• 제목/요약/키워드: pre-extraction

검색결과 510건 처리시간 0.023초

상압조건의 마이크로파 공정과 현행 방법에 의한 인삼근 유용성분의 추출효율 비교 연구 (Comparative Effects of Microwave-Assisted Process Under Atmospheric Pressure Condition and Conventional Process on Extraction Efficiencies Ginseng Components)

  • 권중호;김경은
    • 한국식품영양과학회지
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    • 제28권3호
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    • pp.586-592
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    • 1999
  • Microwave assisted extraction(MAE) is known as a more environmental friendly process with economic advantages in terms of less time, less solvent, less energy and less wastes than the current time consuming reflux method. It was applied to develop a rapid extraction method for soluble ginseng components that are major materials used for the processing of ginseng products. In a comparative study between pre established MAE(ethanol 60%, power 80 W, process time 4 min$\times$5) and current extraction method(ethanol 80%, temp. 85oC, time 8 hr$\times$5), MAE was more efficient than the current method to obtain an extract yield(soluble solid), but it was insufficient to extract individual ginsenosides, total phenols, reducing components and acidic polysaccharides. MAE with 80% ethanol by 5 times showed, however, that its extraction efficiency on soluble solid, crude saponin, major ginsenosides, and the other components was equal or superior to that of the current method, indicating that ethanol concentration is one of the critical parameters influencing the MAE process. The quality of ginseng extracts from MAE was assured by evaluating the corresponding standards and by comparing TLC and HPLC patterns with the control.

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지리정보시스템을 이용한 장기유출모형의 개발(II) -전.후처리 시스템 개발- (Development of a Cell-based Long-term Hydrologic Model Using Geographic Information System(II) - Pre and Post Processor Development -)

  • 최진용;정하우;김대식
    • 한국농공학회지
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    • 제39권2호
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    • pp.103-112
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    • 1997
  • A CELTHYM(CEll-based Long-term HYdrologic Model), a pre-processor and a post-processor that can he integrated with geographic information system(GIS) were developed to predict the stream flow of a small agricultural watershed. Three kinds of routines, that are watershed boundary extraction routine(WBER), curve number calculation routine(CNR) and maximum available soil moisture calculation routine(MASR) composed pre-processor that was nicely interfaced with CELTRYM and GIS. Two kinds of routines, grapher and map composer composed post-processor that was well adapted CELTHYM output to chart making and GIS map making. The developed pre-post processor was useful for the GIS integration and spatial comprehension of the CELTHYM output.

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밤 외피 추출물을 이용한 면직물 염색에서의 두즙 전처리효과 (Reelection Device for Dyeability of Cotton Fabrics with Chestnut Husk Extract by Bean Sap Pre-treatment)

  • 김병미
    • 한국의상디자인학회지
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    • 제5권3호
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    • pp.15-23
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    • 2003
  • Chestnut trees have been used as a dyeing material, which are grow naturally, are cultivated all the area of Korea. So, there is abundant amount of the materials and they have better colorfastness than other natural dyeing materials. But chestnut husk extract is good at silk and wool fabrics, not cotton fabrics. That's why many methods using chestnut extraction for dyeing are being studied. But most of them depend on treatment method with chemical material which doesn't fit with the aim, using natural materials. Therefore in this research, we used protein pre-treatment method which is dyeing chestnut husk extract after treating at cotton fabrics with bean sap. And we studied the effect of dyeability of chestnut husk extract to cotton fabrics. As a result of pre-treatment of bean sap at cotton fabrics, dyeability was increased. Besides laundering fastness, dry cleaning fastness, perspiration fastness and light fastness were almost increased.

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이온성 액체를 이용한 바이오매스 추출에 의해 얻어진 추출물의 건조 방법 (Method for Drying of Crude Extract Obtained by Biomass Extraction Using an Ionic Liquid)

  • 김슬기;김진현
    • Korean Chemical Engineering Research
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    • 제54권3호
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    • pp.374-379
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    • 2016
  • 이온성 액체를 보조용매로 이용할 경우 바이오매스로부터 파클리탁셀의 추출 효율은 획기적으로 개선되지만 잔류 이온성 액체로 후속 농축 및 건조에 많은 어려움이 따른다. 따라서 본 연구에서는 공정 효율 향상을 위하여 이온성 액체를 이용한 바이오매스 추출물을 효과적으로 건조할 수 있는 새로운 방법을 개발하였다. 추출물을 물로 전처리하고 추가적으로 세척함으로써 잔류 이온성 액체 제거를 통해 효과적으로 건조할 수 있었다. 물 전처리을 위한 최적의 시료/물 비, 혼합시간 및 추가세척을 위한 최적의 시료/물 비는 각각 1:70 (w/v), 4분, 1:100 (w/v)이었다. 또한 진공 건조보다 마이크로웨이브를 이용한 건조의 경우 건조시간을 9배 정도 단축 가능하여 공정 효율이 획기적으로 개선될 것으로 판단된다.

