• Title/Summary/Keyword: scanning microscopy

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Development and Performance Evaluation of Positively Charged Porous Filter media for Water Purification System (정수 설비를 위한 양전하가 부가된 다공성 수처리 필터 개발과 성능평가)

  • Lee, Chang-Gun;Joo, Ho-Young;Lee, Jae-Keun;Ahn, Young-Chull;Park, Seong-En
    • Proceedings of the SAREK Conference
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    • 2006.06a
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    • pp.95-98
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    • 2006
  • Filtration by fibrous filter is one of the Principle methods used for removing pollutant particles in the liquid. Because of the increasing need to protect both human health and valuable devices from exposure to fine particles, filtration has become more important. Filters have been developed with modified surface charge characteristics to capture and adsorb particles by electrokinetic interaction between the filter surface and particles contained in water. The main purposes of this study are to develop and evaluate the performance evaluation of the apparatus for making a positively charged porous filter media and to analyze the surface characteristics of the filter media for capturing negavitely charged contaminants mainly bacteria and virus from water. The experimental apparatus consists of a mixing tank, a vacuum pumping system, a injection nozzle, a roller press and a controller. The filter media is composed of glass fiber(50-750 nm), cellulose($10-20{\mu}m$) and colloidal charge modifier. The characteristics of filter media is analyzed by SEM(Scanning Electron Microscopy), AFM(Atomic Force Microscopy) and quantified by measuring the zeta potential values.

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Differentiation of the Fetal Rat Pulmonary Epithelial Cells in Organotypic Culture (기관형 배양에서 흰쥐 태자 폐상피세포의 분화)

  • 홍혜남;조운복
    • The Korean Journal of Zoology
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    • v.35 no.3
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    • pp.295-307
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    • 1992
  • In order to study the differentiation of the epithelial cells during the development of fetal rat lung tissue, histological changeB in organotypic culture and in vivo were examined. Light microscopy and scanning electron microscopy were used to analvre the histological change in rat lung from the 15th nary of gestation to the 111th nary after birth. In organotypic culture system, the pulmonary epithelial cell differentiation was studied by scanning electron microscopy. The results obtained from this study were as follows. 1. During deveiopment of lung, the glandular stage lasted from the Isth day to the lsth naut of gestation; the canalicular stage from the 17th nay to the 19th naut of gestation; the saccuiar stage from 20th nary to the birth. Alveolar stage was observed at the 3rd nary of postnatal rat lung. 2. In organotvpic culture of fetal rat lung cells organized alveolar-like structures resembling those of in uiuo state were observed on the gelatin matrix. In contrast with in vivo state, fetal lung cells formed group of type ll pneumocytes predominently along the contours of the matrix. These cells have large apical surface, short microvilli and secreted materials which may be sunactant. These results suggested that an orsanotypic culture retaining epithelial- -mesenchvmal relationships is appropriate culture model to study the pulmonary epithelial cell (especially type ll pneumocvte) differentation.

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Analysis of dislocation density in strain-hardened alloy 690 using scanning transmission electron microscopy and its effect on the PWSCC growth behavior

  • Kim, Sung-Woo;Ahn, Tae-Young;Kim, Dong-Jin
    • Nuclear Engineering and Technology
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    • v.53 no.7
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    • pp.2304-2311
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    • 2021
  • The dislocation density in strain-hardened Alloy 690 was analyzed using scanning transmission electron microscopy (STEM) to study the relationship between the local plastic strain and susceptibility to primary water stress corrosion cracking (PWSCC) in nuclear power plants. The test material was cold-rolled at various thickness reduction ratios from 10% to 40% to simulate the strain-hardening condition of plant components. The dislocation densities were measured at grain boundaries (GB) and in grain interiors of strain-hardened specimens from STEM images. The dislocation density in the grain interior monotonically increased as the strain-hardening proceeded, while the dislocation density at the GB increased with strain-hardening up to 20% but slightly decreases upon further deformation to 40%. The decreased dislocation density at the GB was attributed to the formation of deformation twins. After the PWSCC growth test of strain-hardened Alloy 690, the fraction of intergranular (IG) fracture was obtained from fractography. In contrast to the change in the dislocation density with strain-hardening, the fraction of IG fracture increased remarkably when strain-hardened over 20%. From the results, it was suggested that the PWSCC growth behavior of strain-hardened Alloy 690 not only depends on the dislocation density, but also on the microstructural defects at the GB.

