• 한국세라믹학회지
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• 제29권7호
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• pp.525-532
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• 1992

TiO2 fine powder was synthesized in the gas phase by chemical vapor deposition using hydrolysis of TiCl4. Content of rutile phase in the powder was investigated. Powder characteristics such as size, crystallinity and morphology were also studied by means of TEM, SEM and XRD. Rutile phase in TiO2 powder started to be formed from 100$0^{\circ}C$ and the content increased with the reaction temperature and TiCl4 concentration. As the temperature increased from 80$0^{\circ}C$ to 140$0^{\circ}C$, the primary particle size increased while secondary particle size decreased. Spherical secondary particle with fine primary crystals agglomerated was produced at low temperature of 80$0^{\circ}C$ whereas the grown primary particle being final particle size was produced at higher temperature of 140$0^{\circ}C$. Other effects of TiCl4 and H2O partial pressures on particle size were also reported in this study.

• Nuclear Engineering and Technology
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• 제29권5호
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• pp.361-367
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• 1997

The phase separation in ferrite phase of duplex stainless steel is the primary cause of thermal aging embrittlement of the LWR primary pressure boundary components. In this study the phase separation of simulated duplex stainless steel was detected by Mossbauer spectroscopy and magnetic property analysis by VSM(Vibrating Specimen Magnetometer). The simulated duplex stainless steels, Fe-Cr binary, Fe-Cr-Ni ternary, and Fe-Cr-Ni-Si quarternary allots, were aged at 370 and 40$0^{\circ}C$ up to 5,340 hours. It was observed from Mossbauer spectra analysis that internal magnetic field increases with aging time and from VSM that the specific saturation magnetization and Curie temperature increase with aging time. These result are indicative that phase separation into Fe-rich region and Cr-rich region is caused by thermal aging in the temperature range of 370~40$0^{\circ}C$ In cases of specimens containing Ni, the increase of specific saturation magnetization is much higher. This implies that Ni seems to promote Fe-Cr interdiffusion, which accelerates the phase separation into Fe-rich $\alpha$ phase and Cr-rich $\alpha$' phase.

• 수산해양교육연구
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• 제23권3호
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• pp.533-548
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• 2011

This study examined the concern levels of primary school teachers regarding transitional education from early childhood phase to primary education. Concern Based Adoption Model (CBAM) instrument of Hall and Hord (2006) was used to survey 104 primary school teachers. The results indicated that the majority of respondents' concern level was at 'informational' level (stage 1). And first peak of concern level was at 'unconcerned' level (stage 0). The first-second peak analysis of stage 0 (unconcerned) group indicated that there were 5 types of groups and each had distinguished features. Finally there were statistical differences at the unconcerned stage by in-service training and career of the first-year class. A discussion of the limitations of this study and implications for teacher education programs and operational support systems were suggested.

• 조명전기설비학회논문지
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• 제27권2호
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• pp.84-94
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• 2013

In case when the existing TRIAC phase controlled dimmer is drove for the LED lighting equipments, there are many problems such as the LED flicker in low phase-angles, the acoustic noise and elements damage by increase of the peak voltage in the input filter capacitor, mulfunction by insufficiency of the TRIAC holding current, and the abnormal oscillation by LC resonant. In this paper, we proposes the single-stage quasi-resonant PSR(Primary Side Regulation) PWM converter, and the design, the simulation and experiment are performed. As a result, it could confirm that the proposed PWM converter is the lighting equipments for LED drive which can alternate the existing 60W class incandescent bulbs and it has the high drive performance of the efficiency 80% and over, the power factor 0.95 and over under the normal voltage 220V. Finally, total harmonic distortion(THD) is gratified with a standard[1] of the lighting equipments and the durability is evaluated as the high reliablilty of 150,000 hours and over.

• 디지털산업정보학회논문지
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• 제9권4호
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• pp.51-57
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• 2013

Research on calibration of array antenna has become a hot spot in the area of signal processing and it is necessary to obtain the phase mismatch of each antenna channel. This paper presents a new calibration method for an array antenna system. In order to calibrate the phase mismatch of each antenna channel, we used primary synchronization signal (PSS) which exists in LTE downlink frame. Primary synchronization signal (PSS) is based on a Zadoff-Chu sequence which has a good correlation characteristic. By using correlation calculation, we can extract primary synchronization signal (PSS). After extracting primary synchronization signal (PSS), we use it to calibrate and reduce the phase errors of each antenna channel. In order to verify the new array antenna calibration algorithm which is proposed in this paper, we have simulated the proposed algorithm by using MATLAB. The array antenna system consists of two antenna elements. The phase mismatch of first antenna and second antenna is calculated accurately by proposed algorithm in the experiment test. Theory analysis and MATLAB simulation results are shown to verify the calibration algorithm.

• 대한한방부인과학회지
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• 제35권3호
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• pp.122-136
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• 2022

Objectives: The aim of this study is to investigate Heart Rate Variability (HRV) characteristics of patients with primary dysmenorrhea at the menstrual phase. Methods: 7 databases (Pubmed, Cochrane library, CNKI, RISS, KISS, OASIS, ScienceON) were searched for eligible studies published before 2021 December. The studies comparing HRV between patients with primary dysmenorrhea and controls were included. A random-effects model was used to evaluate differences of HRV parameters between patients with primary dysmenorrhea and controls. Results: 4 articles were included in this review based on inclusion and exclusion criteria. SDNN (Standard deviation of NN intervals), RMSSD (Square root of the mean squared difference of successive NN intervals), mean PR (Mean of pulse rate), LF (Low frequency), HF (High frequency), was the most frequently used as HRV parameters. RMSSD was significantly lower in patients with primary dysmenorrhea than controls. There was no statistically significant difference of other HRV parameters between patients with primary dysmenorrhea and controls. Conclusions: This study suggests that parasympathetic activity and overall functions of autonomic nervous system might be decreased in patients with primary dysmenorrhea at the menstrual phase. In the future, well-designed clinical studies using HRV and additional meta-analysis should be conducted to obtain a wealth of information about HRV characteristics of patients with primary dysmenorrhea.

