• Title/Summary/Keyword: microscopic analysis

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Study for the Standardization of Talcum and Comparison Property before and after Talcum Processing Method (골석(滑石)의 품질기준 및 포제전후의 성질비교)

  • Kook Yoon-Bum
    • Herbal Formula Science
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    • v.12 no.1
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    • pp.225-246
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    • 2004
  • Objectives: This study has been done to compare the Talcum's composition before and after using processing method and to clarify its quality and naming through the historical herbal books. Methods: I studied the Talcum and processed Talcum by physical and chemical method which contain microscopic analysis, X-ray diffraction analysis, thermal analysis, XRF, ICP, etc, to compare the compositions and its characters. Results: Talcum is a magnesium hydroxidfe(($Mg_3[Si_4O_{10}][OH]_2$)). Talcum contains a main ingredients of MgO 29.03-30.40%(31.70%), $SiO_2$ $62.00{\sim}62.40%(63.50%)$, $H_2O$ $4.40{\sim}4.85%(4.80%)$ and small ingredients, also. Conclusion: A radio-element contents of U, Th contain less than average contents of the lithosphere's U 1.8ppm, Th 7.2ppm. There are two sorts of Talcum which are a northern Talcum(solid Talcu) and southern Talcum(soft Talcum). A northern natural products of Talcum(solid Talcum) are used mostly in korea and china.

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Fracture Mechanism of Gas Turbine Compressor Blades in a Combined Cycle Power Plant (복합화력발전소 가스터빈 압축기 블레이드에 대한 손상원인 고찰)

  • Yang, Kyeong-Hyeon;Song, Oh-Seop;Cho, Cheul-Whan;Yun, Wan-No;Jung, Nam-Geun
    • Transactions of the Korean Society for Noise and Vibration Engineering
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    • v.20 no.11
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    • pp.1025-1032
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    • 2010
  • Gas turbine compressor blades used in a combined cycle power plant are possibly damaged and fractured during their operation. There are two possible causes of the failure of compressor blades; one is a defect of material quality which can be detected through some microscopic inspections for the fracture section, the other is high cycle fatigue problem caused by vibration and can be diagnosed by carrying out dynamic characteristics analysis for the blades. In this paper, in order to determine the cause of the failure of compressor blades in a combined cycle power plant, examination of the fracture section and the propagation mechanism of the crack via stress analysis are performed. Dynamic characteristics analysis via FRF estimation is also performed to identify the cause of failure.

Characteristic of GaN Growth on the Periodically Patterned Substrate for Several Reactor Configurations (반응로 형상에 따른 주기적으로 배열된 패턴위의 GaN 성장 특성)

  • Kang, Sung-Ju;Kim, Jin-Taek;Pak, Bock-Choon;Lee, Cheul-Ro;Baek, Byung-Joon
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.31 no.3 s.258
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    • pp.225-233
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    • 2007
  • The growth of GaN on the patterned substances has proven favorable to achieve thick, crack-free GaN layers. In this paper, numerical modeling of transport and reaction of species is performed to estimate the growth rate of GaN from tile reaction of TMG(trimethly-gallium) and ammonia. GaN growth rate was estimated through the model analysis including the effect of species velocity, thermal convection and chemical reaction, and thermal condition for the uniform deposition was to be presented. The effect of shape and construction of microscopic pattern was also investigated using a simulator to perform surface analysis, and a review was done on the quantitative thickness and shape in making GaN layer on the pattern. Quantitative analysis was especially performed about the shape of reactor geometry, periodicity of pattern and flow conditions which decisively affect the quality of crystal growth. It was found that the conformal deposition could be obtained with the inclination of trench ${\Theta}>125^{\circ}$. The aspect ratio was sensitive to the void formation inside trench and the void located deep in trench with increased aspect ratio.

