• Title/Summary/Keyword: pesticide analysis

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Current status on pesticide residues in commercial agricultural commodities in Seoul area (서울시내 유통 농산물에서의 농약잔류 실태)

  • 한선희
    • Proceedings of the Korea Society of Environmental Toocicology Conference
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    • 2003.10a
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    • pp.49-53
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    • 2003
  • Through the five years analysis of monitoring data on pesticide residues from 1998 to 2002, current status on pesticide residues on commercial agricultural products in Seoul area was evaluated. The rate of over maximum residue limits(MRLs) has been decreased into 5.8% in 1998, 2.5% in 1999, 1.6% in 2000, 1.4% in 2001, and 1.5% in 2002 gradually, where as total sample numbers analyzed increased 1,300 in 1998, 4,200 in 1999, 5740 in 2000, 6,160 in 2001, and 5,440 in 2002 annually, The pesticide which frequently detected in samples were endosulfan, procymidone, chlorotalonil, vinclozolin, and chlorpyriphos and pesticide found over MRLs were procymidone, vinclozolin, endosulfan and etc.

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Consumers' Awareness and Information Needs towards Food Hygiene(I): Focused on Pesticide Residues (식품위생에 대한 소비자의 인식도 및 정보요구도에 관한 연구(I): 잔류농약을 중심으로)

  • 김효정;김미라
    • Journal of the Korean Home Economics Association
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    • v.41 no.1
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    • pp.15-26
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    • 2003
  • The purpose of this study was to examine the consumers' awareness and information needs towards pesticide residues and to find out the factors affecting the information needs. Data were collected from 506 adults in Seoul, Daegu and Busan by the self-administered questionnaire. Frequencies, X²tests, and regression analysis were conducted to analyze the data by SPSS Windows. The results of this study were as follows: (1) many respondents showed the high concerns and information needs for pesticide residues (2) many people worried to eat vegetables, fruits and cereals in turn due to pesticide residues, and did not trust the results from food safety tests by the government, and (3) age, educational attainment and concerns about pesticide residues were factors affecting the consumers' information needs.

Monitoring and Exposure Assessment of Pesticide Residues in Domestic Agricultural Products (국내 유통 다소비 농산물의 잔류농약 모니터링 및 노출평가)

  • Kang, Namsuk;Kim, Seongcheol;Kang, Yoonjung;Kim, Dohyeong;Jang, Jinwook;Won, Sera;Hyun, Jaehee;Kim, Dongeon;Jeong, Il-Yong;Rhee, Gyuseek;Shin, Yeongmin;Joung, Dong Yun;Kim, Sang Yub;Park, Juyoung;Kwon, Kisung;Ji, Youngae
    • The Korean Journal of Pesticide Science
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    • v.19 no.1
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    • pp.32-40
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    • 2015
  • This study was implemented to evaluate food safety on residual pesticides in agricultural products of Korea and to use as a data base for the establishment of food policy. A total of 196 pesticide upon these products were analyzed using multi class pesticide multiresidue methods of Korean Food Code, and 232 samples of 15 agricultural products collected from 9 regions were supplied for this study. In the results, 64 kinds of pesticides were detected in 53 samples, chlorpyrifos and procymidone of them were shown a high frequency of detection in the analyzed pesticides. Among them, two samples (chlorpyrifos in perilla leaves and picoxystrobin in peach) were detected over Maximum Residue Limits (MRLs). The levels of the detected pesticide residues were within safe levels. Also, the intake assessment for pesticide residues including chlorpyrifos at multi pesticide residue monitoring were carried out. The result showed that the ratio of EDI (estimated daily intake) to ADI (acceptable daily intake) was 0.001~0.902% which means that the detected pesticide residues were in a safe range so that residual pesticides in the agricultural products in Korea are properly controlled.

Monitoring of Pesticide Residues in Special Products (지역특산품 중 잔류농약 실태조사)

  • Kim, Mi-Ra;Na, Mi-Ae;Jung, Woo-Young;Kim, Chang-Soo;Sun, Nam-Kyu;Seo, Eun-Chae;Lee, Eun-Mi;Park, You-Gyoung;Byun, Jung-Ah;Eom, Joon-Ho;Jung, Rae-Seok;Lee, Jin-Ha
    • The Korean Journal of Pesticide Science
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    • v.12 no.4
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    • pp.323-334
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    • 2008
  • This experiment was carried out to analyze for pesticide residues in 17 different types of the special of geographical indication. We purchased 3 cereal grains, nuts and seeds, 3 fruits, 8 vegetables, mushrooms and other plants (Korean medicines) mainly at the agricultural cooperative's joints markets. Total 209 pesticides including multi-analysed pesticides (204) and single-analysed pesticides (5 ; acephate, methamidophos, monocrotophos, omethoate, vamidothion) were analysed with a GC/MS/MS, an HPLC/UVD (PDA) and a GC/FPD. No. 83 method and single-analysed method (Screening of multi-pesticide residue in the special products of geographical indication) of Korea Food Code was selected for validation in recovery and interferences of matrice. The results were as follows: among the selected 17 the special products, the residual pesticides were detected in 8 types of the special products (40 in 302 samples, detection ratio; 13.2%). All of the samples were not detected over MRLs, but tebuconazole, procymidone and isoprothioran were detected with considerable high frequency. These results could be used as KFDA official methods for the analysis of pesticide residues in foods and reference data will be provided to the related institutions.

