• Title/Summary/Keyword: sub-zero treatment

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Study on the Surface Treatment and Performance Evaluation of Mold Steel (금형강의 표면처리 및 성능평가에 관한 연구)

  • Lim, Kyu-seong;Choi, Seong-Dae
    • Journal of the Korean Society of Manufacturing Process Engineers
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    • v.21 no.1
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    • pp.81-89
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    • 2022
  • It is necessary to increase the surface hardness and improve the wear resistance and peeling resistance through the surface treatment and performance evaluation of the mold steel. As a result of vacuum heat treatment analysis, residual austenite measurement and surface treatment wear test, retained austenite should be removed by sub-zero treatment, and retained austenite was completely removed by treatment at -196℃. The TiMon film coated on the sub-zero treated STD11 specimen showed the lowest coefficient of friction.

Effect of Heat Treatment on Microstructure, Mechanical Property and Corrosion Behavior of STS 440C Martensitic Stainless Steel (STS 440C 마르텐사이트계 스테인리스 강의 열처리에 따른 미세조직, 기계적 특성 및 부식 거동)

  • Kim, Mingu;Lee, Kwangmin
    • Korean Journal of Materials Research
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    • v.31 no.1
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    • pp.29-37
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    • 2021
  • Martensitic stainless steel is commonly used in the medical implant instrument. The alloy has drawbacks in terms of strength and wear properties when applied to instruments with sharp parts. 440C STS alloy, with improved durability, is an alternative to replace 420 J2 STS. In the present study, the carbide precipitation, and mechanical and corrosion properties of STS 440C alloy are studied as a function of different heat treatments. The STS 440C alloy is first austenitized at different temperatures; this is immediately followed by oil quenching and sub-zero treatment. After sub-zero treatment, the alloy is tempered at low temperatures. The microstructures of the heat treated STS 440C alloy consist of martensite and retained austenite and carbides. Using EDX and SADP with a TEM, the precipitated carbides are identified as a Cr23C6 carbide with a size of 1 to 2 ㎛. The hardness of STS 440C alloy is improved by austenitization at 1,100 ℃ with sub-zero treatment and tempering at 200 ℃. The values of Ecorr and Icorr for STS 440C increase with austenitization temperature. Results can be explained by the dissolution of Cr-carbide and the increase in the retained austenite. Sub-zero treatment followed by tempering shows a little difference in the properties of potentiodynamic polarizations.

Effect of Heat Treatment on Mechanical Properties of STD11 and STS3 (공구강의 열처리 조건에 빠른 기계적 성질)

  • 박지환;이종권;류근걸;이윤배
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.5 no.3
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    • pp.204-209
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    • 2004
  • Using STD11 and STS3 as a mold set, accuracy of a mold product could be improved by heat treatment. Results of Charpy impact test and measurement of retained austenite in STS3 and STD11, STD11 was superior than STS3 in effect of sub-zero treatment and stability of working and measure. Decrease of retain austenite by sub-zero treatment in STS3 did not occured.

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Low-temperature Mechanical Behavior of Super Duplex Stainless Steel Considering High Temperature Environment (고온 환경의 영향을 고려한 슈퍼듀플렉스 강의 저온 기계적 거동 평가)

  • Kim, Myung-Soo;Jung, Won-Do;Kim, Jeong-Hyeon;Lee, Jae-Myung
    • Journal of Ocean Engineering and Technology
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    • v.28 no.4
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    • pp.306-313
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    • 2014
  • Super duplex stainless steels (sDSS) are excellent for use under severely corrosive conditions such as offshore and marine applications like pipelines and flanges. sDSS has better mechanical properties and corrosion resistance than the standard duplex stainless steel (DSS) but it is easier for a sigma phase to appear, which depresses the mechanical property and corrosion resistance, compared to DSS, because sDSS has a higher alloy element than DSS. In addition, sDSS has a feeble ductile-brittle transition temperature (DBTT) because it has a 50% ferrite microstructure. In the actual operating environment, sDSS would be thermally affected by welding and a sub-zero temperature environment. This study analyzed how precipitated sDSS behaves at a sub-zero temperature through annealing heat treatment and a sub-zero tensile test. Six types of specimens with annealing times of up to 60 min were tested in a sub-zero chamber. According to the experimental results, an increase in the annealing time reduced the elongation of sDSS, and a decrease in the tensile test temperature raises the flow stress and tensile stress. In particular, the elongation of specimens annealed for 15 min and 30 min was clearly lowered with a decrease in the tensile test temperature because of the increasing sigma phase fraction ratio.

