성형성 및 공정해석)

  • Han, S.H.;Choo, D.K.;Kang, C.G.
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2006.05a
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    • pp.48-52
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    • 2006
  • The drawability of AZ31B magnesium sheet is estimated at various temperatures (200, 250, 300, 350 and $400^{\circ}C$), and forming speed (20, 50, 100 mm/min), thickness (0.5, 0.8, 1.0, 1.4 mm). The deep drawing process of circular cup and square cup were used in forming experiments. Experimental and FEM analysis are performed to investigate drawability and affection of controlled blank holding force. Through the controlled blank holding force, drawability was improved. This result is verified by FEM analysis. Through the observation of microstructure, the main cause is investigated as a quantity of the dynamic recrystallization.

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Thermodynamic Design of HTS Current Leads Conduction-Cooled by 2-Stage Cryocooler (2단냉동기로 전도냉각되는 HTS전류도입선의 열역학 설계)

  • 장호명
    • Proceedings of the Korea Institute of Applied Superconductivity and Cryogenics Conference
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    • 1999.02a
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    • pp.198-201
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    • 1999
  • An optimal cooling method for HTS(high Tc superconductor) current leads has been analytically sought to minimize the required refrigerator power. The binary current lead is a series combination of a normal metal conductor at the warmer part and an HTS at the colder part. The lead is cooled by direct contacts with a two-stage cryocooler at the joint and at the cold end. It is clearly proven that there exists unique optimal values for the joint temperature and the current density to minimize the refrigerator power per unit current. the actual power input to the cryocooler in the optimal conditions is compared with its thermodynamic limit, and some significant issues in practical design are presented with a useful graphical method.

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Properties of Sequential Lateral Solidification (SLS) Crystallized Poly-Si Films and Melting Process Simulation

  • Kim, Yong-Hae;Sohn, Choong-Yong;Chung, Choong-Heui;Ko, Young-Wook;Lee, Jin-Ho
    • 한국정보디스플레이학회:학술대회논문집
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    • 2003.07a
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    • pp.248-251
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    • 2003
  • The large size grain of poly-Si film is obtained above the upper limit of excimer laser energy at which the random nucleation occurs. We simulate the time dependent temperature profile of ${\alpha}-Si/SiO_2/Si$ substrate structure according to the excimer laser energy with $ANSYS^{\circledR}$ simulator. As the thickness is increased, the laser energy for the melting of ${\alpha}-Si$ film is increased.

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A Study on the Application Analysis of the Resistive type Superconducting Fault Current Limiters using PSCAD/EMTDC (PSCAD/EMTDC를 이용한 저항형 초전도한류기의 계통적용분석 연구)

  • Heo Tae Jeon;Bang Jong Hyun;Bae Hyeong Thaek;Park Min Won;Yu In Keun
    • Progress in Superconductivity and Cryogenics
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    • v.7 no.1
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    • pp.25-31
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    • 2005
  • Since the discovery of the high temperature superconductors many researches have been performed for the practical applications of superconductivity technologies in various fields. As results, significant progress has been achieved. Especially, Superconducting Fault Current Limiter (SFCL) offers an attractive means In limit fault current in power systems. HTS resistive type SFCL is based on the ultra fast transition from the superconducting (non resistive) state to the normal (resistive) state by overstepping the critical current density, In this study, the simulation method of resistive type superconducting fault current limiter using EMTDC is proposed and the developed EMTDC model of SFCL is applied to the modeled power network using the Parameters of real system.