영상처리 기술을 이용한 도로 및 차량 추출 기법에 관한 연구 (A Study on the Extraction of Road & Vehicles Using Image Processing Technique)

  • 가칠오;변영기;유기윤;김용일
    • 대한공간정보학회지
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    • 제13권4호
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    • pp.3-9
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    • 2005
  • 최근 영상 처리를 이용한 교통 정보 추출은 기존의 물리적인 장비들에 비하여 상대적으로 간단한 설치와 적은 비용으로 다양한 정보를 추출하는 장점으로 인하여 널리 연구되고 있다. 이러한 영상을 기반으로 하는 교통정보 추출 알고리즘들은 영상에서 관심 정보인 차량을 정확히 추출하는데서 시작된다. 교통 정보를 추출하는 전단계로서 영상 내에서 움직이는 차량을 검출하기 위해 많이 사용되는 배경빼기(background subtraction) 연산 후 영상 이진화 과정에서 상당한 양의 노이즈가 발생하며, 이는 교통정보의 정확도에 영향을 미친다. 이러한 노이즈는 모든 교통정보가 도로를 주행하고 있는 차량들로부터 추출됨에도 불구하고 실제 영상에서는 비도로영역의 가로수나 행인이 차량과 함께 움직임으로 검출되기 때문에 발생한다. 이를 위해 본 연구에서는 차선정보를 이용하여 도로영역을 추출함으로써 노이즈의 상당부분을 제거할 수 있었으며, 연산의 속도도 높일 수 있었다. 또한, 연속된 영상간의 비(ratio)를 이용하여 차량으로 인한 그림자의 효과를 최소화하였다.

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국내 담수역 남조류 원격탐사를 위한 피코시아닌 추출법 비교 연구 (A Study on Comparison of Phycocyanin Extraction Methods for Hyperspectral Remote Sensing of Cyanobacteria in Turbid Inland Waters)

  • 하림;신현주;남기범;박상현;강태구;송현오;이혁
    • 한국물환경학회지
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    • 제32권6호
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    • pp.520-527
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    • 2016
  • Phycocyanin (PC) is one of the water-soluble accessory pigments of cyanobacteria species, and its concentration is used to estimate the presence and relative abundance of cyanobacteria. In laboratory experiments, PC content of field data were determined using Sarada's freeze-thaw method in algal bloom season. The effectiveness of three selected extraction methods (repeated freeze-thaw method, homogenization, power control) for PC were determined. The extraction efficiency of phycocyanin was the highest (of the methods compared) when a single freezing-thawing cycle was followed by pre-sonication. Applying this optimized method to surface water of Korean inland waters, the average concentration distribution was estimated at $2.9{\sim}51.9mg/m^3$. It has been shown that the optimized pre-sonication method is suitable to measure cyanobacteria PC content for the characterization of inland waters. The approach and results of this study indicates the potential of effective methods for remote monitoring and management of water quality in turbid inland waters using hyperspectral remote sensing.

시료 중 잔류 항생제 분석 방법: II. 액상 시료 전처리 방법 (Determination of Antibiotic Residues: II. Extraction and Clean-up Methods for Liquid Samples_A Review)

  • 김찬식;류홍덕;정유진;김용석;류덕희
    • 한국물환경학회지
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    • 제32권6호
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    • pp.628-648
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    • 2016
  • Increased attention has been paid to the presence of veterinary antibiotics in various environmental matrices due to their toxicological behavior in the ecosystem and development of antibiotic-resistant strains of pathogenic bacteria. In the this review, 37 target antimicrobials were selected based on annual sales of antibiotics for livestock in South Korea 2014. Also, extraction and clean-up methods for the determination of the antibiotic residues in liquid samples including water, milk, and honey were comprehensively reviewed in the literature. Solid-phase extraction (SPE) was commonly used as a pre-treatment method for the samples. Most of the analytes were extracted in acidic conditions (2.5~4.0) except for aminoglycosides, which were extracted in neutral conditions (7.0~8.0). ${\beta}-Lactams$ showed the highest recoveries in neutral pH due to their degradation characteristics in acidic media. Starta-X, Oasis HLB, and Oasis MCX were frequently applied as an SPE cartridge and Oasis HLB showed the highest recoveries for the majority of antibiotic classes. The homogenized honey and milk were extracted by mixing with acids for deproteinization. Solids and other interfering substances in the extract were eliminated by centrifugation followed by membrane filtration or SPE before injection into HPLC.