Evaluation of Results in Pesticide Residues on Incongruity Commercial Agricultural Commodities using Network Analysis Method (네트워크 분석을 활용한 유통농산물 잔류농약 부적합 현황 분석)

  • Park, Jae Woo;Seo, Jun Ho;Lee, Dong Hun;Na, Kang In;Cho, Sung Yong;Bae, Man Jae
    • Journal of Food Hygiene and Safety
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    • v.33 no.1
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    • pp.23-30
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    • 2018
  • The purpose of this research was to introduce network analysis method for analyzing pesticide residues in incongruity commercial agricultural commodities. Based on the "results in pesticide residues on incongruity commercial agricultural commodities" on "Guidelines for food safety management 2017", we used centrality analysis for pesticide residues via degree, closeness and betweenness centrality measurement. In case of degree centrality result, chlorpyrifos and diazinon were the most highly "connected node" in pesticide network. For the closeness centrality result, the most pesticides showed the similar closeness trend except for 19 species of pesticides. Fludioxonil and chlorpyrifos are recognized as the "bridge" of pesticides network with their high betweenness centrality. The results of network analysis show the "relation" data, which could not represent through out the conventional statistical analysis, among the pesticide residues. We hope that the network analysis method will be appropriate and precise tool for analyzing pesticide residues via elaboration and optimization.

The Effects of Food Safety Accident on the Consumption of Eggs : Focusing on the Pesticide-related Accident (식품안전사고가 계란 소비에 미치는 영향: 계란의 살충제검출사고를 중심으로)

  • Han, Byeol;Yang, Sung-Bum
    • Korean Journal of Organic Agriculture
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    • v.27 no.1
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    • pp.17-32
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    • 2019
  • The objective of this study is to investigate the effect of pesticide-related accident on prices and sales of eggs and the perception of food safety accidents among consumers. For this, we analyzed the impact of the pesticide incident on consumers' purchases by separating large discount stores and eco-friendly specialty stores with econometrics methods. In addition, the value changes for each egg certification were analyzed after the accident. Perception of food safety accidents was conducted through a survey to investigate the awareness of the pesticide-related accidents, changes in purchases, and the causes of the pesticide accidents. Furthermore, the risk analysis was conducted. This results show the importance of trust and communication in food safety accidents between distributors, consumers and concerned authorities. Also, after the accident, consumers' interest and premium exist in the breeding process such as animal welfare, not only in the final product. Therefore in order to actively respond to food safety accidents such as pesticides-related accident, response and improvement are necessary considering various aspects such as risk assessment, risk management, and risk communication.

Determination and Validation of an Analytical Method for Dichlobentiazox in Agricultural Products with LC-MS/MS (LC-MS/MS를 이용한 농산물 중 Dichlobentiazox 시험법 개발 및 검증)

  • Gu, Sun Young;Lee, Han Sol;Park, Ji-Su;Lee, Su Jung;Shin, Hye-Sun;Kang, Sung Eun;Chung, Yun Mi;Choi, Ha Na;Yoon, Sang Soon;Jung, Young-Hyun;Yoon, Hae Jung
    • Korean Journal of Environmental Agriculture
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    • v.40 no.2
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    • pp.108-117
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    • 2021
  • BACKGROUND: Dichlobentiazox is a newly registered pesticide in Korea as a triazole fungicide and requires establishment of an official analysis method for the safety management. Therefore, the aim of this study was to determine the residual analysis method of dichlobentiazox for the five representative agricultural products. METHODS AND RESULTS: Three QuEChERS methods were applied to establish the extraction method, and the EN method was finally selected through the recovery test. In addition, various adsorbent agents were applied to establish the clean-up method. As a result, it was found that the recovery of the tested pesticide was reduced when using the d-SPE method with PSA and GCB, but C18 showed an excellent recovery. Therefore this method was established as the final analysis method. For the analysis, LC-MS/MS was used with consideration of the selectivity and sensitivity of the target pesticide and was operated in MRM mode. The results of the recovery test using the established analysis method and inter laboratory validation showed a valid range of 70-120%, with standard deviation and coefficient of variation of less than 3.0% and 11.6%, respectively. CONCLUSION: Dichlobentiazox could be analyzed with a modified QuEChERS method, and the method determined would be widely available to ensure the safety of residual pesticides in Korea.

