• Title/Summary/Keyword: tem-8

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TEM sample preparation using micro-manipulator for in-situ MEMS experiment

  • Hyunjong Lee;Odongo Francis Ngome Okello;Gi-Yeop Kim;Kyung Song;Si-Young Choi
    • Applied Microscopy
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    • v.51
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    • pp.8.1-8.7
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    • 2021
  • Growing demands for comprehending complicated nano-scale phenomena in atomic resolution has attracted in-situ transmission electron microscopy (TEM) techniques for understanding their dynamics. However, simple to safe TEM sample preparation for in-situ observation has been limited. Here, we suggested the optical microscopy based micro-manipulating system for transferring TEM samples. By adopting our manipulator system, several types of samples from nano-wires to plate-like thin samples were transferred on micro-electro mechanical systems (MEMS) chip in a single step. Furthermore, the control of electrostatic force between the sample and the probe tip is found to be a key role in transferring process.

Input Power Determination of TEM Cell Due to SAR for Mobile Phone Wave Blood Exposure (휴대폰 전자파의 혈액 조사를 위한 SAR별 TEM 셀의 입력 전력 산출)

  • Youn Ji-Hun;Son Tae-Ho
    • The Journal of Korean Institute of Electromagnetic Engineering and Science
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    • v.16 no.8 s.99
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    • pp.810-814
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    • 2005
  • Input power for TEM cell apparatus due to SAR(Specific Absorption Rate) for culture blood cell is determined by the transmission and reflection measurement of blood into the TEM cell. Blood cell with skin cell are reference culture cells for the study of EM wave effect. Exposure RF power from exposure apparatus to culture cell should not only exact for SAR value, but also should be based on the theoretical theory. In this paper, insertion loss of 50 g blood was measured to know exposure power per gram for culture blood cell, and input power of TEM cell due to SAR 0.8, 1.6, 3, 4 mW/g using the measured data are delivered. This study is for applying to EM wave exposure apparatus to culture cell.

Study on Surface Damage of Specimen for Transmission Electron Microscopy(TEM) Using Focused Ion Beam(FIB) (집속 이온빔을 이용한 투과 전자 현미경 시편의 표면 영향에 관한 연구)

  • Kim, Dong-Sik
    • 전자공학회논문지 IE
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    • v.47 no.2
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    • pp.8-12
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    • 2010
  • TEM is a powerful tool for semiconductor material analyses in structure or biological sample in micro structure. TEM observation need to make to coincide specimens for special purpose. in this paper, we have experimented for minimum surface damage on bulk wafer and patterned specimen by various conditions such as accelerating energy, depth of ion beam, ion milling types, and etc. in various specimen preparation methods by FIB (Focus Ion Beam). The optimal qualified specimens are contain low mounts of surface damage(about 5 nm) on patterned specimen.

Microstructure and Third Order Optical Nonlinearities of Ion-Implanted and Thermally Annealed $Cu-SiO_2$ Thin Films

  • 채이;이민영;김현경;문대원
    • Bulletin of the Korean Chemical Society
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    • v.18 no.8
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    • pp.886-889
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    • 1997
  • The crystal structure and optical properties of copper nanoparticles, prepared in fused silica by ion-implantation and subsequent heat-treatment, were characterized by X-ray, TEM, linear absorption, and degenerate four-wave mixing (DFWM) technique. The X-ray data show fcc lattice structure of the nanocrystals and their size was measured as 8-20 nanometer by high resolution TEM. Using DFWM, the third-order nonlinear optical coefficient of the Cu-SiO2 thin films was measured as 0.4-1.1×10-8 esu in the surface plasmon resonance absorption region (540-570 nm).

