• Korea-Australia Rheology Journal
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• v.19 no.4
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• pp.191-199
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• 2007

Precision injection molding process is of great importance since precision optical products such as CD, DVD and various lens are manufactured by those process. In such products, birefringence affects the optical performance while residual stress that determines the geometric precision level. Therefore, it is needed to study residual stress and birefringence that affect deformation and optical quality, respectively in precision optical product. In the present study, we tried to predict residual stress, final shrinkage and birefringence in injection molded parts in a systematic way, and compared numerical results with the corresponding experimental data. Residual stress and birefringence can be divided into two parts, namely flow induced and thermally induced portions. Flow induced birefringence is dominant during the flow, whereas thermally induced stress is much higher than flow induced one when amorphous polymer undergoes rapid cooling across the glass transition region. A numerical system that is able to predict birefringence, residual stress and final shrinkage in injection molding process has been developed using hybrid finite element-difference method for a general three dimensional thin part geometry. The present modeling attempts to integrate the analysis of the entire process consistently by assuming polymeric materials as nonlinear viscoelastic fluids above a no-flow temperature and as linear viscoelastic solids below the no-flow temperature, while calculating residual stress, shrinkage and birefringence accordingly. Thus, for flow induced ones, the Leonov model and stress-optical law are adopted, while the linear viscoelastic model, photoviscoelastic model and free volume theory taking into account the density relaxation phenomena are employed to predict thermally induced ones. Special cares are taken of the modeling of the lateral boundary condition which can consider product geometry, histories of pressure and residual stress. Deformations at and after ejection have been considered using thin shell viscoelastic finite element method. There were good correspondences between numerical results and experimental data if final shrinkage, residual stress and birefringence were compared.

• Journal of the Korean Data and Information Science Society
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• v.10 no.1
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• pp.47-56
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• 1999

In this paper, for whole line ($0,\;{\infty}$), the estimation procedure of mean residual life function using product-limit estimator is studied with asymptotic properties. And also, the small sample properties of proposed estimator of MRLF are investigated through Monte Carlo study and compared with Kaplan-Meier type estimator.

• Polymer(Korea)
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• v.36 no.2
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• pp.131-136
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• 2012

Residual stress is developed in the injection molded articles during the molding process due to temperature variation and shear stress. The residual stress causes the deformation and warpage in the injection molded parts shortly within several days or after several years. Therefore, the injection molding conditions should be optimized to reduce the residual stress. And residual stress in the part should be also relaxed after molding process to maintain its shape. According to the annealing conditions, such as relative humidity, temperature and time, this study investigates the relaxation of residual stress generated in the transparent injection molded specimens. Through the experimental results, it was realized that the residual stress was relaxed at a relative humidity higher than 50%. Utilizing photoelasticity equipment, it was found that the residual stress was rapidly relaxed near glass transition temperature. Additionally, we recognized that the specimen shrunk along the flow direction but expanded to the perpendicular direction of the flow during the annealing processes, which resulted in the warpage of the specimen.

• Transactions of Materials Processing
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• v.28 no.4
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• pp.212-218
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• 2019

In this study, the first drawing die for the production of coil wedge is redesigned in order to enhance properties such as dimensional accuracy, dimensional uniformity, non-magnetism, and residual stress. The equivalent strain distribution is observed to be asymmetric at certain corners of the product and un-filling of material is also observed at the same location, based on the results of FEM simulation for the current drawing process. Additionally, a relatively huge amount of deformation is concentrated on the surface of the reference product leading to an increase in magnetic component and surface residual stress. After re-designing the cross-section of the first drawing step process conformed to relatively higher amount of reduction ratio, reduction of both surface residual stress and the volume fraction of magnetic component could be achieved for the finally-drawn coil wedge product.

• Polymer(Korea)
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• v.35 no.1
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• pp.1-6
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• 2011

Pressurized high temperature plastic resin flows into the cavity of mold and is solidified in injection molding process. Residual stress is being developed in injection molded part because of high temperature variations and high pressure. Developed residual stress relaxes as time goes. Consequently this makes part deformed and deteriorates quality of product. A measurement method of residual stress for injection molded transparent articles has been investigated using photoelasticity. Light, a composite of electromagnetic waves, is purified into a single wave by a polarized film. When this wave passes through the specimen, birefringence is developed according to the level of residual stress in the specimen and color fringed pattern appears after the second polarized film. Residual stress in the injection molded transparent flat a part has been measured quantitatively using the color fringed pattern. Optical characteristics have been a part also predicted by computer simulation and compared with experimental results.

