• Proceedings of the KSME Conference
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• 2008.11a
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• pp.1806-1809
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• 2008

Study that form micro pattern by direct ink jet printing method is getting attention recently. Direct ink jet printing spout fine droplet including nano metal particle by force or air pressure. There is reason which ink jet printing method is profitable especially in a various micro-patterning technology. It can embody patterns directly without complex process such as mask manufacture or screen-printing for existent lithography. In this study, research of a technology that ejects fine droplet form of Pico liter and forms metal micro pattern was carried with inkjet head of piezoelectricity drive system. Droplet established pattern while ejecting consecutively and move on the surface at the fixed speed. Patterns formed in ink are mixed with organic solvent and polymer that act as binder. So added thermal hardening process after evaporate organic solvent at isothermal after printing. I executed high frequency special quality estimation of CPW transmission line to confirm electrical property of manufactured circuit board. We tried a large area printing to confirm application possibility of an ink jet technology.

• Journal of the Optical Society of Korea
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• v.13 no.1
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• pp.75-79
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• 2009

A four beam interference optical system for laser micro structuring using a pulse laser was demonstrated. The four beam interference optical system using a pulse laser(picosecond laser) can fabricate micro structure on mold material(NAK80) directly. Micro structure on the polymer can be reproduced economically by injection molding of the micro structure on the mold material. The four beam interference optical system was composed by the DOE(Diffractive Optical Element) and two lenses. The laser intensity distribution of four beam interference was explained by an interference optics point of view and by the image optics point of view. We revealed that both views showed the same result. The laser power distribution of a $1{\mu}m$ peak pattern was made by the four beam interference optical system and measured by the objective lens and CCD. A $1{\mu}m$ pitch dot pattern on the mold material was fabricated and measured by SEM(Scanning Electron Microscopy).

• YAKHAK HOEJI
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• v.41 no.1
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• pp.48-59
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• 1997

Sustained release matrix tablets, pellets, and coated pellets for the delivery of sulindac were prepared using cellulose derivatives at various ratios, and evaluated for the dis solution pattern. The release of sulindac, from matrix tablets prepared with low viscosity HPMC was relatively fast, and especially the tablets made of Metolose SM released all of sulindac within 1 hr. The release of drug from tablets made of other HPMC derivatives were retarded in the order of the following: Pharmacoat 645>Pharmacoat 606>Pharrnacoat 606+HPC-L>HPC-L. The most sustained release pattern was observed with the preparation of high viscous polymer. Metolose 90 SH. While release of sulindac, from matrix type pellet containing 10mg/cap of Metolose 90 SH or 60 SH was completed within 1 hr, a prolonged release formulation (30% in 1 hr) was obtained by the inclusion of EC. Pellets coated with HPMC showed a fast release pattern (${\geq}$ 80% within 2 hrs), whereas pellets coated with HPMC and EC (molar ratio 1 : 1) showed a sustained release pattern (${\geq}$ 80% in 12 hrs), vath the release from EC pellets being the most sustained. Fast (naked) and slow release pellets coated with EC, Metolose 60SH 50cps and propylene glycol. and enteric pellets coated with HPMCP 55 and Myvacet$^{\circledR}$ were prepared, and combined at various ratios for the assessment of dissolution pattern. The result indicates the possibility that the development of 24 hr sustained release delivery systems containing sulindac for oral administration could be achieved by means of combining sustained and fast release pellets at a proper portion.

• Computers and Concrete
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• v.29 no.4
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• pp.219-235
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• 2022

Strengthening slender reinforced concrete (RC) columns is a challenge. They are susceptible to overall buckling that induces bending moment and axial compression. This study presents the precise three-dimensional finite element modeling of slender RC columns strengthened with fiber-reinforced polymer (FRP) composites sheets with various patterns under concentric or eccentric compression. The slenderness ratio λ (height/width ratio) of the studied columns ranged from 15 to 35. First, to determine the optimal modeling procedure, nine alternative nonlinear finite element models were presented to simulate the experimental behavior of seven FRP-strengthened slender RC columns under eccentric compression. The models simulated concrete behavior under compression and tension, FRP laminate sheets with different fiber orientations, crack propagation, FRP-concrete interface, and eccentric compression. Then, the validated modeling procedure was applied to simulate 58 FRP-strengthened slender RC columns under compression with minor eccentricity to represent the inevitable geometric imperfections. The simulated columns showed two cross sections (square and rectangular), variable λ values (15, 22, and 35), and four strengthening patterns for FRP sheet layers (hoop H, longitudinal L, partial longitudinal L_w, and longitudinal coupled with hoop LH). For λ=15-22, pattern L showed the highest strengthening effectiveness, pattern L_w showed brittle failure, steel reinforcement bars exhibited compressive yielding, ties exhibited tensile yielding, and concrete failed under compression. For λ>22, pattern L_w outperformed pattern L in terms of the strengthening effectiveness relative to equivalent weight of FRP layers, steel reinforcement bars exhibited crossover tensile strain, and concrete failed under tension. Patterns H and LH (compared with pattern L) showed minor strengthening effectiveness.