Synthesis of ZnO/Zn(OH)2 Nanosheets Using Ionic Layer Epitaxy (이온층 에피택시법을 이용한 ZnO/Zn(OH)2 나노시트의 합성)

  • Jeong, Gyu Hyun;Nam, Dong Hyun;Ryu, Gyeong Hee
    • Korean Journal of Materials Research
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    • v.32 no.3
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    • pp.153-160
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    • 2022
  • ZnO nanosheets have been used for many devices and antibacterial materials with wide bandgap and high crystallinity. Among the many methods for synthesizing ZnO nanostructures, we report the synthesis of ZnO/Zn(OH)2 nanosheets using the ionic layer epitaxy method, which is a newly-developed bottom-up technique that allows the shape and thickness of ZnO/Zn(OH)2 nanosheets to be controlled by temperature and time of synthesis. Results were analyzed by scanning electron microscopy and atomic force microscopy. The physical and chemical information and structural characteristics of ZnO/Zn(OH)2 nanosheets were compared by X-ray photoelectron spectroscopy and X-ray diffraction patterns after various post-treatment processes. The crystallinity of the ZnO/Zn(OH)2 nanosheets was confirmed using scanning transmission electron microscopy. This study presents details of the control of the size and thickness of synthesized ZnO/Zn(OH)2 nanosheets with atomic layers.

Manufacturing of SPL system having a large scanning area (대면적 SPL(Scanning Probe Lithography) 시스템 제작)

  • Yoon, Sang-Joon;Kim, Won-Hyo;Seong, Woo-Kyeong;Park, Young-Geun;Hwang, Kyu-Ho;Chung, Kwan-Soo
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2004.11a
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    • pp.699-702
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    • 2004
  • Next generation lithography technologies, such as EBL(Electron Beam Lithography), X-ray lithography, SPL(Scanning Probe Lithography), have been studied widely for getting over line width limitation of photolithography. Among the next generation lithography technologies, SPL has been highlighted because of its high resolution advantage. But is also has problem which are slow processing time and sample size limitation. The purpose of this study is complement of present SPL system. Brand new SPL system was made. SPL test was performed with the system in ultra thin PMMA(polymethlymethacrylate) film.

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Scanning System Stability for Improving SEM Image (전자현미경의 이미지 향상을 위한 주사시스템의 안정성)

  • Kim, Seung-Jae;Kim, Dong-Hwan
    • Journal of the Korean Society of Manufacturing Technology Engineers
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    • v.18 no.5
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    • pp.455-461
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    • 2009
  • In a scanning electron microscopy, image distortion is a critical issue and it is needed to be eliminated by some kinds of schemes. In this work, scanning frequency and scanning wave form are adjusted to have an improved image. The relationship between scan coil and its driver is investigated and appropriate frequency and wave form are suggested. It is proved that the selected frequency and wave form showed an enhanced image with less distortion, which were done by experiments. In addition, a noise elimination is addressed, providing improved image with a GROUND signal integration with the amplifier and the scan driver.

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Morphology Observation and Electrical Properties measuring of Self-Assembled Organic Monolayers on Au(111) Substrate Using Scanning Tunneling Microscopy (STM을 이용한 Au(111)기판에 자기조립화된 유기초박막의 모폴로지관찰 및 전기적특성 측정)

  • Lee, Nam-Suk;Shin, Hoon-Kyu;Chang, Jeong-Soo;Kwon, Young-Soo
    • Proceedings of the KIEE Conference
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    • 2004.07c
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    • pp.1715-1717
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    • 2004
  • We attempt to investigate morphology of self-assembled dipyridinium dithioacetate on Au(111) substrate by Scanning Tunneling Microscopy(STM). Also, we measured electrical properties using Scanning Tunneling Spectroscopy(STS). Sample that use this experiment acquires thiol function beside quantity by dipyridinium dithioacetate, is structure that can be self-assembled easily to Au(111) substrate. The same self-assembly procedure was used for two different concentrations, 0.5mmol/ml and 1mmol/ml. Dilute density of sample by 0.5mmol/ml, 1mmol/ml and observed dipyridinium dithioacetate's image by STM after self-assembled on Au(111) substrate. The structure of Tip/SAMs/Au(111) has been used measurement for electrical properties(i-v) using STM. The current-voltage measurement result, observed negative differential resistance(NDR) properties.