• Nuclear Engineering and Technology
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• v.50 no.7
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• pp.1184-1189
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• 2018

Pyroprocessing uses various molten salts during electrochemical unit processes. Reaction products after the electrochemical processes must contain a significant amount of residual salts to be separated. Vacuum distillation is a common method to separate the residual salts; however, its high operation temperature may cause side reactions. In this study, a simple rotation technique using centrifugal force was suggested to separate the residual salts from the reaction products at relatively low temperature compared to the distillation technique. When a reaction product container with porous wall rotates inside a vessel heated above the melting point of the residual salt, the residual salt in the liquid phase is separated through centrifugal force. It was shown that the $LiNO_3-Al_2O_3$ mixture can be separated by this technique to leave solid $Al_2O_3$ inside the container, with a separation efficiency of 99.4%.

• Environmental Analysis Health and Toxicology
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• v.19 no.3
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• pp.315-320
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• 2004

Environmental waste treatment technology is transforming from incineration system to pyrolysis gasification system. And there it is necessary for our country to adapt gasification system urgently to prevent the land pollution and lack of landfill area. The objective of this study was to determine the pesticides residues of derived product of pyrolysis gasification system for recycling of waste plastic by gas chromatograph-mass selective detector and nitrogen phosphorus detector. The residual pesticides were not detected in derived product of waste recyling. But some pesticide was detected on raw level (0.02 ～ 0.05 ppm) in waste plastic sample.

• KOREAN JOURNAL OF PACKAGING SCIENCE & TECHNOLOGY
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• v.10 no.1
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• pp.63-68
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• 2004

The regulations for migration amounts in USA, EU and Korea are investigated to compare the actual overall and specific migration date from plastic food packaging materials. Among the packaging materials regulated in above countries, printing ink solvents on packaging materials is used very widely and sometimes cause off-flavor in the food by migration of residual solvents. Even though migration of the residual solvents dose not generally cause safety problems in the contained food, it certainly can generate off-flavor and finally deteriorate quality of the finished product. Therefore regulation and development of analytical method for amount of residual ink solvents are very important issue in food industry. The headspace analytical method and tenax method for residual ink solvent on food packaging materials were evaluated from the accuracy, precise, swiftness and convenience of viewpoint. Headspace analytical method was selected and recommended for using in food industry field.

• Proceedings of the IEEK Conference
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• 2001.10a
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• pp.555-559
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• 2001

A by-product, waste sludge water produced from ready mixed concrete(remicon) factories may affect our environmental contamination if it is discharged without proper waste disposal. In Korea, all waste sludge water has been recycled in the way of mixing water of remicon, but the quality of the concrete then produced can be deteriorated, so it might cause slump loss or irregular compressive strength. In this study, waste sludge water is divided into two parts, remicon sludge and residual water in order to make it's property more stable. Then, the remicon sludge and high-alkaline residual water were used as admixture and alkali activator respectively. In this paper we research about quality of with remicon sludge and residual water and performed the fundamental properties of cement matrix mixed with remicon sludge and residual water.

• Transactions of Materials Processing
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• v.12 no.4
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• pp.302-307
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• 2003

Hot rolled strip is cooled by air and water in Run-Out-Table. In this process, phase transformation and shape deformation occurs due to temperature drop. Because of un-ideal cooling condition of ROT, irregular shape deformation and phase transformation arise in the strip. which affect the strip property and lead to the residual stress of strip. And these exert effects on the following processes, coiling process, coil cooling process, and re-coiling process. Through these processes, the residual stress becomes higher and severe. For the prediction of residual stress distribution and shape deformation of final product, Finite element(FE) based model was used. It consists of non-steady state heat transfer analysis, elasto-plastic analysis. thermodynamic analysis and phase transformation kinetics. Successive FEM simulation were applied from ROT process to coil cooling process. In each process simulation, previous process simulation results were used for the next process simulation. The simulation results were matched well with the experimental results.