Degradation of Phenol by "TiO2 Ceramic Membrane+UV+H2O2" AOP ("TiO2 촉매막+UV+H2O2" 고도산화법(AOP)을 이용한 페놀 분해)

  • Choung, Youn Kyoo;Kim, Jin Wook
    • KSCE Journal of Civil and Environmental Engineering Research
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    • v.14 no.3
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    • pp.645-654
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    • 1994
  • Photocatalytic oxidation conditions of reactant recirculation flow rate 275 mL/min, aeration rate 2 LPM and $UV+TiO_2+H_2O_2$(500 mg/L) proved to be appropriate for water including organic materials treatment. With increasing turbidity and suspended solids concentration, at turbidity 10 NTU-suspended solids concentration 29 mg/L the phenol degradation efficiency increased, which in turn decreased at turbidity 50 NTU-suspended solids concentration 170 mg/L, however no significant differences were observed, demonstrating similar results with those obtained at zero turbidity and suspended solids concentration. The degradation efficiency of phenol decreased with increasing influent phenol concentrations. The $UV+TiO_2+H_2O_2$ photocatalytic advanced oxidation process conducted is considered to be possibly applied to the drinking water treatment, and the post-treatment process of biological wastewater treatment.

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Shooting and Fruiting Characteristics of 'Hachiya' Persimmon Tree Affected by Sub-zero Temperature Treatment at Early Budding Stage (발아 초기에 영하온도 처리에 따른 감나무 '갑주백목' 의 신초 생장과 착과 특성)

  • Kim, Ho Cheol
    • The Journal of the Convergence on Culture Technology
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    • v.5 no.4
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    • pp.395-399
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    • 2019
  • The purpose of this study was to investigate shooting and fruiting characteristics of persimmon 'Hachiya' affected by sub-zero temperature at early budding stage. The number of developed shoots, and the number of shoots with young fruits, and the shooting and fruiting of terminal buds of one-year-old branch (1YOB) were significantly decreased with the sub-zero temperature treatment (SZT). The number of shoots developed in the top of 1YOB decreased 47.2% due to SZT. The number of shoots with fruits was significantly decreased at 50% or higher in non-budding rate of 1-YOB. Especially the number of fruits (Y) at the three terminal buds of 1YOB was significantly affected by SZT and the non-budding rate (X) as Y = -0.145X + 12.950 ($r^2=0.4672^*$). Therefore, in the early budding stage of persimmon, when tree is affected by SZT ($-2^{\circ}C$, 3 hours), shoots growth is reduced and increase of 10% in non-budding rate reduces 1.4 of fruits per the three terminal buds of 1YOB.

Mathematical and experimental study of hydrogen sulfide concentrations in the Kahrizak landfill, Tehran, Iran

  • Asadollahfardi, Gholamreza;Mazinani, Safora;Asadi, Mohsen;Mirmohammadi, Mohsen
    • Environmental Engineering Research
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    • v.24 no.4
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    • pp.572-581
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    • 2019
  • The emission of hydrogen sulfide (H2S) from the Kahrizak landfill was studied. Firstly, the field measurements were conducted in the summer and winter seasons; and the samples were analyzed using Jacob method. We predicted the H2S concentrations in the downwind using AERMOD and ISCST3. According to the AERMOD, the maximum concentration of H2S in the summer and winter were 117 ㎍/㎥ and 205 ㎍/㎥ respectively. The downwind concentrations reached zero at the distance of 35 km from the leachate treatment plant. The Geometric mean bias, Geometric variance, Fractional bias, Fraction of predictions within a factor of two of the observations and Normalized mean square error for the AERMOD were 0.58, 1.35, -0.12, 1.91 and 0.042, respectively in the summer and 1.39, 1.35, -0.05, 1.46 and 0.027 in the winter; and for the ISCST3, were 0.85, 1.03, 0.02, 1.45 and 0.04 in the summer and 1.18, 1.03, 0.15, 1.16 and 0.04 in the winter. The results of the AERMOD were compared with the ISCST3 and indicated that the AERMOD performance was more suitable than the ISCST3.

