• Title/Summary/Keyword: mixed resin

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Fabrication and Characterization of PZT Suspensions for Stereolithography based on 3D Printing

  • Cha, JaeMin;Lee, Jeong Woo;Bae, Byeonghoon;Lee, Seong-Eui;Yoon, Chang-Bun
    • Journal of the Korean Ceramic Society
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    • v.56 no.4
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    • pp.360-364
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    • 2019
  • PZT suspensions for photo-curable 3D printing were fabricated and their characteristics were evaluated. After mixing the PZT, photopolymer, photo-initiator, and dispersant for 10 min by using a high-shear mixer, the viscosity characteristics were investigated based on the powder content. To determine an appropriate dispersant content, the dispersant was mixed at 1, 3, and 5 wt% of the powder and a precipitation test was conducted for two hours. Consequently, it was confirmed that the dispersibility was excellent at 3 wt%. Through thermogravimetric analysis, it was confirmed that weight reduction occurred in the photopolymer between 120? and 500?, thereby providing a debinding heat treatment profile. The fabricated suspensions were cured using UV light, and the polymer was removed through debinding. Subsequently, the density and surface characteristics were analyzed by using the Archimedes method and field-emission scanning electron microscopy. Consequently, compared with the theoretical density, an excellent characteristic of 97% was shown at a powder content of 87 wt%. Through X-ray diffraction analysis, it was confirmed that the crystallizability improved as the solid content increased. At the mixing ratio of 87 wt% powder and 13 wt% photo-curable resin, the viscosity was 3,100 cps, confirming an appropriate viscosity characteristic as a stereolithography suspension for 3D printing.

TREATMENT OF CROWN-ROOT FRACTURE BY INTENTIONAL REPLANTATION : CASE REPORT (의도적 재식술을 이용한 치관-치근 파절의 치험례)

  • Son, Ju-Hyo;Choi, Hyung-Jun;Sohn, Heung-Kyu
    • Journal of the korean academy of Pediatric Dentistry
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    • v.27 no.2
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    • pp.256-261
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    • 2000
  • Trauma to the tooth is the most common accidents in pediatric dentistry and tooth fracture occurs frequently. Fracture is classified into crown fracture, root fracture, and crown-root fracture which involves both. Also, it is classified into simple or complicated fracture depending on whether the pulp is exposed or not. When the fracture is extended down to the subgingival level following the long axis of the root, or when more than 1/3 of the root is involved, extraction is the primary treatment. But alternative treatment such as extruding the root fragment with orthodontic force and restoring it, or intentionally extracting the tooth and replanting it to a position which it can be restored. This is a case report on intentional replantation of a traumatized maxillary central incisor with crown-root fracture of a patient with mixed dentition. The teeth was extracted and immediate endodontic treatment, retrograde filling and resin restoration were carried out.

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EFFECT OF FLUORIDE APPLICATION ON DENTIN BONDING (불소도포가 상아질 접착에 미치는 영향)

  • Kwon, Hyoung-Jo;Park, Jin-Hoon;Cho, Kyeu-Zeung
    • Restorative Dentistry and Endodontics
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    • v.20 no.1
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    • pp.113-128
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    • 1995
  • The purpose of this study was to investigate the effect of stannous fluoride on the dentin bonding with three kinds of commercially available dentin bonding systems containing different adhesive monomers. Dentin specimens with exposed labial dentin prepared from freshly extracted bovine mandibular anterior teeth were divided into experimental and control groups. The specimens of experimental groups were bonded with dentin bonding systems and composite resins including All bond 2 ㅡ& Bisfil, Scotchbond Multi-Purpose & Z100, and Denthesive II Charisma after 2 % stannous& fluorided application for S minutes and washing for 1 minute. The specimens of control groups were bonded with the same dentin bonding systems and composite resins as used in the experimental groups. After bonded specimens were stored in $37^{\circ}C$ distilled water for 24 hours, the tensile bond strength and cohesive failure rate were measured, and then the pretreated dentin surfaces and the fractured dentin surfaces were examined under scanning electron microscope. The results were as follows : Mean bond strength of stannous fluoride applied groups of All bond 2, Scotchbond MP, and Denthesive II were 2.5MPa, 1.1MPa, and 1.1MPa respectively, and those of control groups were 7.5MPa, 8.1MPa, and 4.6MPa. Bond strength values of stannous fluoride applied groups were significantly lower than those of the control groups(p<0.05). SEM findings of dentin surfaces after stannous fluoride application demonstrated an appearance of partially remained smear layer and smear plugs inspite of pretreatment with 10 % phosphoric aicd or maleic acid solution, and an appearance of smear layer covered surface under Denthesive II priming. But those of control groups commonly showed clean dentin surfaces without smear layer and smear plugs. On SEM observation of the fractured dentin-resin interface, while most of the specimens of stannous fluoride applied groups showed adhesive failure mode, those of All bond 2 and Scotchbond MP control groups showed mainly adhesive-cohesive mixed failure mode, and mainly adhesive failure mode in Denthesive II control group.