• Applied Chemistry for Engineering
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• v.17 no.2
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• pp.217-222
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• 2006

Polyimides have been investigated extensively and used widely over the past three decades because of their high performance properties such as excellent thermal, mechanical, and electrical properties. Polyimides are difficult to be processed because of the aromatic moieties, imide group, and insoluble nature in most organic solvents. The soluble polyimides were synthesized from 2,2,-bis(3-amino-4-hydroxyphenyl) hexafluoropropane (BAPAF) and 3,3,-diamino-4,4-dihydroxybyphenyl (HAB) as aromatic diamines and 4,4-(hexafluoroisopropylidene)diphthalic dianhydride (6FDA), pyromellitic dianhydride (PMDA), 4,4-oxydiphthalic dianhydride (OPDA), 3,3,4,4-benzophenone tetracarboxylic dianhydride (BTDA) and 3,3,4,4-diphenylsulfone tetracarboxylic dianhydride (DSDA) as aromatic dianhydrides. The polyimides were characterized by NMR, FR-IR, TGA and the dielectric constant of the obtained polyimides was calculated from storage of electro-capacity. A novel photosensitive polyimide was synthesized by the reaction of polyimide, containing hydroxyl group and methacryloyl chloride using triethylamine. The good micro-pattern was obtained with photosensitive polyimide from the photolithographic technique.

• Korean Journal of Optics and Photonics
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• v.17 no.1
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• pp.99-103
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• 2006

A tunable wavelength filter was proposed and demonstrated by using the UV nanoimprint technique. It consists of a Bragg grating in polymer waveguides and a heating electrode. The manufacturing of the grating was substantially simplified with the introduction of a smart imprint stamp containing a waveguide pattern integrated with the grating pattern. The center wavelength of the filter was successfully tuned by taking advantage of the thermooptic effect in polymers, which was induced by supplying electrical power to the electrode. For the fabricated device, a transmission dip of ${\~}$15 dB and a 3-dB bandwidth of 0.8 nm were obtained at the Bragg wavelength of ${\~}$l560 nm. The achieved thermooptic tuning efficiency was ${\~}$0.28 nm/mW, while the center wavelength was shifted from 1560 nm to 1558 nm with the electrical power consumption of 7 mW.

• Applied Chemistry for Engineering
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• v.19 no.4
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• pp.402-406
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• 2008

A series of random copolymers, composed of 1H,1H,2H,2H-perfluoro decyl methacrylate (FDMA) as a $CO_2$-philic monomer and tert-butyl methacrylate (TBMA) as an acid labile monomer, were synthesized by free radical polymerization. The solubility of copolymers in carbon dioxide, light sensitivity at 365 nm exposure, and photoresist pattern formation properties were investigated. Furthermore, sub micron-sized poly(styrenesulfonate) : poly(3,4-ethylenedioxythiophene) (PSS : PEDOT) conducting polymer patterns were successfully prepared by pattern transfer.

• Polymer(Korea)
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• v.26 no.1
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• pp.128-138
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• 2002

1,3-Bis(2-chloroethyl)-1-nitrosourea (BCNU, Carmustine)-loaded poly(D, L-lactide-co-glycolide) (PLGA, lactide/glycolide mole ratio 75 : 25) microparticles were prepared and fabricated into wafers in an attempt to study the possibility for the treatment of malignant glioma by direct inserting the wafers to the tumor or the cavity remained after surgical resection of the tumor. SEM observation of the microparticles prepared by spray drying method revealed that the microparticles were spherical, i. e. microspheres. Significant reduction of the crystallinity of BCNU encapsulated in PLGA was confirmed by X-ray diffraction and differential scanning calorimetry analyses of the BCNU-loaded PLGA microparticles. Release pattern of BCNU was dependent on several preparation parameters, such as the molecular weight and concentration of PLGA, and initial BCNU loading amount, etc. In vitro release of BCNU was prolonged over 8 weeks with close to zero-order release pattern after initial burst effect. Observations of morphological change of wafers and pH change of release media during release test period confirmed that hydration and degradation of PLGA would be facilitated with an increase of BCNU-loading amount.

• Polymer(Korea)
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• v.35 no.1
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• pp.1-6
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• 2011

Pressurized high temperature plastic resin flows into the cavity of mold and is solidified in injection molding process. Residual stress is being developed in injection molded part because of high temperature variations and high pressure. Developed residual stress relaxes as time goes. Consequently this makes part deformed and deteriorates quality of product. A measurement method of residual stress for injection molded transparent articles has been investigated using photoelasticity. Light, a composite of electromagnetic waves, is purified into a single wave by a polarized film. When this wave passes through the specimen, birefringence is developed according to the level of residual stress in the specimen and color fringed pattern appears after the second polarized film. Residual stress in the injection molded transparent flat a part has been measured quantitatively using the color fringed pattern. Optical characteristics have been a part also predicted by computer simulation and compared with experimental results.

• Polymer(Korea)
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• v.38 no.3
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• pp.358-363
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• 2014

Adhesion forces between acrylate imprinting resin and a surface treated atomic force microscope (AFM) tip were investigated. Compared to the untreated silicon tip, 38% of the adhesion force is reduced for the hydrophobic tip treated with $CH_4$ plasma whereas 1.6 time increases is found for the hydrophilic tip with $O_2$ plasma treatment. Such a measurement of the adhesion force using AFM provides very quantitative results on adhesion comparing to the crosscut adhesion test which gives qualitative results. Since the adhesion area becomes larger as the imprinting pattern size gets smaller, the surface treatment issue becomes more important in the nano-imprinting process.