• Title/Summary/Keyword: resin composites

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Optimum Mixing Ratio of Epoxy for Glass Fiber Reinforced Composites with High Thermal Stability (에폭시 배합비에 따른 내열성 복합재료 최적조건)

  • Shin, Pyeong-Su;Wang, Zuo-Jia;Kwon, Dong-Jun;Choi, Jin-Yeong;Sung, Ill;Jin, Dal-Saem;Kang, Suk-Won;Kim, Jeong-Cheol;Park, Joung-Man
    • Composites Research
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    • v.27 no.4
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    • pp.168-173
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    • 2014
  • The optimum condition of glass fiber/epoxy composites was investigated according to mixing ratio of two epoxy matrices. Novolac type epoxy and isocyanate modified epoxy were used as composites matrix. Based on chemical composition of mixing matrix, optimum mixing ratio of epoxy resins was obtained through various experiments. In order to investigate thermal stability and interface of epoxy resin, glass transition temperature was observed by DSC instrument, and static contact angle was measured by reflecting microscope. Change of IR peak and $T_g$ was conformed according to different epoxy mixing ratio. After fabrication of glass fiber/epoxy composites, tensile, compression, and flexural properties were tested by UTM by room and high temperature. The composites exhibited best mechanical properties when epoxy mixing ratio was 1:1.

Developement of New Glass Fiber Reinforced Composite Insulating Material by Reactive Plasma Surface Treatment(II) (반응성 플라즈마 표면처리기법을 도입한 새로운 유리섬유 강화 복합재료의 개발 및 물성연구(II))

  • 박정후;조정수;성문열;김두환;김규섭
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 1995.05a
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    • pp.216-219
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    • 1995
  • One of the principal problems encountered in the use of glass fiber reinforced Plastic composites(GFRP) is to establish an active fiber surface to achieve maximum adhesion between resin and fiber surface. In order to develope new process to overcome the disadvantage of chemical agent, we have studied the effect of reactive plasma glass surface treatment on the electrical and mechanical properties of glass fiber reinforced epoxy composites. It is found that the electrical and mechanical characteristics of the composites treated with plasma is improved especially in the dielectric strength by 20% and tensile strength by 15%, whereas the tan $\delta$ is decreased significantly.

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Elastic Model of Twisted Yarn Composites (Twisted Yarn 복합재료의 탄성계수 예측모델)

  • 변준형;이상관;엄문광
    • Proceedings of the Korean Society For Composite Materials Conference
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    • 2002.05a
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    • pp.57-60
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    • 2002
  • The stiffness model has been proposed to predict elastic constants of twisted yarn composites. The model is based upon the unit cell structure, the coordinate transformation, and the volume averaging of compliance constants for constituent materials. For the correlation of analytic results with experiments, composite samples of various yarn twist angle were tested. The samples were fabricated by the RTM process using glass yarns and epoxy resin. The correlations of elastic constants showed relatively good agreements. The model provides the predictions of the three-dimensional engineering constants, which are valuable input data for the analytic characterization of textile composites made of twisted yarn.

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Electromagnetic Interference Reflectivity of Nanostructured Manganese Ferrite Reinforced Polypyrrole Composites

  • Chakraborty, Himel;Chabri, Sumit;Bhowmik, Nandagopal
    • Transactions on Electrical and Electronic Materials
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    • v.14 no.6
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    • pp.295-298
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    • 2013
  • Nano-size manganese ferrite reinforced conductive polypyrrole composites reveal a core-shell structure by in situ polymerization, in the presence of dodecyl benzene sulfonic acid as the surfactant and dopant, and iron chloride as the oxidant. The structure and magnetic properties of manganese ferrite nano-fillers were measured, by using X-ray diffraction and vibrating sample magnetometer. The morphology, microstructure, and conductivity of the composite were characterized by transmission electron microscopy, Fourier transform infrared spectroscopy, and four-wire technique. The microwave-absorbing properties of composites reinforcement dispersed in resin coating with the coating thickness of 1.2 nm were investigated, by using vector network analyzers, in the frequency range of 8~12 GHz. A reflection loss of -8 dB was observed at 10.5 GHz.

Tribological Characteristics of Carbon Fiber Reinforced Plastics Prepared by Ion-Assisted Reaction (이온도움반응법에 의한 탄소섬유복합재의 트라이볼로지 특성연구)

  • 오성모;김정기;이봉구
    • Journal of the Korean Society for Precision Engineering
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    • v.21 no.4
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    • pp.103-108
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    • 2004
  • Carbon fiber reinforced composites(CFRP) were fabricated with phenolic resin matrix by hot press molding, and its surface was modified by the ion-assisted reaction process. When we tested the friction coefficient and wear rate variation and observed the effect of fibers with respect to friction and wear characteristics, the amount of pitch based carbon fiber was 45wt% and the average friction coefficient was the lowest at 0.12. When the amount of ion-irradiation was $1\times10^{l6}ions/cm^2$, the friction coefficient of the composites was about 0.12 and the wear mode was stable, whereas, the friction coefficient of the non-treated composites was about 0.16 and the wear mode was very unstable. But if the amount of ion-irradiation was $5\times10^{l6}ions/cm^2$$1\times10^{l6}ions/cm^2$ion-irradiation case.