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Mix Design and Mechanical Properties of Aerated Concrete for Incorporation of Low Temperature PCM (저온 PCM 혼입을 위한 경량기포콘크리트의 배합설계 및 기계적 특성)

  • Baasankhuu, Batzaya;Lim, Myung-Kwan;Lim, Hee-Seob;Choi, Dong-Uk
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.21 no.4
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    • pp.110-115
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    • 2017
  • This research was performed to investigate the mechanical performance of lightweight concrete including phase changing material(Low temperature PCM). Micro capsulised PCM consisted of wax type core and melamine based wall. Also, for PCM of one single kind, paraffin wax was inserted into Vermiculite and the surface was coated with melamine resin. Interfacial polymerization is based on the principle that macromolecule reaction takes place on the surfaces between 1-dodecanol(core material) and water (solvent) to form the wall material. Lightweight concrete has compressive strength of 10 MPa, tensile strength of 1.5 MPa, and oven dried density of 1.0kg/liter which included 10%, 20%, or 30% PCM by weight. To do so, this study fabricated light-weight foamed concrete ($1.0kg/m^3$) in pre-foaming method and mixed it with PCM micro capsule of 1-dodecanol and melamine to examine its physical properties.

The Field Applicability of Road Pavement Layer with Grid Typed Reinforcement and Dispersive Fiber (그리드형 보강재와 분산성 섬유를 활용한 도로 포장층의 현장 적용 특성)

  • Park, Ju-Won;Kim, Hun-Kyum;Kim, Sung-Bo
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.22 no.3
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    • pp.53-59
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    • 2018
  • This study analyzed the field applicability through the combination of environment-friendly grid-typed reinforcements and pre-mixed fiber with filler. The film of the grid-typed reinforcement is made by recycled PE resin. And, Ascon fiber is obtained the dispersion by pre-mixing of filler. To be able to recognize in advance the various circumstances that could arise in the construction of the road pavement layer, we conducted a basic field application test of the (Mock Up) pavement layer. As a result, it was found that the pavement with environment-friendly grid-typed reinforcement and dispersive fiber construction had improved strength, stress, and rutting resistance. It is consistent with the strength and stress results of the actual test of the mock up specimen. It is expected to perform an effective role in the safety as well as the use of environment-friendly fibers in actual construction.

THE STUDY ON THE PHYSICAL PROPERTY OF THE PERMANENT SOFT DENTURE LINERS (영구 연성 의치상 이장재의 물리적 성질에 관한 연구)

  • Kim, Yeon-Mi;Bae, Jeong-Sik
    • The Journal of Korean Academy of Prosthodontics
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    • v.37 no.6
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    • pp.809-818
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    • 1999
  • This study was performed to evaluate the tensile bond strength and modulus of elasticity of three permanent soft denture liners (Molloplast $B^{(R)}$, Ufi Gel $C^{(R)},\;Tokuyama^{(R)}$) before and after thermocycling. And their water sorption were also evaluated. Each soft denture liner was bonded to PMMA denture base resin blocks and the tensile bond strength and modulus of elasticity were measured by using universal testing machine. For the water sorption, weight measured after immersion of sea denture liners in $37{\pm}1^{\circ}C$ water bath for 4 weeks. The results were as follows : 1. Molloplast $B^{(R)}$ had the highest tensile bond strength, while Tokuyama had the lowest tensile bond strength. There was no significant difference between $Tokuyama^{(R)}$ and Molloplast $B^{(R)}$ in the both nonthermocycling and thermocycling. There was significant difference in tensile strength of $Tokuyama^{(R)}$ before and after thermocycling(p<0.05). 2. For the modulus of elasticity, there was no significant difference between Ufi Gel $C^{(R)}\;and\;Tokuyama^{(R)}$ in the both nonthermocycling and thermocycling. There was significant difference in modulus of elasticity of $Tokuyama^{(R)}$ before and after thermocycling(p<0.05). 3 The failure modes of Molloplast $B^{(R)}$ and Ufi Gel $C^{(R)}$ were mainley adhesive type and that of $Tokuyama^{(R)}$ was mainly mixed type in case of nonthermocycling and cohesive type after thermocycling. 4. The water sorption of each soft liners was within ${\pm}2%$ in times (p<0.05) but. there was no significant difference among the soft liners in times.