Effect of Carburizing Heat Treatment Process on Microstructure and Residual Stress Changes in AISI 9310 Steel. (AISI 9310강의 침탄열처리 경로가 조직 및 잔류응력 변화에 미치는 영향)

  • Youngchul Jeong;Joohyeon Bae;Jaeman Park;Seungjun OH;Janghyun Sung;Yongsig Rho
    • Journal of the Korean Society for Heat Treatment
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    • v.37 no.3
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    • pp.128-137
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    • 2024
  • In this study, the carburizing heat treatment process used in aircraft gear manufacturing was compared with the general carburizing heat treatment process using AISI 9310 steel. The process of carburizing followed by slow cooling, and then quenching after austenitizing(Process A) showed less compressive residual stress and less retained austenite in the surface layer compared to the process of quenching directly after carburizing(Process B). In prpcess B, there was a large amount of retained austenite when quenched immediately after carburization, and when treated with subzero, martensite rapidly increased and the compressive residual stress increased significantly, but at the same time, there is a risk of cracking due to severe expansion in volume. Therefore, in the case of aviation parts, it is believed that a step-by-step heat treatment cycle was adopted to ensure stability against heat treatment cracks. As a result of the final tempering after sub-zero treatment, the A process specimen showed a deeper effective case depth and HV700 depth and a higher hardness value above HV700 than the B process specimen.

Application of Electro-membrane for Regeneration of NaOH and H2SO4 from the Spent Na2SO4 Solutions in Metal Recovery Process (금속회수공정에서 발생되는 Na2SO4 폐액으로 부터 NaOH 및 H2SO4 재생을 위한 Electro-membrane 응용)

  • Cho, Yeon-Chul;Kim, Ki-Hun;Ahn, Jae-Woo
    • Resources Recycling
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    • v.31 no.5
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    • pp.3-19
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    • 2022
  • Electro-membrane technology is a process for separating and purifying substances in aqueous solution by electric energy using an ion exchange membrane with selective permeability, such as electrodialysis (ED) and bipolar electrodialysis (BMED). Electro-membrane technology is attracting attention as an environmental friendly technology because it does not generate by-products during the process and the recovered base or acid can be reused during the process. In this paper, we investigate the principles of ED and BMED technologies and various characteristics and problems according to the cell configuration. In particular, by investigating and analyzing research cases related to the treatment of waste sodium sulfate (Na2SO4), which is generated in large amounts during the metal recovery process.

RELATION BETWEEN BLACK HOLE MASS AND BULGE LUMINOSITY IN HARD X-RAY SELECTED TYPE 1 AGNS

  • Son, Suyeon;Kim, Minjin;Barth, Aaron J.;Ho, Luis C.
    • Journal of The Korean Astronomical Society
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    • v.55 no.2
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    • pp.37-57
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    • 2022
  • Using I-band images of 35 nearby (z < 0.1) type 1 active galactic nuclei (AGNs) obtained with Hubble Space Telescope, selected from the 70-month Swift-BAT X-ray source catalog, we investigate the photometric properties of the host galaxies. With a careful treatment of the point-spread function (PSF) model and imaging decomposition, we robustly measure the I-band brightness and the effective radius of bulges in our sample. Along with black hole (BH) mass estimates from single-epoch spectroscopic data, we present the relation between BH mass and I-band bulge luminosity (MBH-MI,bul relation) of our sample AGNs. We find that our sample lies offset from the MBH-MI,bul relation of inactive galaxies by 0.4 dex, i.e., at a given bulge luminosity, the BH mass of our sample is systematically smaller than that of inactive galaxies. We also demonstrate that the zero point offset in the MBH-MI,bul relation with respect to inactive galaxies is correlated with the Eddington ratio. Based on the Kormendy relation, we find that the mean surface brightness of ellipticals and classical bulges in our sample is comparable to that of normal galaxies, revealing that bulge brightness is not enhanced in our sample. As a result, we conclude that the deviation in the MBH-MI,bul relation from inactive galaxies is possibly because the scaling factor in the virial BH mass estimator depends on the Eddington ratio.