Development of TEM Coil for Animal Experiments at 3T MRI System

  • Chu, Myung-Ja;Choe, Bo-Young;Kim, Kyung-Nam;Chung, Sung-Taek;Oh, Chang-Hyun;Lee, Hyoung-Koo;Suh, Tae-Suk
    • Proceedings of the Korean Society of Medical Physics Conference
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    • 2002.09a
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    • pp.365-366
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    • 2002
  • A novel TEM resonator coil was developed for the imaging of small animals. The functional elements of the TEM resonator were 8 inner conductors, distributed in a cylindrical pattern and connected at the ends with capacitors to the cylindrical outer shield. The TEM resonator coil with cavity elements was robust to the surrounding influences due to the self-shielding structure. The TEM resonator coil with high Q factor could provide high quality MR images at 3.0T MRI system. Also, the TEM resonator coil has an advantage for a fine tune with length adjustment of each cavity elements. Thus, The TEM resonator coil at 3.0T, even higher field could be used in the research studies.

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Extended-Spectrum $\beta$-Lactamase (ESBL) Typing of Klebsiella pneumoniae Isolated from Clinical Specimen in Pusan (부산시내 종합병원의 임상 검체에서 분리된 Extended -Spectrum $\beta$-Lactamase 생성 Klebsiella pneumoniae의 형별 분류)

  • 김윤태;이훈구
    • Korean Journal of Microbiology
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    • v.36 no.3
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    • pp.221-227
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    • 2000
  • This study was performed to investigate the biological characteristics of twenty isolates of extended spectnlm $\beta$-lactamase (ESBL) producing Klebsiellapnezm~onia collected kom the various clinical specimens of three hospitals in Pusan. Isoelectric focusing (IEF) and PCR were used to determine the types of $\beta$-lactamase gene in this study. Twenty isolates of ESBL producing Klebsiellnp~ieun~or~iae could be divided by PCR, such as TEM type (I1 strains), SHV type (8 strains); non TEM non SHV type (1 strain). In the isoelechic focusing test, the PI of TEM type was 5.2-6.0 and that of SHV type was 6.9-7.4. According to the pI value and PCR bands, twenty strains of ESBL Klebsiellapneumoniae were divided into 5 types: TEM type @I 5.2-6.0; 1080 bp on PCR band), TEM + SHV type (pI 5.2-6.0; andpI 7.0-7.4; 1080 bp and 599 bp on PCR band), SHV type (pl7.0-7.4; 599 bp on PCR band), non TEM non SHV type, and otber type (PCR result was SHV type but pI was not detected).

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Characterization of cefotaxime-resistant Escherichia coli isolated from wastewater treatment plant in Daegu (대구지역 폐수처리장에서 분리한 cefotaxime-resistant Escherichia coli의 특성)

  • Kim, Hwan-Deuk;Park, Dae-Hyun;Lee, Mi-Ree;Kim, Eun-Jeong;Cho, Jae-Keun
    • Korean Journal of Veterinary Service
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    • v.37 no.4
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    • pp.225-231
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    • 2014
  • In this study, 185 cefotaxime-resistant Escherichia coli were isolated from different stages of a wastewater treatment plant (WWTP) in Daegu in Korea. Among them, 99.5% (184 isolates) originated from raw sewage and 0.5% (1 isolates) from the final effluent. Cefotaxime-resistant E. coli were high resistant to ampicillin, piperacillin, cefazolin, cephalothin, cefachlor and cefamandole (99.5~100%). About 93% of the cefotaxime-resistant E. coli were extended-spectrum ${\beta}$-lactamases (ESBL)-producing E. coli. The $bla_{TEM+CTX}$ gene was the most predominant of the ESBL genes (72.5%), followed by $bla_{CTX-M}$ (16.2%), $bla_{TEM}$ (8.7%), $bla_{TEM+CTX+SHV}$ (1.1%), $bla_{TEM+SHV}$, $bla_{TEM+OXA}$, and $bla_{TEM+CTX+SHV}$ (respectvely 0.5%). Class 1 and 2 integron were found in 49.7% and class 3 integron was not found. All of integron positive isolates were multiresistant (i.e. resistant to four or more antibiotics). Our findings showed WWTP is contaminated with antibiotic resistant bacteria with resistance genes.