• Membrane and Water Treatment
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• 제13권4호
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• pp.201-208
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• 2022

Emulsion Liquid Membrane (ELM) is a prominent technique for the separation of heavy metal ions from wastewater due to the fast extraction and is a single-stage operation of stripping-extraction. The selection of the components (Surfactant and Carrier) of ELM is a very significant step for its preparation. In the ELM technique, the primary water- in-oil (W/O) emulsion is emulsified in water to produce water-in-oil-in-water (W/O/W) emulsion. The water in oil emulsion was prepared by mixing the membrane phase and internal phase. To prepare the membrane phase, the extractant D2EHPA (di-2-ethylhexylphosphoric acid) was used as a mobile carrier, Span-80 as a surfactant, and Paraffin as a diluent. Moreover, the internal (receiving) phase was prepared by dissolving sulphuric acid in water. Di-(2- ethylhexyl) phosphoric acid such as surfactant concentration, carrier concentration, sulphuric acid concentration in the receiving (internal) phase, agitation time (emulsion phase and feed phase), the volume ratio of the membrane phase to the receiving phase, the volume ratio of the external feed phase to the primary water-in-oil emulsion and pH of feed were studied on the percentage extraction of metal ions at 20℃. The results show that it is possible to remove 78% for As(V), 98% for Cd(II), and 99% for Pb(II). Emulsion Liquid Membrane (ELM) is a well-known technique for separating heavy metal ions from wastewater due to the fast extraction and is a single-stage operation of stripping-extraction. The selection of ELM components (Surfactant and Carrier) is a very significant step in its preparation. In the ELM technique, the primary water-in-oil (W/O) emulsion is emulsified to produce water-in-oil-in-water (W/O/W) emulsion. The water in the oil emulsion was prepared by mixing the membrane and internal phases. The extractant D2EHPA (di-2-ethylhexylphosphoric acid) was used as a mobile carrier, Span-80 as a surfactant, and Paraffin as a diluent. Moreover, the internal (receiving) phase was prepared by dissolving sulphuric acid in water. Di-(2-ethylhexyl) phosphoric acid such as surfactant concentration, carrier concentration, sulphuric acid concentration in the receiving (internal) phase, agitation time (emulsion phase and feed phase), the volume ratio of the membrane phase to the receiving phase, the volume ratio of the external feed phase to the primary water-in-oil emulsion and pH of feed were studied on the percentage extraction of metal ions at 20℃. The results show that it is possible to remove 78% for As(V), 98% for Cd(II), and 99% for Pb(II).

• Journal of Welding and Joining
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• 제16권3호
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• pp.111-120
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• 1998

To predict and evaluate metallurgical and mechanical behavior of th welds, it is essential to understand solidification behavior and microstructural evolution experienced in the welds, neither of which follows the equilibrium phase diagram because of rapid heating and cooling conditions. Metallurgical phenomena in austenitic stainless steel fusion welds, types 304, 309S, 316L, 321 and 304N, were investigated in this study. Autogenous GTA welding was performed on weld coupons, and primary solidification mode and phase distribution were investigated from the welds. Varestraint test was employed to evaluate solidification cracking susceptibilities of the alloys. GTA weld fusion zones in type 304, 321 and 304N stainless steels experienced primary ferrite solidification while those in type 309S primary austenite solidification. Type 316L exhibited a mixed type of primary ferrite and primary austenite solidification. The primary solidification mode strongly depended on $Cr_{eq}/Ni_{eq}$ ratio. In terms of solidification cracking susceptibility, type 309S that solidified as primary austenite exhibited high cracking susceptibility while the alloys experienced primary ferrite solidification showed low cracking susceptibility. The relative ranking in solidification cracking susceptibility was type 304=type 304N < type 321 < type 316L < type 309S.

• 한국소성가공학회:학술대회논문집
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• 한국소성가공학회 2004년도 추계학술대회논문집
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• pp.111-114
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• 2004

It is many devices to obtain the globular structure because the globularity of the structure is the key to the low apparent viscosity and also to good rheological properties. In this study, the morphology of the change of primary Al phase in A356 alloy by electro magnetic stirrer was investigated to obtain the globular structure. The parameters are the current, stirring time, pouring temperature individually. The greater current and longer stirring time was to get the finer the primary however in case of over the 80A of current and 60sec of stirring time, the primary Al was merged together and was increased. The effect of pouring temperature has an important effect on the size of primary phase. About the $675^{\circ}C$, the primary Al was very fined.

• 대한기계학회논문집
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• 제9권6호
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• pp.714-724
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• 1985

본 논문에서는 입자가 부상된 2상유동의 해석에서 여러유동조건의 유동을 공 통적으로 해석할 수 있고 또 유동의 난류구조를 규명할 수 있도록 하기 위해서 2-방정 식 난류모델을 적용하였고 또 지배방정식들 속에 나타나는 1유체와 2유체의 2차 상관 관계들을 모형화 할 때 Taweel and Landau의 스펙트럼 이론을 확장발전시켜 적용하였 다.