Analysis of Nonfibrous Matters in the Textiles Exhumed from Keumreung-Ri, Pajoo Application of KS Test Method (파주 금릉리 출토복식의 섬유외 성분 연구 -KS 시험규격의 활용을 중심으로-)

  • 안춘순;조한국
    • Journal of the Korean Society of Clothing and Textiles
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    • v.22 no.6
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    • pp.772-780
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    • 1998
  • The purpose of this research was to investigate the fiber content of and the characteristics of non-fibrous matters within the textiles exhumed from Keumreung-Ri, Pajoo of Kyunggi-do. Various microscopic methods' and the IR spectroscopy were used for the identification of fibers. The KS K 0251 Test Method as well as the IR spectroscopy and the SEM were used for the analysis of econ-fibrous matters. Fiber identification showed that each of the Pajoo samples were composed either of silk, cotton, or ramie. The results of the analysis of non-fibrous matters were as follows. The amount of water-extracted compound exceeded that of chloroform-extracted compound in both Pajoo 2 and Pajoo 5 samples. In Pajoo 5 sample which have already been dry cleaned using the mixed solution of n-hexane and n-dacane, the amount of chloroform extracted compound was 0% of the total extracted matter. The enzyme and HCI disintegration steps further removed the soils those were nonsoluble in water or chloroform. The most extraction was achieved at the HCI extraction stage.

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Characterizing Barium Titanate Piezoelectric Material Using the Finite Element Method

  • Butt, Zubair;Rahman, Shafiq Ur;Pasha, Riffat Asim;Mehmood, Shahid;Abbas, Saqlain;Elahi, Hassan
    • Transactions on Electrical and Electronic Materials
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    • v.18 no.3
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    • pp.163-168
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    • 2017
  • The aim of the current research was to develop and present an effective methodology for simulating and analyzing the electrical and structural properties of piezoelectric material. The finite element method has been used to make precise numerical models when dielectric, piezoelectric and mechanical properties are known. The static and dynamic responses of circular ring-shaped barium titanate piezoelectric material have been investigated using the commercially available finite element software ABAQUS/CAE. To gain insight into the crystal morphology and to evaluate the purity of the material, a microscopic study was conducted using a scanning electron microscope and energy dispersive x-ray analysis. It is found that the maximum electrical potential of 6.43 V is obtained at a resonance frequency of 35 Hz by increasing the vibrating load. The results were then compared with the experimentally predicted data and the results agreed with each other.

Molecular Phylogeny and Morphology of Mycosphaerella nawae, the Causal Agent of Circular Leaf Spot on Persimmon

  • Lee, Seung-Yeol;Lim, Yang-Sook;Jung, Hee-Young
    • Mycobiology
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    • v.44 no.4
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    • pp.191-201
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    • 2016
  • In this study, the phylogeny and morphology of Mycosphaerella nawae (Dothideomycetes, Ascomycota) were examined using Korean and Japanese isolates, to establish the phylogenetic relationship between M. nawae and its allied species. Korean and Japanese isolates of M. nawae were collected from circular leaf spot-diseased leaves and were confirmed based on internal transcribed spacer (ITS) sequence data. Phylogenetic analysis was conducted using multiple genes, including the ITS region, 28S rDNA, ${\beta}-tubulin$, translation elongation $factor-1{\alpha}$, and actin genes. Our results revealed that M. nawae is closely related to members of the genus Phaeophleospora but are distant from the Ramularia spp. In addition, microscopic analysis revealed pseudothecia on the adaxial and abaxial surface of overwintered diseased leaves (ODL) and only on the abaxial surface of diseased leaves. Ascospores are oval to fusiform, one-septate, tapered at both ends, $1.7{\sim}3.1{\times}8.1{\sim}14.1{\mu}m$, and were observed in ODL. Conidia are oval, guttulate, one-septate, $3.5{\sim}4.9{\times}12.8{\sim}19.8{\mu}m$, and barely discernable on 30-day cultures. To our knowledge, this is the first report on the phylogeny of M. nawae, which is closely related to the genus Phaeophleospora, especially P. scytalidii.

Immunoelectron Microscopic Localization and Analysis of Herpes simplex Virus Type 2 Antigens (전자현미경 기법을 이용한 Herpes simplex 2형 바이러스 항원의 면역학적 분석)

  • 김천식;오명환
    • Korean Journal of Microbiology
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    • v.40 no.1
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    • pp.23-28
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    • 2004
  • Antigenic analysis of Herpes simplex type 2 virus was performed and its major antigen was localized using an immunoelectron microscopy. Antigens of 32, 43, 59 and 69 kDa were constantly expressed during the course of infection for 48 hr in the infected Vero cell. An antigen of 51 kDa was turned out to be the major one in inducing a immune response in Western-blot analysis. The 51 kDa antigen was localized on the surface of HSV-2 by immunoelectron microscopy using colloidal golds and anti-HSV 2 polyc1onal antibody. Immunofluorescence assay indicated that viral antigens were found throughout the infected cell and, especially, on the surface of the cell.