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SHEAR BOND STRENGTH OF SELF-ETCHING ADHESIVES TO DENTIN AND SEM ANALYSIS (상아질에 대한 자가 산부식 접착제의 전단결합강도와 SEM 분석 비교)

  • Cho, Young-Gon;Roh, Kee-Sun;Kim, Soo-Mee;Lee, Young-Gon;Jeong, Jin-Ho;Ki, Young-Jae
    • Restorative Dentistry and Endodontics
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    • v.28 no.3
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    • pp.222-231
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    • 2003
  • The purpose of this study was to compare shear bond strength and interfacial pattern of composite bond-ed to dentin using self-etching adhesive systems. Sixty extracted human molars with exposed occlusal dentin were divided into four groups and bonded with four adhesives and composites. Single Bond/Filtek Z 350(SB), Tyrian SPE-One-Step Plus/Aelitefil(TY), Prompt L-Pop/Filtek Z 250(LP), and One-Up Bond F/palfique Toughwell(OU). The results of this study were as follows; 1 Shear bond strength for OU was significantly lower than that of other groups(p<0.05). No significant difference was founded among SB, TY, and LP. 2. Failure modes to dentin showed adhesive and mixed for SB TY and LP, but them for OU showed adhesive in all spceimens. 3. Dentin-resin interface showed close adaptation for SB, TY, and LP, but it showed gap for OU. 4. The hybrid layers for TY, LP OU were thinner than that of SB. Adhesive layers were observed between composite and hybrid layer, which were 5 $\mu\textrm{m}$ thick for TY and 10 $\mu\textrm{m}$ thick for OU.

An Experimental Study on the Permeability of Reinforcement Concrete on Consideration of Pre-loading (선행하중을 고려한 보강 콘크리트의 투수성능에 관한 실험적 연구)

  • Han, Byoung-Young;Bae, Ju-Seong
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.9 no.3
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    • pp.87-92
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    • 2005
  • The permeability of concrete affects largely on the durability of concrete, therefore it is required that the correct assessment and improvement of permeability. Therefore it is rational method that the permeability of concrete structures is estimated in the common use states under loading than in the early sound conditions. In this study, to improve the permeable efficiency of concrete, some kinds of fiber and resin are mixed in making of concrete specimens. And also, for the reasonable assessment of permeability, after 50% and 70% pre-loadings of its compressive strength were acted on the specimens, the tests were executed. From the results of this study, in the case of 50% pre-loading coefficients of permeability were increased about 1.4times against the nonpre-loading specimens and in the case of 70% pre-loading they were increased about 17.8times. And it turned out that hybrid steel fiber reinforcement is most effective for the improvement of permeable efficiency of concrete.

SURGICAL REPOSITIONING OF AN IMPACTED INCISOR IN MIXED DENTITION (매복된 중절치의 재식)

  • Choi, Su-Mi;Lee, Keung-Ho;Choi, Yeong-Chul;Park, Jae-Hong
    • Journal of the korean academy of Pediatric Dentistry
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    • v.32 no.4
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    • pp.687-692
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    • 2005
  • Delayed eruption of a maxillary incisor results in midline shift, the space occupied by adjacent teeth and different levels of alveolar height. Extraction or surgical/orthodontic therapy is the most common treatment for a impacted maxillary incisor. Surgical repositioning provides another option for treatment of this problem. The advantages of this approach include immediate esthetic improvement, use of a single and simplified surgical procedure, simple and short orthodontic therapy, a normal gingival margin and the possibility of the developing root adapting to the new position. Autotransplantation of an immature tooth provides for possible adaptation of the developing root apex to the new position. A root with an open apex has good chance of pulp revascularization after transplantation.

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A Study on Failure Mechanisms of Composite Tubes with Woven Fabric Carbon, Glass and Kevlar/epoxy Under Compressive Loadings (직조된 탄소, 유리 및 케블라 섬유 복합소재 튜브의 압축하중하에서 파손 메커니즘 분석 연구)

  • Kim, Jung-Seok;Yoon, Hyuk-Jin;Lee, Ho-Sun;Kwon, Tae-Soo
    • Journal of the Korean Society for Railway
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    • v.12 no.4
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    • pp.590-596
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    • 2009
  • In this study, the failure modes and energy absorption characteristics of four different kinds of circular tubes made of carbon, glass, Kevlar and carbon-Kevlar hybrid fibres composites with epoxy resin have been evaluated. To achieve these goals, compressive tests were conducted for the tubes under 10mm/min loading speed. Based on the test results, the carbon/epoxy tube showed the best energy absorption capability, while carbon-Kevlar/epoxy tubes were worst. In the failure mode during crushing, both of the carbon/epoxy tubes and the glass/epoxy tubes were crushed by brittle fracturing mode. The Kevlar/epoxy tubes were collapsed by local buckling mode like steel, while the carbon-Kevlar hybrid tubes were collapsed by mixed mode of local buckling and lamina bending.