Pesticide exposure of alpine agricultural workers in Gangwon-do and the measurement of their health status measured by SF-12 (강원도 고랭지 농업인의 농약 노출 및 SF-12를 이용한 건강수준 측정)

  • Song, Jae-Seok;Park, Woong-Sub;Seo, Jong-Chul;Kwak, Youn-Hee;Kim, Sang-Ah;Kim, Byung-Sup;Choi, Hong-Soon
    • The Korean Journal of Pesticide Science
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    • v.9 no.4
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    • pp.287-291
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    • 2005
  • The development of agricultural technology makes the increasement of pesticide usage. The results of pesticide usage were the increment of agricultural outcomes, but the health hazard was increasing also. Especially, alpine agriculture needs more pesticide than general agriculture and they suffered from more pesticide induced health symptoms. There were no study about the pesticide usage and subjective health status. So, this study was performed to investigate the relationship between pesticide usage and health status. The health status was measured by SF-12. SF-12 was well known health status measurement tool. SF-12 have two components, which were mental component score and physical component score. As a results of analysis, the alpine agricultural workers had higher pesticide exposure index and acute symptom score. As the results of multivariate analysis, physical component score was affected by pesticide exposure, but mental component score was not. Although, this study has many limitations, the result of this study can suggest the need of political advise and the further study.

Monitoring and Risk Assessment of Pesticide Residues for Circulated Agricultural Commodities in Korea-2013 (국내 유통 농산물의 잔류농약 모니터링 및 위해평가-2013년)

  • Kim, Jae-Young;Lee, Sang-Mok;Lee, Han-Jin;Chang, Moon-Ik;Kang, Nam-Sook;Kim, Nam-Sun;Kim, Heejung;Cho, Yoon-Jae;Jeong, Jiyoon;Kim, Mee Kyung;Rhee, Gyu-Seek
    • Journal of Applied Biological Chemistry
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    • v.57 no.3
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    • pp.235-242
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    • 2014
  • The purpose of this study is the establishment of scientific processes for making food safety policies. Thus, we investigated pesticide residue level of the agricultural commodities from market, and performed risk assessment. Fifteen agricultural items are chosen based on the frequency of Korean consumption. The samples were collected from 9 cities where populations are more than one million. Total 283 active ingredients were monitoring ( total sample number =232). Single-analysis of target pesticides was for three kinds of possible growth regulators and the multicomponent analysis was for 280 kinds of pesticides, a total of 283 species were selected to perform the pesticide residues. Before monitoring the analytes, the improvements of the analytical methods were done by method validations under the CODEX analytical method development guidelines and can produce metrics that represent the international standards applied in accordance with the guidelines. In addition to residual pesticides detected during monitoring we compare the ADI to EDI values using detected result and dietary consumption data which is extracted from annual market basket survey. The 163 samples were non-detected in the total 232 samples so it means that every agricultural commodity will residual pesticides-free in 70.3%. The detected residual pesticides showed for a total of 69 cases (29.7%). Two of samples violate Korean MRL (0.9%). The ratio of EDI compared to ADI resulted in only from 0.00087 to 0.902%. In result, we can assume that all detected residual pesticides are very safe level and current policies of Korean pesticides control may be working.

Development of Colorimetric Paper Sensor for Pesticide Detection Using Competitive-inhibiting Reaction

  • Kim, Hyeok Jung;Kim, Yeji;Park, Su Jung;Kwon, Chanho;Noh, Hyeran
    • BioChip Journal
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    • v.12 no.4
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    • pp.326-331
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    • 2018
  • Contamination by pesticides is an everincreasing problem associated with fields of environmental management and healthcare. Accordingly, appropriate treatments are in demand. Pesticide detection methods have been researched extensively, aimed at making the detection convenient, fast, cost-effective, and easy to use. Among the various detecting strategies, paper-based assay is potent for real-time pesticide sensing due to its unique advantages including disposability, light weight, and low cost. In this study, a paper-based sensor for chlorpyrifos, an organophosphate pesticide, has been developed by layering three sheets of patterned plates. In colorimetric quantification of pesticides, the blue color produced by the interaction between acetylcholinesterase and indoxyl acetate is inhibited by the pesticide molecules present in the sample solutions. With the optimized paper-based sensor, the pesticide is sensitively detected (limit of detection =8.60 ppm) within 5min. Furthermore, the shelf life of the device is enhanced to 14 days after from the fabrication, by treating trehalose solution onto the deposited reagents. We expect the paper-based device to be utilized as a first-screening analytic device for water quality monitoring and food analysis.