Conductivity stability of carbon nanofiber/unsaturated polyester nanocomposites

  • Wu, Shi-Hong;Natsuki, Toshiaki;Kurashiki, Ken;Ni, Qing-Qing;Iwamoto, Masaharu;Fujii, Yoshimichi
    • Advanced Composite Materials
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    • v.16 no.3
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    • pp.195-206
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    • 2007
  • Carbon nanofiber (CNF)/unsaturated polyester resin (UPR) was prepared by a solvent evaporation method, and the temperature dependency of electrical conductivity was investigated. The CNF/UPR composites had quite a low percolation threshold due to CNF having a larger aspect ratio and being well dispersed in the UPR matrix. The positive temperature coefficient (PTC) was found in the CNF/UPR composites and it showed stronger effect around the percolation threshold. The electrical resistance of the CNF/UPR composites decreased and had lower temperature dependency with increasing numbers of thermal cycles.

Preparation of Si-SiC Composites by Si-Infiltration (Si 침윤에 의한 Si-SiC 복합체 제조)

  • 김인술;장주민;오기동;박홍채
    • Journal of the Korean Ceramic Society
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    • v.29 no.9
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    • pp.750-756
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    • 1992
  • Reaction bonded si-SiC composites were prepared by silicon infiltration technique at temperature of 1$600^{\circ}C$ for 30 minutes in vaccum atmosphere. The microstructure and mechanical properties of Si-SiC composites were investigated and characterized. UF-15 and SE-10 as SiC powders, phenolic resin and carbon black as carbon source, and metallic silicon powder as molten Si source were used as starting materials. New SiC crystallines nucleatd and grown by reaction of Si and C were detected by TEM and SEM-EDS. The bonding between new and original SiC was found to be strong. But the wetting of SiC by unreacted metallic Si and the rapid grain growth of new SiC decreased density and fracture toughness. Fracture toughness and modulus of rupture of Si-SiC composite were about 3.2 MPa.m1/2 and 480 MPa, respectively.

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Experimental analysis of pultrusion process for phenolic foam composites (발포 복합재료 Pultrusion 공정의 실험적 해석)

  • Yun MyungSeok;Lee WooIl
    • Proceedings of the Korean Society For Composite Materials Conference
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    • 2004.10a
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    • pp.143-146
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    • 2004
  • Pultrusion process of phenolic foam composite is investigated. Phenolic foam composites provide heat and flame resistance with less weight. When made into foam, a variety of properties can be obtained with different bubble size and number density. In this study, effect of process variables on the foaming characteristics of phenolic resin composites during pultrusion process has been studied experimentally. The process variables considered are the heating temperature and the pulling speed as well as the mass fraction of blowing agent. Experiments were performed using a laboratory scale pultrusion apparatus. Optimal process condition was found by observing the micro-morphology.

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Durability of Fiber Reinforced Composites under Salt Water Environments (염수환경을 고려한 섬유강화 복합재의 내구성 평가)

  • Yoon Sung-Ho;Hwang Young-Eun
    • Proceedings of the KSR Conference
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    • 2005.05a
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    • pp.391-396
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    • 2005
  • Salt water spray test and salt water immersion test were experimentally conducted in order to investigate the durability of fiber reinforced composites under salt water environment. The specimens were made of glass fabric reinforcement and phenolic resin. Mechanical test was performed to obtain mechanical properties such as tensile properties, flexural properties, and shear properties by varying with exposure times. Also dynamic mechanical test and FTIR were conducted to investigate a change in chemical structure as well as thermal analysis properties such as storage shear modulus, loss shear moduls, and tan ${\delta}$. According to the results, salt water environment has effected on mechanical properties and thermal analysis properties and especially the durability of glass fabric/phenolic composites were severely affected on salt water immersion environment rather than salt water spray environment.

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Electrical Properties and Lifetime Prediction of Epoxy/$SiO_2$Composites with Water Absorption Ageing (흡수열화에 따른 Epoxy/$SiO_2$ 복합체의 전기적 특성 및 수명예측)

  • 김탁용;이덕진;홍진웅
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.13 no.9
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    • pp.758-763
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    • 2000
  • Dielectric strength of insulators made of epoxy composites rapidly decreases due to ageing to interfaces between the matric resin and filler particles. The adhesion variation of interfaces caused by moisture absorption also alters electrical properties that are the basic characteristics of insulators, particularly, in outdoor use. In this paper, electrical properties of epox/SiO$_2$composites were investigated at boiling absorption condition to observe the influences of moisture. In order to analyze the basic physical properties of samples, scanning electron microscopy and DC, AC and impulse voltage dielectric strength were measured. Also, the breakdown time of samples was measured under AC 6[kV] applied voltage, and the variation of lifetime was verified by using Weibull distribution function.

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