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Microscopic Feature, Protein Marker Expression, and Osteoinductivity of Human Demineralized Dentin Matrix

  • Park, Sung-Min;Hwang, Jung-Kook;Kim, Young-Kyun;Um, In-Woong;Lee, Geun-Ho;Kim, Kyung-Wook
    • Journal of Korean Dental Science
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    • v.5 no.2
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    • pp.77-87
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    • 2012
  • Purpose: This study examined the scanning electron microscopic feature, protein marker expression and osteoinductive activity of demineralized dentin matrix (DDM) from human for nude mice. Materials and Methods: Twenty healthy nude mice, weighing about 20 g were used for study. DDM from Human was prepared and implanted into the dorsal portion of nude mouse. Before implantation, DDM was examined by scanning electron microscopy (SEM). Nude mice were sacrificed at 2 weeks, 4 weeks and 8 weeks after DDM grafting and evaluated histologically by H-E, MT staining. And also immunohistochemistry analysis (ostecalcin, osteopontin) was performed. Result: Dentinal tubules and collagen fibers were observed by SEM of dentin surface of DDM. The DDM induced bone and cartilage independently in soft tissues. And, the histological findings showed bone forming cells like osteoblasts, fibroblasts at 2, 4 and 8 weeks. On immunohistochemistry analysis, osteocalcin and osteopontin positive bone forming cells were observed. Conclusion: This results showed that the DDM from human has osteoinductive ability and is a good alternative to autogenous bone graft materials.

Current Trend of Ultrahigh Vacuum Low Temperature Scanning Tunneling Microscopy (초고진공 저온 주사터널 현미경 장치의 최신 경향)

  • Ham, Ungdon;Yeom, Han Woong
    • Vacuum Magazine
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    • v.3 no.4
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    • pp.14-18
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    • 2016
  • In this article, we will summarize recent advances in ultrahigh vacuum (UHV) low-temperature scanning tunneling microscopy (STM) during the last decade. Leading STM groups have finished or are constructing UHV milli-Kelvin high magnetic field STM capable of a few tens of milli-Kelvin and ~ 10 tesla. Applications with UHV sub-Kelvin high magnetic STM have been increased since mid-2000's. Active research using UHV low temperature tuning fork atomic force microscopes and UHV photon low-temperature scanning tunneling microscopes will be introduced. Considering these advances of UHV low-temperature STM we will discuss next trend in STM in the near future.

Current-Voltage Properties measuring of Dipyridinium Molecule Using Scanning Tunneling Microscopy (STM에 의한 Dipyridinium 분자의 전압-전류 특성 측정)

  • Lee, Nam-Suk;Shin, Hoon-Kyu;Chang, Jeong-Soo;Kwon, Young-Soo
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2004.11a
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    • pp.485-488
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    • 2004
  • 본 연구에서는 dipyridinium dithioacetate 분자를 Au(111) 표면에 자기조립하여 STM 탐침-유기 단분자막-Au(111)기판의 수직구조로 STM 측정시스템을 이용하여, 전기적 특성을 관찰하였다. 먼저 Au(111)기판을 Piranha용액$(H_2SO_4:H_2O_2=3:1)$으로 Au 표면을 전처리 하였다. 전처리한 Au(111) 기판을 dipyridinium dithioacetate 1mol/ml 농도로 자기조립 하였으며, 자기조립막의 표면 구조를 STM으로 관찰하였다. dipyridinium dithioacetate의 전기적 특성은 STM 탐침-유기단분자막-Au(111) 기판의 수직구조로 STS를 이용하여 조사하였다. 전압과 전류 측정에서 전압이 증가함에 따라 전류가 감소하는 부성 미분저항(NDR)의 특성이 관찰 되었다. NDR 수치가 $-545\;[m\Omega/cm^2]$였고, PVCR은 1.64:1 이었다.

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