Role of Annexin A5 on Mitochondria-Dependent Apoptosis Induced by Tetramethoxystilbene in Human Breast Cancer Cells

  • Hong, Mihye;Park, Nahee;Chun, Young-Jin
    • Biomolecules & Therapeutics
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    • v.22 no.6
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    • pp.519-524
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    • 2014
  • We have previously shown that 2,4,3',5'-tetramethoxystilbene (TMS), a trans-stilbene analogue, induces apoptosis in human cancer cells. However, the detailed mechanisms of mitochondria-dependent apoptosis induced by TMS are not fully understood. In the present study, the possible roles of annexin A5 in TMS-mediated apoptosis were investigated in MCF7 human breast cancer cells. Quantitative real-time PCR analysis and Western blot analysis showed that the expression of annexin A5 was strongly increased in TMS-treated cells. TMS caused a strong translocation of annexin A5 from cytosol into mitochondria. Confocal laser scanning microscopic analysis clearly showed that TMS induced translocation of annexin A5 into mitochondria. TMS increased the expression and oligomerization of voltage-dependent anion channel (VDAC) 1, which may promote mitochondria-dependent apoptosis through disruption of mitochondrial membrane potential. When cells were treated with TMS, the levels of Bax, and Bak as well as annexin A5 were strongly enhanced. Moreover, we found that the cytosolic release of apoptogenic factors such as cytochrome c, or apoptosis-inducing factor (AIF) in mitochondria was markedly increased. Annexin A5 depletion by siRNA led to decreased proapoptotic factors such as Bax, Bak, and annexin A5. Taken together, our results indicate that annexin A5 may play an important role in TMS-mediated mitochondrial apoptosis through the regulation of proapoptotic proteins and VDAC1 expression.

Uncertainty quantification in decay heat calculation of spent nuclear fuel by STREAM/RAST-K

  • Jang, Jaerim;Kong, Chidong;Ebiwonjumi, Bamidele;Cherezov, Alexey;Jo, Yunki;Lee, Deokjung
    • Nuclear Engineering and Technology
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    • v.53 no.9
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    • pp.2803-2815
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    • 2021
  • This paper addresses the uncertainty quantification and sensitivity analysis of a depleted light-water fuel assembly of the Turkey Point-3 benchmark. The uncertainty of the fuel assembly decay heat and isotopic densities is quantified with respect to three different groups of diverse parameters: nuclear data, assembly design, and reactor core operation. The uncertainty propagation is conducted using a two-step analysis code system comprising the lattice code STREAM, nodal code RAST-K, and spent nuclear fuel module SNF through the random sampling of microscopic cross-sections, fuel rod sizes, number densities, reactor core total power, and temperature distributions. Overall, the statistical analysis of the calculated samples demonstrates that the decay heat uncertainty decreases with the cooling time. The nuclear data and assembly design parameters are proven to be the largest contributors to the decay heat uncertainty, whereas the reactor core power and inlet coolant temperature have a minor effect. The majority of the decay heat uncertainties are delivered by a small number of isotopes such as 241Am, 137Ba, 244Cm, 238Pu, and 90Y.

McCARD/MIG stochastic sampling calculations for nuclear cross section sensitivity and uncertainty analysis

  • Ho Jin Park
    • Nuclear Engineering and Technology
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    • v.54 no.11
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    • pp.4272-4279
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    • 2022
  • In this study, a cross section stochastic sampling (S.S.) capability is implemented into both the McCARD continuous energy Monte Carlo code and MIG multiple-correlated data sampling code. The ENDF/B-VII.1 covariance data based 30 group cross section sets and the SCALE6 covariance data based 44 group cross section sets are sampled by the MIG code. Through various uncertainty quantification (UQ) benchmark calculations, the McCARD/MIG results are verified to be consistent with the McCARD stand-alone sensitivity/uncertainty (S/U) results and the XSUSA S.S. results. UQ analyses for Three Mile Island Unit 1, Peach Bottom Unit 2, and Kozloduy-6 fuel pin problems are conducted to provide the uncertainties of keff and microscopic and macroscopic cross sections by the McCARD/MIG code system. Moreover, the SNU S/U formulations for uncertainty propagation in a MC depletion analysis are validated through a comparison with the McCARD/MIG S.S. results for the UAM Exercise I-1b burnup benchmark. It is therefore concluded that the SNU formulation based on the S/U method has the capability to accurately estimate the uncertainty propagation in a MC depletion analysis.