극초단파를 이용한 건고추 올레오레진의 추출조건 설정 (Pre-establishment of Microwave-Assisted Extraction Conditions for Oleoresins from Dried Red Pepper)

  • 이정은;권중호;김현구
    • 한국식품저장유통학회지
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    • 제7권3호
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    • pp.267-272
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    • 2000
  • 건고추로부터 올레오레진을 신소가게 추출하고자 기존 추출방법들에 비하여 신속성과 환경친화성이 인정되고 있는 극초단파 추출공정에 필요한 몇 가지 기본조건을 검토하였다. 극초단파 추출에서 건고추의 입자 크기는 60 mesh, 시료와 용매(에탄올)의 비는 1:10(g/mL)이 적당하였고, 에너지 용량은 50 W에서 올레오레진과 capsanthin에 대한 추출효율이 가장 높게 나타났다. 가용성 고형분은 에탄올농도가 낮을수록 증가하였으나 capsanthin 함량은 75% 이상의 에탄올 농도에서 높은 증가현상을 나타내었다. 극초단파에 의한 올레오레진과 capsanthin의 추출은 짧은 시간에 이루어지므로 1회 추출시간은 3~5분이 적당한 것으로 나타났다.

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활엽수 알칼리 선추출물 내 헤미셀룰로오스의 분리 및 정제 (Isolation and Purification of Hemicelluloses in Alkali Pre-extractives from Mixed Hardwood)

  • 심규정;신희내;윤혜정;이학래
    • 펄프종이기술
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    • 제42권4호
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    • pp.64-70
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    • 2010
  • In this study, hemicelluloses were pre-extracted from mixed hardwood chips using sodium hydroxide solution and then they were isolated from pre-extractives by using various solvents. Isolation was conducted by precipitating hemicelluloses with isopropanol, ethanol, 1,4-dioxane, dimethylsulfoxide (DMSO) and potassium hydroxide (KOH), respectively. The precipitate yield on alkali pre-extractives was the highest when hemicelluloses were isolated by DMSO and then precipitated with ethanol. Most precipitates were yellow colored. The efficiency of isolation was evaluated by analysing the characteristics of isolated hemicelluloses. Isolation using DMSO, KOH and 1,4-dioxane ($80^{\circ}C$) showed rather high efficiency. The highest total separation efficiency was about 77% when alkali pre-extractives were reacted with KOH and precipitated with ethanol. The quantity and purity of isolated hemicelluloses were affected by the solvent type.

Three-dimensional changes in lip vermilion morphology of adult female patients after extraction and non-extraction orthodontic treatment

  • Liu, Zhi-Yu;Yu, Jie;Dai, Fan-Fan;Jiang, Ruo-Ping;Xu, Tian-Min
    • 대한치과교정학회지
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    • 제49권4호
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    • pp.222-234
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    • 2019
  • Objective: To investigate the three-dimensional lip vermilion changes after extraction and non-extraction orthodontic treatment in female adult patients and explore the correlation between lip vermilion changes and incisor changes. Methods: Forty-seven young female adult patients were enrolled in this study (skeletal Class III patients were excluded), including 34 lip-protruding patients treated by extraction of four first premolars (18 patients requiring mini-implants for maximum anchorage control and 16 patients without mini-implants) and 13 patients requiring non-extraction treatment. Nine angles, seven distances, and the surface area of the lip vermilion were measured by using pre- and post-treatment three-dimensional facial scans. Linear and angular measurements of incisors were performed on lateral cephalograms. Results: There were no significant changes in the vermilion measurements in the non-extraction group. The vermilion angle, vermilion height, central bow angle, height/width ratio, and vermilion surface area decreased significantly after the orthodontic treatment in the extraction groups, but the upper/lower vermilion proportion remained unchanged. Significant correlations were found between the changes in incisor position and those in vermilion angles, vermilion height, and surface area. Conclusions: Extraction of the four first premolars probably produced an aesthetic improvement in lip vermilion morphology. However, the upper/lower vermilion proportion remained unchanged. The variations in the vermilion were closely related to incisor changes, especially the upper incisor inclination changes.