Modified TEM Horn for Enhanced Radiation Characteristics at Low Frequency

  • Kim, Jae Sik;Park, Hyeong Soon;Yoon, Young Joong;Ryu, Jiheon;Choi, Jin Soo
    • Journal of electromagnetic engineering and science
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    • v.14 no.2
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    • pp.74-78
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    • 2014
  • This paper presents a modified TEM horn that improves radiation characteristics at a low frequency region. The proposed antenna consists of an asymmetric TEM (ATEM) horn and a loop structure with an elliptical shape. The bandwidth and gain at low frequency region can be enhanced by using the ATEM horn configuration and adding a loop structure with an elliptical shape to the ATEM horn. The bandwidth of the proposed antenna is from 2.14 to over 20 GHz, whereas that of the conventional TEM horn is from 2.7 to over 20 GHz, where the dimensions of both antennas are the same except for the thickness of the loop structure. The physical and electrical dimensions of the proposed antenna are $60mm{\times}62.5mm{\times}64mm$ ($width{\times}height{\times}length$) and $0.428{\lambda}_L{\times}0.445{\lambda}_L{\times}0.456{\lambda}_L$, where ${\lambda}_L$ corresponds to the lowest frequency of the bandwidth. The realized gain of the proposed antenna is improved by 0.802 dB on average at the low frequency region (2 to 8 GHz), where the maximum gain increase is 2.932 dB when compared to a conventional TEM horn.

Change in Engine Exhaust Characteristics Due to Automotive Waste Heat Recovery (엔진 배기 폐열회수로 인한 배기 특성 변화)

  • Kim, Kibum
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.15 no.8
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    • pp.4723-4728
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    • 2014
  • In this study, a thermoelectric module (TEM) and a diesel engine were modeled using 1-D commercial software AMESim, and the performance of the TEM was evaluated when the engine was operated under the NEDC driving cycle. The goal of TEM modeling was to investigate not only the waste heat recovery (WHR) rate and energy converting efficiency, but also the heat transfer rate by taking the materials characteristics into account. In addition, a diesel oxidation catalyst (DOC) was designed, and it was found that the waste heat recovery with TEM affects the activation of DOC and alters engine exhaust composition. The simulation indicated that the WHR using TEM is beneficial for decreasing the fuel consumption of vehicles, but the reduction in the exhaust temperature affects the activation of DOC, resulting in an approximately 14% increase in CO and HC emissions. Therefore, the effect of waste heat recovery on the automotive emission characteristics must be considered in the development of automotive engine WHR systems.

TEM analysis of IBAD/RABiTS substrates prepared by Tripod polishing (Tripod polishing을 이용한 IBAD/RABiTS 기판의 TEM 분석)

  • Choi, Soon-Mee;Chung, Jun-Ki;Yoo, Sang-Im;Park, Chan;Oh, Sang-Soo;Kim, Cheol-Jin
    • Progress in Superconductivity and Cryogenics
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    • v.8 no.1
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    • pp.9-14
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    • 2006
  • Sample preparation plays a critical role in microstructure analysis using TEM. Although TEM specimen has been usually prepared by jet-polishing or Ar-ion beam milling technique. these methods could not be applied to YBCO CC which is composed of IBAD or RABiTS substrates, several buffet layers, and YBCO superconducting layer because of big difference in mechanical strengths between the metallic phase and oxide phases. To obtain useful cross-sectional information such as interface between the phases or second phases in YBCO CC, it is prerequisite to secure the large area of thin section in the cross-sectional direction. The superconducting layer or the buffer layers are relatively weak and fragile compared to the metallic substrate such as Ni-5wt%W RABiTS of Hastelloy-based IBAD, and preferential removal of weak ceramic phases during polishing steps makes specimen preparation almost impossible. Tripod polisher and small jig were home-made and employed to sample preparation. The polishing angle was maintained <$1^{\circ}$ throughout the polishing steps using 2 micrometers attached to the tripod plate. TEM specimens with large and thin area could be secured and used for RABiTS/IBAD substrate analyses. In some cases, additional Ar-beam ion milling with low beam current and impinging angle was used for less than 30 sec. to remove debris or polishing media attacked to the specimens.